CAS No.124-63-0,Methanesulfonyl chloride Suppliers

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Synthetic route

: 624-92-0
Dimethyldisulphide

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With hydrogenchloride; manganese(IV) oxide; potassium sulfate; water at 60 - 90℃; for 22h; Reagent/catalyst; Temperature; Large scale;	99.81%
With chloro-trimethyl-silane; potassium nitrate In dichloromethane at 50℃; for 8h;	90%

: 868-84-8
S,S-dimethyl dithiocarbonate

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With water; chlorine at 5 - 10℃; for 0.25h;	95%

: 2344-80-1
Chloromethyltrimethylsilane

A: 1719-57-9
Chloro(chloromethyl)dimethylsilane

B: 20991-92-8
sulfate de bis-(dimethylchloromethylsilyle)

C: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With chlorosulfonic acid at 50 - 80℃;	A n/a B 92% C n/a

...Expand

: 766-92-7
[(methylthio)methyl]-benzene

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With hydrogenchloride; iodosylbenzene for 0.0833333h; Chlorination; oxidation;	91%
With hydrogenchloride; iodosylbenzene for 0.0833333h;	91 % Chromat.

: 71954-24-0
N-chlorodimesylamine

: 3049-24-9
diphenyl phenylphosphonate

A: 102173-66-0
N-Mesyl-triphenoxyphosphinimid

B: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
In dichloromethane for 18h;	A 82% B n/a

...Expand

: 867-44-7
S-Methylisothiourea sulfate

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With tert-butylhypochlorite In water; acetonitrile at 0 - 20℃;	79%
In diethyl ether; water at 0 - 20℃; for 0.5h; Green chemistry;	0.808 g

: 34557-54-5
methane

A: 75-09-2
dichloromethane

B: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With sulfur dioxide; chlorine at 25℃; under 2250.23 Torr; for 1h; Concentration; Wavelength; Irradiation;	A n/a B 69%

: 71954-24-0
N-chlorodimesylamine

A: 29651-24-9
N-Mesyl-trichlorphosphinimid

B: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With phosphorus trichloride In dichloromethane; chloroform for 12h;	A 61% B n/a

: 34557-54-5
methane

A: 56-23-5
tetrachloromethane

B: 74-87-3
methylene chloride

C: 75-09-2
dichloromethane

D: 67-66-3
chloroform

E: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With hydrogenchloride; sulfur dioxide; chlorine at 63 - 67℃; under 6750.68 Torr; Photolysis;	A n/a B n/a C n/a D n/a E 55%

...Expand

: 34557-54-5
methane

A: 75-09-2
dichloromethane

B: 67-66-3
chloroform

C: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With sulfur dioxide; chlorine at 65℃; under 2250.23 Torr; for 1h; Temperature; Irradiation;	A n/a B n/a C 54.9%

...Expand

: 5926-38-5
(dichloromethyl)trimethylsilane

A: 124-63-0
methanesulfonyl chloride

B: 107716-52-9
C3H7Cl3O3SSi

C: 107716-51-8
C3H7Cl3O3SSi

D: 107716-53-0
C6H14Cl4O4SSi2

Conditions

Conditions	Yield
at 90 - 100℃; Further byproducts given;	A n/a B 51% C n/a D n/a

...Expand

: 75-75-2
methanesulfonic acid

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With 1,3,5-trichloro-2,4,6-triazine; triethylamine In acetone for 20h; Heating;	47%
With thionyl chloride at 95℃;
With phosphorus trichloride at 80℃;

: 34557-54-5
methane

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With sulfur dioxide; chlorine at -10 - 110℃; for 2h; Product distribution / selectivity; Sealed reactor;	47%
With sulfuryl dichloride; sulfur trioxide; dihydrogen peroxide; rhodium(III) chloride; urea In sulfuric acid at 60℃; under 36201.3 Torr; for 12h;	1.9 mmol

: 34557-54-5
methane

A: 67-66-3
chloroform

B: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With sulfur dioxide; chlorine at 25℃; under 2250.23 Torr; for 1h; Temperature; Irradiation;	A n/a B 43.3%

: 676-85-7
methylsulphinyl chloride

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With chlorine	13.5%

: 556-64-9
methyl thiocyanate

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With water; chlorine
With water; chlorine

: 917-64-6
methyl magnesium iodide

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With sulfuryl dichloride; diethyl ether at 10℃;

: 75-18-3
dimethylsulfide

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With water; chlorine

: 5813-48-9
Methanesulfenyl chloride

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With diethyl ether; nitric acid at -15℃;

: 14527-26-5, 867-44-7
2-methylisothiourea sulphate

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With water; chlorine at 10 - 15℃;

: 7143-01-3
Methanesulfonic anhydride

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With hydrogenchloride at 105℃;

: 592-76-7
1-Heptene

: 5799-68-8
methanedisulfonyl chloride

A: 5799-71-3
1,3-dichlorooctane

B: 5799-72-4
3-chloro-octanesulfonyl chloride

C: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With dibenzoyl peroxide In benzene Heating;

...Expand

: 64258-22-6
α,α-Dichlor-dimethylsulfid

: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With water; chlorine In acetic acid

: 676-85-7
methylsulphinyl chloride

A: 2949-92-0
methanethiosulfonic acid S-methyl ester

B: 75-18-3
dimethylsulfide

C: 13882-12-7
S-methyl methanethiosulfinate

D: 14128-56-4
methyl methanesulfinyl sulfone

E: 19186-23-3
Zinc methanesulfinate

F: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With zinc In various solvent(s) at -30℃; for 1.5h; Mechanism; Product distribution; var. solv., var. time, var. temp.;	A 7 % Spectr. B 1 % Spectr. C 3 % Spectr. D 1 % Spectr. E 5 % Spectr. F 9 % Spectr.

...Expand

: 676-85-7
methylsulphinyl chloride

A: 2949-92-0
methanethiosulfonic acid S-methyl ester

B: 75-18-3
dimethylsulfide

C: 22224-96-0
S-(chloromethyl) methanesulphonothioate

D: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
triethylamine In diethyl ether at 22 - 24℃; for 24h; Product distribution; other amines;	A 6 % Spectr. B 5 % Spectr. C 27 % Spectr. D 3 % Spectr.

...Expand

: 67-68-5
dimethyl sulfoxide

A: 2949-92-0
methanethiosulfonic acid S-methyl ester

B: 67-71-0
dimethylsulfone

C: 26394-12-7
hydrochloric acid, dimethyl sulphoxide

D: 124-63-0
methanesulfonyl chloride

Conditions

Conditions	Yield
With chlorine In dichloromethane at -0.1℃;
With chlorine In dichloromethane at -0.1℃; Further byproducts given;

...Expand

: 2081-44-9
Tetrahydro-pyran-4-ol

: 124-63-0
methanesulfonyl chloride

: 134419-59-3
4-oxanyl methanesulfonate

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 0 - 20℃; for 2.5h;	100%
With triethylamine In dichloromethane at 0 - 20℃; for 2.5h;	100%
With triethylamine In dichloromethane at 0℃; for 1.5h;	100%

: 67-56-1
methanol

: 124-63-0
methanesulfonyl chloride

: 66-27-3
Methyl methanesulfonate

Conditions

Conditions	Yield
Stage #1: methanol With triethylamine In dichloromethane at 25℃; Stage #2: methanesulfonyl chloride In dichloromethane at 0 - 20℃;	100%
With pyridine; diethyl ether at -30℃;
With triethylamine

: 71-23-8
propan-1-ol

: 124-63-0
methanesulfonyl chloride

: 1912-31-8
propyl methanesulfonate

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 0 - 20℃; for 1h;	100%
With pyridine 1.) from -20 deg C to 30 deg C, 2.) room temp., 2 h;	65%
With pyridine at 0℃;

: 100-02-7
4-nitro-phenol

: 124-63-0
methanesulfonyl chloride

: 20455-07-6
p-nitrophenyl methanesulfonate

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 0 - 20℃; for 0.75h;	100%
With triethylamine In dichloromethane at 0 - 20℃;	98%
With triethylamine In ethyl acetate at 0 - 20℃; for 0.166667h; Green chemistry;	97%

: 821-09-0
n-Pent-4-enyl alcohol

: 124-63-0
methanesulfonyl chloride

: 64818-35-5
4-pentenyl mesylate

Conditions

Conditions	Yield
With triethylamine In dichloromethane at -15℃; for 1h; Green chemistry;	100%
With triethylamine In dichloromethane at -5℃; for 0.666667h;	98%
With triethylamine In dichloromethane at 0 - 20℃; for 91312.5h; Inert atmosphere;	98%

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