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Conditions | Yield |
---|---|
With methanol; sodium hydroxide |
diphenylantimony(V) bromide oxide
sodium cacodylate
[(Sb(C6H5)2)2(O)2(O2As(CH3)2)2]
Conditions | Yield |
---|---|
In dichloromethane reflux (24 h); filtration, removal of solvent, crystn. (CHCl3/hexane); elem. anal.; | 86% |
Conditions | Yield |
---|---|
In ethanol; water stirring MoO3*H2O in aq. H2O2 at 30°C until a soln. was obtained,addn. of NaO2AsMe2 in EtOH at room temp. followed by addn. of (Me4N)Cl in H2O; addn. of EtOH, cooling to 4°C, filtration, washing (cold EtOH; Et2O), drying in air; elem. anal.; | 85% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 3h; Darkness; | 82% |
sodium cacodylate
μ-oxo-bis[bromotriphenylantimony(V)]
[(Sb(C6H5)3)2(O)(O2As(CH3)2)2]
Conditions | Yield |
---|---|
In dichloromethane reflux (20 h); filtration, removal of solvent (vac.), dissoln. (CHCl3), diffusion of hexane into the soln.; elem. anal.; | 74% |
Conditions | Yield |
---|---|
In ethanol; water stirring MoO3*H2O in aq. H2O2 at 30°C until a soln. was obtained,addn. of NaO2AsMe2 in EtOH at room temp. followed by addn. of (n-Bu4N)C l in H2O; addn. of EtOH, cooling to 4°C, filtration, washing (cold EtOH; Et2O), drying in air; elem. anal.; | 60% |
sodium cacodylate
N,N-bis[2-(4,5-dimethyl)benzimidazolylmethyl]-N',N'-bis(2-pyridylmethyl)-1,3-diamino-2-propanol
Conditions | Yield |
---|---|
In water; acetonitrile 2 equiv. of aq. Zn-salt soln. and 1 equiv. of aq. As-compd. soln. were added to MeCN soln. of N-base; crystn. by diffusion of Et2O into the soln. for 4 d, elem. anal.; | 55% |
Conditions | Yield |
---|---|
Stage #1: palladium diacetate; sodium cacodylate In aq. buffer at 20℃; for 48h; pH=7; Stage #2: water | 3% |
sodium cacodylate
Conditions | Yield |
---|---|
With hydrogen selenide In ethanol |
Conditions | Yield |
---|---|
In water at 37℃; for 1h; |
Conditions | Yield |
---|---|
In water formation in aq. soln. of (Cr(H2O)6)(NO3)3 and Na cacodylate (molar ratio 1:1);; not isolated;; |
Conditions | Yield |
---|---|
In water formation in aq. soln. of (Cr(H2O)6)(NO3)3 and Na-cacodylate (molar ratio 1:2);; not isolated;; |
Conditions | Yield |
---|---|
In benzene room temp.; crystn. (several weeks); |
Conditions | Yield |
---|---|
In methanol; ethanol elem. anal.; |
methanol
sodium cacodylate
iron(III) chloride
N,N,N′,N′-tetrakis(2-benzimidazolylmethyl)-2-hydroxo-1,3-diaminopropane
Conditions | Yield |
---|---|
In methanol; acetonitrile |
N-methyl-N,N',N'-tris(2-benzimidazolylmethyl)-2-hydroxy-1,3-diaminopropane
sodium cacodylate
iron(III) chloride
Conditions | Yield |
---|---|
In methanol equimolar amts. of perchlorate, chloride and arsinate; crystn. (several days); |
Conditions | Yield |
---|---|
With perchloric acid In water aq. solns. of Me2AsO2Na and Na2MoO4*2H2O mixed; pH ajusted to 4.0 by adnn. of HClO4; aq. soln. of CsCl added; ppt. filtered off, washed with cold H2O, dried in air; elem. anal.; |
Conditions | Yield |
---|---|
With perchloric acid In water aq. solns. of Me2AsO2Na and Na2MoO4*2H2O mixed, pH adjusted to 4.0 by addn. of HClO4; concd.; ppt. isolated; |
methanol
sodium cacodylate
diphenyltin(IV) dichloride
[Ph(Cl)Sn(O2AsMe2)(μ-OMe)]2
Conditions | Yield |
---|---|
In methanol byproducts: NaCl, C6H6; 1 equiv. of As-compd. in MeOH added to soln. of Sn-compd. in MeOH at ambient temp.; soln. filtered after a week, filtrate stored in an open flask at ambienttemp. for 9 d, crystals filtered off; |
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