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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Tetrakis Hydroxymethyl Phosphonium Chloride supplier in China

Cas:124-64-1

Min.Order:1 Kilogram

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Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb

THPC(Tetrakis(hydroxymethyl)phosphonium chloride)

Cas:124-64-1

Min.Order:1 Kilogram

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Tetrakis(hydroxymethyl)phosphonium chloride Cas 124-64-1 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, F

Tetrakis(hydroxymethyl)phosphonium chloride Cas 124-64-1

Cas:124-64-1

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

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Hefei TNJ chemical industry co.,ltd

Do you want to buy Tetrakis Hydroxymethyl Phosphonium Chloride THPC CAS 124-64-1 TNJ offers the best quality and lowest price Tetrakis Hydroxymethyl Phosphonium Chloride THPC.For more informations please mail sales23@tnjchem.com Properties

Tetrakis Hydroxymethyl Phosphonium Chloride THPC CAS 124-64-1

Cas:124-64-1

Min.Order:1 Metric Ton

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Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1

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Type:Other

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

Tetrakis Hydroxymethyl Phosphonium Chloride (THPC)

Cas:124-64-1

Min.Order:1 Metric Ton

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Chemwill Asia Co., Ltd.

Tetrakis(hydroxymethyl)phosphonium chloride Manufacturer Factory CAS 124-64-1 Tetrakis(hydroxymethyl)phosphonium chloride Manufacturer High quality Best price In stock factory CAS 124-64-1 Tetrakis(hydroxymethyl)phosphonium chloride COA TDS pric

Tetrakis(hydroxymethyl)phosphonium chloride Manufacturer Factory CAS 124-64-1

Cas:124-64-1

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Tetrakis(hydroxymethyl)phosphonium chloride Basic information Product Name: Tetrakis(hydroxymethyl)phosphonium chloride Synonyms: THPC;TETRA(HYDROXYMETHYL)PHOSPHONI

TIANFU-CHEM Tetrakis(hydroxymethyl)phosphonium chloride 124-64-1

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1 Gram

FOB Price: $1.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 124-64-1 with best quality

Cas:124-64-1

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name Tetrakis(hydroxymethyl)phosphonium chloride Molecular Formula C10H24O12P2 CAS 124-64-1

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:Clear light pink or yellow-green solution Storage:Room temperature Package:200kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Any port in china

High Quality Tetrakis(hydroxymethyl)phosphonium chloride (THPC)

Cas:124-64-1

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Phosphonium,tetrakis(hydroxymethyl)-, chloride (1:1) 124-64-1

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:Clear colorless liquid Storage:keep in cool and

CAS 124-64-1 High quality Tetrakis Hydroxymethyl Phosphonium Chloride supplier in China THPC

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Phosphonium,tetrakis(hydroxymethyl)-, chloride (1:1)

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

Tetrakis(hydroxymethyl)phosphonium chloride CAS NO.124-64-1

Cas:124-64-1

Min.Order:10 Gram

Negotiable

Type:Trading Company

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in lead acetate, diphenyl ethylamine and other chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countrie

Tetrakis(hydroxymethyl)phosphonium chloride CAS No.: 124-64-1 CAS No.: 124-64-1

Cas:124-64-1

Min.Order:1 Kilogram

FOB Price: $100.0

Type:Trading Company

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Lab/Research institutions

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Lonwin Chemical Group Limited

Tetrakis(hydroxymethyl)phosphonium chloride CAS:124-64-1 Specification Item Specification Appearance Clear Colorless Liquid Assay 98%min Density 1.341 g/mL at 25 °C Boiling Point 1

Factory Supply Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Phosphonium,tetrakis(hydroxymethyl)-, chloride (1:1)

Cas:124-64-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Tetrakis Hydroxymethyl Phosphonium Chloride

Cas:124-64-1

Min.Order:0

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Type:Manufacturers

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: Tetrakis(Hydroxymethyl)phosphonium Chloride CAS No.:124-64-1 Molecule Formula:C10H24O12P2 Molecule Weight:398.24 Purity: 80.0% Package: 180kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard

Best Quality Tetrakis(Hydroxymethyl)phosphonium Chloride

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Tetrakis(hydroxymethyl)phosphonium chloride

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Falcon Life Sciences Pvt. Ltd

Water Treatment THPC/Tetrakis(hydroxymethyl)phosphonium Chloride 124-64-1 CAS No.: 124-64-1 Type.: Water treatment Appearance: Clear, weak straw yellow liquid Molecular Formula: C4H12ClO4P Shelf Life: - Min Order Quantity: As requirements

Water Treatment THPC/Tetrakis(hydroxymethyl)phosphonium Chloride 124-64-1

Cas:124-64-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Synthetic route

formaldehyd
50-00-0

formaldehyd

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Conditions
ConditionsYield
Stage #1: formaldehyd With phosphorus; bis(tri-n-butyltin)oxide; 1,1'-azobis(1-cyanocyclohexanenitrile) In ethanol at 20℃; for 16h;
Stage #2: With hydrogenchloride In 1,4-dioxane; ethanol at 20℃; for 4h; Catalytic behavior; Reagent/catalyst; Cooling with liquid nitrogen;
80%
With hydrogenchloride; phosphorus hydrogen; water at 80℃;
With hydrogenchloride; phosphan
hydrogenchloride
7647-01-0

hydrogenchloride

formaldehyd
50-00-0

formaldehyd

phosphorus

phosphorus

tri-n-butyl-tin hydride
688-73-3

tri-n-butyl-tin hydride

A

tributyltin chloride
1461-22-9

tributyltin chloride

B

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Conditions
ConditionsYield
Stage #1: phosphorus; tri-n-butyl-tin hydride In toluene at 20℃; for 16h; Schlenk technique; Irradiation;
Stage #2: formaldehyd In ethanol at 20℃; for 16h;
Stage #3: hydrogenchloride In 1,4-dioxane; ethanol at 20℃; for 2h; Cooling with liquid nitrogen;
A 96%
B 75%
formaldehyd
50-00-0

formaldehyd

phosphan
7803-51-2

phosphan

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Conditions
ConditionsYield
With hydrogenchloride In water passing PH3 in aq. formaldehyde soln. containing HCl at ambient temp.;;
With hydrogenchloride In water passing PH3 in aq. formaldehyde soln. containing HCl at 80 °C;;
With HCl In water passing PH3 in aq. formaldehyde soln. containing HCl at 80 °C;;
With HCl In water passing PH3 in aq. formaldehyde soln. containing HCl at ambient temp.;;
formaldehyd
50-00-0

formaldehyd

phosphine

phosphine

hydrochloric acid

hydrochloric acid

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Conditions
ConditionsYield
With water
formaldehyd
50-00-0

formaldehyd

tris(hydroxymethyl)phosphine
2767-80-8

tris(hydroxymethyl)phosphine

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Conditions
ConditionsYield
With hydrogenchloride
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

tris(hydroxymethyl)phosphine
2767-80-8

tris(hydroxymethyl)phosphine

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With potassium hydroxide In methanol; water at 15 - 20℃; for 0.166667h;
Stage #2: With zinc(II) chloride; sodium sulfite In methanol; water at 25℃; Reagent/catalyst; Solvent;
98.3%
With triethylamine at 60℃; for 4h; Elimination;95%
With sodium hydroxide
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

p-toluidine
106-49-0

p-toluidine

Tetrakis-(p-tolylamino-methyl)-phosphonium; chloride

Tetrakis-(p-tolylamino-methyl)-phosphonium; chloride

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;95%
In ethanol for 2h;
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

1-amino-naphthalene
134-32-7

1-amino-naphthalene

C44H40N4P(1+)*Cl(1-)

C44H40N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;100%
1-amino-4-chloronaphthalene
4684-12-2

1-amino-4-chloronaphthalene

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

C44H36Cl4N4P(1+)*Cl(1-)

C44H36Cl4N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;91%
4-Bromo-1-naphthylamine
2298-07-9

4-Bromo-1-naphthylamine

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

C44H36Br4N4P(1+)*Cl(1-)

C44H36Br4N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;85%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

4-methoxy-aniline
104-94-9

4-methoxy-aniline

C32H40N4O4P(1+)*Cl(1-)

C32H40N4O4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;97%
2-Fluoroaniline
348-54-9

2-Fluoroaniline

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

C28H28F4N4P(1+)*Cl(1-)

C28H28F4N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;97%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

anthranilic acid nitrile
1885-29-6

anthranilic acid nitrile

C32H28N8P(1+)*Cl(1-)

C32H28N8P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;94%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

m-cyanoaniline
2237-30-1

m-cyanoaniline

C32H28N8P(1+)*Cl(1-)

C32H28N8P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;92%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

4-Aminobenzonitrile
873-74-5

4-Aminobenzonitrile

C32H28N8P(1+)*Cl(1-)

C32H28N8P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;91%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

4-chloro-aniline
106-47-8

4-chloro-aniline

C28H28Cl4N4P(1+)*Cl(1-)

C28H28Cl4N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;90%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

p-aminoiodobenzene
540-37-4

p-aminoiodobenzene

C28H28I4N4P(1+)*Cl(1-)

C28H28I4N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;97%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

4-aminoethylbenzene
589-16-2

4-aminoethylbenzene

C36H48N4P(1+)*Cl(1-)

C36H48N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;93%
4-propylaniline
2696-84-6

4-propylaniline

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

C40H56N4P(1+)*Cl(1-)

C40H56N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;85%
4-Isopropylaniline
99-88-7

4-Isopropylaniline

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

C40H56N4P(1+)*Cl(1-)

C40H56N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;87%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

4-fluoroaniline
371-40-4

4-fluoroaniline

C28H28F4N4P(1+)*Cl(1-)

C28H28F4N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;83%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

4-bromo-aniline
106-40-1

4-bromo-aniline

C28H28Br4N4P(1+)*Cl(1-)

C28H28Br4N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;83%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

methyl iodide
74-88-4

methyl iodide

[hydroxymethyl(methyl)phosphanyl]methanol
5958-52-1

[hydroxymethyl(methyl)phosphanyl]methanol

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With triethylamine at 20℃; for 18h;
Stage #2: methyl iodide In tetrahydrofuran at -40 - 20℃;
33%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

2-(trifluoromethyl)benzenamine
88-17-5

2-(trifluoromethyl)benzenamine

C32H28F12N4P(1+)*Cl(1-)

C32H28F12N4P(1+)*Cl(1-)

Conditions
ConditionsYield
In methanol at 20℃; for 2h;72%
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

tris(hydroxymethyl)phosphine sulfide
1067-13-6

tris(hydroxymethyl)phosphine sulfide

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With triethylamine In N,N-dimethyl-formamide; toluene at 60℃; for 1h; Inert atmosphere;
Stage #2: With octasulfur In N,N-dimethyl-formamide; toluene Inert atmosphere;
94%
potassium tetrachloropalladate(II)

potassium tetrachloropalladate(II)

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

C3H9Cl3O3PPd(1-)*K(1+)

C3H9Cl3O3PPd(1-)*K(1+)

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With potassium hydroxide In methanol
Stage #2: potassium tetrachloropalladate(II) In methanol for 336h; Inert atmosphere;
37%
4‐bromobutylferrocene
129826-46-6

4‐bromobutylferrocene

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Fc(CH2)4P(CH2OH)2
1599441-98-1

Fc(CH2)4P(CH2OH)2

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With potassium hydroxide In methanol for 1h; Schlenk technique; Inert atmosphere;
Stage #2: 4‐bromobutylferrocene In methanol for 21h; Schlenk technique; Inert atmosphere; Reflux;
Stage #3: With triethylamine In diethyl ether; water for 1h; Schlenk technique; Inert atmosphere;
ω-bromohexane ferrocene
136237-36-0

ω-bromohexane ferrocene

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Fc(CH2)6P(CH2OH)2
1599442-01-9

Fc(CH2)6P(CH2OH)2

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With potassium hydroxide In methanol for 1h; Schlenk technique; Inert atmosphere;
Stage #2: ω-bromohexane ferrocene In methanol; ethanol for 20.5h; Schlenk technique; Inert atmosphere; Reflux;
Stage #3: With triethylamine In diethyl ether; water for 2h; Schlenk technique; Inert atmosphere;
11-bromo-n-undecylferrocene

11-bromo-n-undecylferrocene

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

Fc(CH2)11P(CH2OH)2
1599442-03-1

Fc(CH2)11P(CH2OH)2

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With potassium hydroxide In methanol for 1h; Schlenk technique; Inert atmosphere;
Stage #2: 11-bromo-n-undecylferrocene In methanol for 20.5h; Schlenk technique; Inert atmosphere; Reflux;
Stage #3: With triethylamine In diethyl ether; water for 2h; Schlenk technique; Inert atmosphere;
N-trimethyl-N-ruthenocenylammonium iodide

N-trimethyl-N-ruthenocenylammonium iodide

tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

RcCH2P(CH2OH)2
1599442-18-8

RcCH2P(CH2OH)2

Conditions
ConditionsYield
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With potassium hydroxide In methanol for 1h; Schlenk technique; Inert atmosphere;
Stage #2: N-trimethyl-N-ruthenocenylammonium iodide In methanol for 20h; Schlenk technique; Inert atmosphere; Reflux;
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

1-Bromo-4-fluorobenzene
460-00-4

1-Bromo-4-fluorobenzene

A

tri(4-fluorophenyl)phosphine oxide
18437-79-1

tri(4-fluorophenyl)phosphine oxide

B

bis(4-fluorophenyl)methylphosphine oxide

bis(4-fluorophenyl)methylphosphine oxide

Conditions
ConditionsYield
With 3 A molecular sieve; potassium carbonate; [(o-Tol)2PC6H4CH2Pd(OAc)]2 In N,N-dimethyl acetamide at 130℃; for 17h;A 10%
B 40%
With 3 A molecular sieve; potassium carbonate; [(o-Tol)2PC6H4CH2Pd(OAc)]2 In N,N-dimethyl acetamide at 130℃; for 17h;A 23 % Chromat.
B 13 % Chromat.
tetrakis(hydroxymethyl)phosphonium chloride
124-64-1

tetrakis(hydroxymethyl)phosphonium chloride

tri(hydroxymethyl)phosphine oxide
1067-12-5

tri(hydroxymethyl)phosphine oxide

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 50℃; for 2h; Elimination;100%
With barium carbonate In water
With sodium hydroxide
With sodium hydroxide; dihydrogen peroxide at 70 - 80℃; for 1h;
With sodium hydroxide at 20℃; Rate constant;
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