CAS No.88-17-5,2-Aminobenzotrifluoride Suppliers

Jiangsu Huaen Energy Co., Ltd.

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Dayang Chem (Hangzhou) Co.,Ltd.

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Wuhan Fortuna Chemical Co.,Ltd

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Henan Allgreen Chemical Co.,Ltd

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply α,α,α-trifluoro-o-toluidine

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Chemwill Asia Co., Ltd.

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Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

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Henan Tianfu Chemical Co., Ltd.

Product Name: 2-Aminobenzotrifluoride Synonyms: α,α,α-Trifluoro-o-toluidine, 2-Aminobenzotrifluoride;2-Aminobenzotrifluoride ,99%;o-Amino-α,α,α-trifluorotoluene;2-(Trifluoromethyl)aniline,α,&al

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Henan Sinotech Import&Export Corporation

Product name 2-Aminotrifluoromethylbenzene Synonyms 2-Aminobenzotrifluor CAS No. 88-17-5 Molecular weight 161.13 Molecular formula C7H6F3N

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Henan Wentao Chemical Product Co., Ltd.

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Hangzhou Keyingchem Co.,Ltd

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Hangzhou J&H Chemical Co., Ltd.

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

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Hangzhou Lingrui Chemical Co.,Ltd.

2-AminotrifluoromethylbenzeneAppearance:Colorless transparent liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...)

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HANGZHOU YUNUO CHEMICAL CO.,LTD

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Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

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Hunan chemfish Pharmaceutical co.,Ltd

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SAGECHEM LIMITED

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Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)

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Kono Chem Co.,Ltd

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GIHI CHEMICALS CO.,LIMITED

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DB BIOTECH CO., LTD

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Aecochem Corp.

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

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Antimex Chemical Limied

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Hangzhou Ocean Chemical Co., Ltd.

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Xiamen AmoyChem Co.,Ltd

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Hubei Langyou International Trading Co., Ltd

High purity 2-Aminobenzotrifluoride CAS 88-17-5 with factory price Application:High purity 2-Aminobenzotrifluoride CAS 88-17-5 with factory price

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Synthetic route

: 344-62-7
N-[2-(trifluoromethyl)phenyl]acetamide

: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With thionyl chloride In methanol at 75℃; for 3h;	94%

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 62-53-3
aniline

: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With 1-acetoxy-1,2-benziodoxol-3-one; potassium acetate In acetonitrile at 80℃; for 13h; Reagent/catalyst; Solvent; Temperature; Time;	89%

: 384-22-5
2-nitrobenzotrifluoride

: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With 1,3-dimethyl-2-imidazolidinone; sodium trimethylsilanethiolate at 185℃; for 24h;	87%
With sodium hydrogensulfide; sodium hydrogencarbonate In methanol; water for 0.5h; Heating;	68%
In water at 31 - 35℃; for 48h; reduction with baker's yeast (Saccharomyces cerevisiae);	66%

: N-(2-(trifluoromethyl)phenyl)picolinamide

: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With hydrogenchloride In ethanol	85%
With hydrogenchloride In ethanol at 100℃; for 12h;	1.13 g
With hydrogenchloride In ethanol Reflux;

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 615-36-1
2-bromoaniline

: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; sodium dodecyl-sulfate; cesium fluoride In toluene at 110℃; for 12h; Inert atmosphere;	70%

: 887144-94-7
Togni's reagent II

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With potassium carbonate In acetonitrile at 75℃; for 6h; Schlenk technique; Inert atmosphere;	A 20% B 66%
With potassium carbonate; nickel(II) hydroxide In dimethyl sulfoxide at 35℃; for 2h; Reagent/catalyst; Solvent; Temperature; Overall yield = 89 %;	A 20% B 61%
With potassium carbonate; nickel(II) hydroxide In dimethyl sulfoxide at 35℃; for 2h; Reagent/catalyst; Solvent; Inert atmosphere;	A 20% B 49%

...Expand

: 2314-97-8
iodotrifluoromethane

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With fac-tris(2-phenylpyridinato-N,C2')iridium(III); potassium carbonate In 1,2-dichloro-ethane at 20℃; for 24h; Inert atmosphere; Schlenk technique; Irradiation; regioselective reaction;	A 34% B 54%
With sulfuric acid; dihydrogen peroxide; iron(II) sulfate; dimethyl sulfoxide In water at 40 - 50℃; for 0.333333h;	A 7.2 %Spectr. B 8.5 %Spectr.
With dihydrogen peroxide; iron(II) sulfate In water; dimethyl sulfoxide	A 13 %Spectr. B 22 %Spectr.

...Expand

: 1548-68-1
1-azido-2-(trifluoromethyl)benzene

A: 90701-87-4
2-methoxy-3-trifluoromethyl-3H-azepine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In tetrahydrofuran; methanol for 15h; Irradiation;	A 49% B 5%

: 2,3,7,8-tetrafluoro-S-(trifluoromethyl)dibenzothiophenium trifluoromethanesulfonate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 30℃; for 3h; Inert atmosphere;	A 23% B 44%

...Expand

: 98-56-6
4-chlorobenzotrifluoride

: 62-53-3
aniline

A: 98-16-8
3-trifluoromethylaniline

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With 2,3,7,8-tetrafluoro-S-(trifluoromethyl)dibenzothiophenium trifluoromethanesulfonate In N,N-dimethyl-formamide at 30℃; for 3h; Reagent/catalyst; Inert atmosphere;	A 23% B 44%

...Expand

: 129922-39-0
3,7-dinitro-Se-(trifluoromethyl)dibenzoselenophenium triflate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide for 0.5h; Ambient temperature; Title compound not separated from byproducts;	A 16 % Spectr. B 39%
In N,N-dimethyl-formamide for 0.5h; Ambient temperature; Title compound not separated from byproducts;	A 16 % Spectr. B 39 % Spectr.

...Expand

: 129946-88-9
Umemoto's reagent

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 80℃; for 5h; Title compound not separated from byproducts;	A 15% B 37%
In N,N-dimethyl-formamide at 80℃; for 7h;	A 18% B 39 % Spectr.
In N,N-dimethyl-formamide at 30℃; for 3h; Inert atmosphere;	A 2% B 5%

...Expand

: 62-53-3
aniline

: 160656-66-6
S-(Trifluoromethyl)-7-nitrodibenzothiophenium-3-sulfonate

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 80℃; for 0.5h;	A 18 % Spectr. B 37%
In N,N-dimethyl-formamide at 80℃; for 0.5h;	A 18% B 37 % Spectr.
In N,N-dimethyl-formamide at 80℃; for 0.5h; Product distribution; other temperature;

...Expand

: 2,6-difluoro-S-(trifluoromethyl)dibenzothiophenium trifluoromethanesulfonate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 30℃; for 3h; Inert atmosphere;	A 17% B 37%

...Expand

: 75-63-8
Bromotrifluoromethane

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With α-picoline; sodium metabisulfite; sulfur dioxide; zinc In N,N-dimethyl-formamide at 20℃; under 2250.2 - 3750.3 Torr; for 2h; Product distribution; other alkylating reagents, other method, other pressure, temp.; various substrates;	A 20% B 36%
With α-picoline; sodium metabisulfite; sulfur dioxide; zinc In N,N-dimethyl-formamide at 20℃; under 2250.2 - 3750.3 Torr; for 2h; also with NaS2O4;	A 20% B 36%
With sulfur dioxide; zinc In N,N-dimethyl-formamide under 2250.2 - 3750.3 Torr; for 2h; Ambient temperature;	A 20% B 36%

...Expand

: 75-63-8
Bromotrifluoromethane

: 95-51-2
2-Chloroaniline

A: 433-94-3
2-chloro-6-(trifluoromethyl)benzenamine

B: 39885-50-2
2-chloro-4-(trifluoromethyl)aniline

C: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With α-picoline; sodium metabisulfite; sulfur dioxide; zinc In N,N-dimethyl-formamide at 50℃; under 2250.2 - 3750.3 Torr; for 4h;	A 21% B 21% C 14%

...Expand

: 2,8-difluoro-5-(trifluoromethyl)-5Hdibenzo[b,d]thiophen-5-ium trifluoromethanesulfonate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 30℃; for 3h; Inert atmosphere;	A 6% B 14%

...Expand

: 384-22-5
2-nitrobenzotrifluoride

A: 393-39-5
4-fluoro-2-(trifluoromethyl)aniline

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With bismuth; hydrogen fluoride In dichloromethane Yields of byproduct given;	A 12% B n/a

: 360-64-5
2-(trifluoromethyl)benzamide

: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With sodium hypobromide

: 314-11-4
N-((2-trifluoromethyl)benzene)phthalimide

: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With steam; hydrazine hydrate

: 77811-21-3
2-(2'-trifluoromethylphenyl)azo-4-phenyl-1,3,4-thiadiazol-5-one

A: 645-48-7
1-phenyl-3-thiosemicarbazide

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With sodium hydroxide; zinc In methanol Heating;

: 129922-33-4
Se-(trifluoromethyl)dibenzoselenophenium triflate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide for 20h; Ambient temperature;	A 4 % Spectr. B 7 % Spectr.
In N,N-dimethyl-formamide for 20h; Ambient temperature; Title compound not separated from byproducts;	A 4 % Spectr. B 7 % Spectr.

...Expand

: 129922-35-6
3-nitro-S-(trifluoromethyl)dibenzothiophenium triflate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide for 0.5h; Ambient temperature; Title compound not separated from byproducts;	A 11 % Spectr. B 18 % Spectr.

...Expand

: 129922-37-8
S-(trifluoromethyl)-3,7-dinitrodibenzothiophenium trifluoromethanesulfonate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide for 2h; Ambient temperature; Title compound not separated from byproducts;	A 26 % Spectr. B 57 % Spectr.

...Expand

: 55642-42-7
bis(trifluoromethyl)tellurium

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 98-16-8
3-trifluoromethylaniline

C: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 140℃; for 60h; Title compound not separated from byproducts;	A 24 % Spectr. B 21 % Spectr. C 21 % Spectr.

...Expand

: 62-53-3
aniline

: 160656-62-2
5-(trifluoromethyl)-5H-dibenzo[b,d]thiophenium-3-sulfonate

A: 455-14-1
4-trifluoromethylphenylamine

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 80℃; for 7h;	A 18 % Spectr. B 36 % Spectr.
In N,N-dimethyl-formamide at 80℃; for 7h; Product distribution; other time;

...Expand

: 129946-88-9
Umemoto's reagent

: 62-53-3
aniline

A: 132-65-0
dibenzothiophene

B: 455-14-1
4-trifluoromethylphenylamine

C: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In d7-N,N-dimethylformamide at 62℃; Kinetics; Thermodynamic data; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.);

...Expand

: 129922-37-8
S-(trifluoromethyl)-3,7-dinitrodibenzothiophenium trifluoromethanesulfonate

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 59005-75-3
3,7-dinitro-dibenzothiophene

C: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In d7-N,N-dimethylformamide at -10℃; Kinetics; Thermodynamic data; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.);

...Expand

: 62-53-3
aniline

: trifluoromethanesulfonic acid diphenyl(trifluoromethyl)sulfonium salt

A: 455-14-1
4-trifluoromethylphenylamine

B: 139-66-2
diphenyl sulfide

C: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In d7-N,N-dimethylformamide at 81.4℃; Kinetics; Thermodynamic data; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.);

...Expand

: 13668-61-6
(cyclopent-2-eneyl)acetic acid

: 88-17-5
2-(trifluoromethyl)benzenamine

: 2-cyclopent-2-enyl-N-(2-trifluoromethyl-phenyl)-acetamide

Conditions

Conditions	Yield
With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane	100%

: 463-71-8
thiophosgene

: 88-17-5
2-(trifluoromethyl)benzenamine

: 1743-86-8
2-(trifluoromethyl)phenyl isothiocyanate

Conditions

Conditions	Yield
In water at 20℃; for 12h;	100%
With sodium hydrogencarbonate In water at 0 - 20℃; for 24h; Inert atmosphere;	95%
With triethylamine In dichloromethane at 20℃; for 1h;

: 39098-97-0
2-thienylacetic acid chloride

: 88-17-5
2-(trifluoromethyl)benzenamine

: 2-(thiophen-2-yl)-N-(2-(trifluoromethyl)phenyl)acetamide

Conditions

Conditions	Yield
In tetrahydrofuran at 20℃;	100%

: 1689-71-0
cis-1,2-diphenyloxirane

: 88-17-5
2-(trifluoromethyl)benzenamine

: 1215118-01-6
C21H18F3NO

Conditions

Conditions	Yield
With 2C12H25O3S(1-)*Zn(2+); (meso)-1,1'-([2,2'-bipyridine]-6,6'-diyl)bis(2,2-dimethylpropan-1-ol) In water at 20℃; for 22h; enantioselective reaction;	100%

: 76-02-8
Trichloroacetyl chloride

: 88-17-5
2-(trifluoromethyl)benzenamine

: 349416-85-9
2,2,2-trichloro-N-(2-(trifluoromethyl)phenyl)acetamide

Conditions

Conditions	Yield
In 1,4-dioxane for 0.5h; Cooling with ice;	100%
With potassium carbonate In dichloromethane at 20℃; Inert atmosphere;	93%

: 1429217-23-1
(R)-N-(1-(3-bromophenyl)ethyl)-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxamide

: 88-17-5
2-(trifluoromethyl)benzenamine

: 1429217-51-5
(R)-3-methoxy-1-methyl-2-oxo-N-(1-(3-(2-(trifluoromethyl)phenylamino)phenyl)ethyl)-1,2-dihydropyridine-4-carboxamide

Conditions

Conditions	Yield
With tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In toluene at 110℃; Inert atmosphere;	100%

: 3282-30-2
pivaloyl chloride

: 88-17-5
2-(trifluoromethyl)benzenamine

: 125686-52-4
N-<2-(trifluromethyl)phenyl>-2,2-dimethylpropanamide

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 0 - 20℃; for 16h;	100%
With triethylamine In tetrahydrofuran at 0 - 20℃; for 12h; Inert atmosphere;
With sodium hydrogencarbonate In dichloromethane at 20℃;

: 15486-96-1
3-Bromopropionyl chloride

: 88-17-5
2-(trifluoromethyl)benzenamine

: 3945-39-9
3-bromo-propionic acid-(2-trifluoromethyl-anilide)

Conditions

Conditions	Yield
With potassium carbonate In dichloromethane at 20℃; for 0.5h; Inert atmosphere;	100%
With potassium carbonate

: 532-55-8
Benzoyl isothiocyanate

: 88-17-5
2-(trifluoromethyl)benzenamine

: 63494-72-4
N-((2-(trifluoromethyl)phenyl)carbamothioyl)benzamide

Conditions

Conditions	Yield
In acetone for 1.5h; Reflux;	99%
In benzene	86%
In tetrahydrofuran at 60 - 65℃; for 0.166667h; Microwave irradiation;	80%

: 1079-66-9
chloro-diphenylphosphine

: 88-17-5
2-(trifluoromethyl)benzenamine

: 648930-41-0
C6H4(o-CF3)NP(C6H5)2P(C6H5)2

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 20℃; for 0.5h;	99%

: 50-00-0
formaldehyd

: 88-17-5
2-(trifluoromethyl)benzenamine

: 1,3,5-tris(2-(trifluoromethyl)phenyl)-1,3,5-triazinane

Conditions

Conditions	Yield
In water for 0.0416667h; microwave irradiation;	99%
In water at 20℃; for 0.416667h; Ionic liquid; Green chemistry;	90%

: 39973-76-7
ethyl 2-benzoyl-3-ethoxyacrylate

: 88-17-5
2-(trifluoromethyl)benzenamine

: 854777-97-2
2-benzoyl-3-(2-trifluoromethylphenylamino)acrylic acid ethyl ester

Conditions

Conditions	Yield
In toluene at 150℃; for 1h; Microwave irradiation;	99%
In toluene for 18h; Heating;	82%

: 88-17-5
2-(trifluoromethyl)benzenamine

: 445-02-3
4-bromo-2-trifluoromethyl-aniline

Conditions

Conditions	Yield
With iron(III) chloride; N-Bromosuccinimide; 1-butyl-3-methylimidazolium trifluoromethanesulfonimide In toluene at 40℃; regioselective reaction;	99%
With N-Bromosuccinimide In N,N-dimethyl-formamide at 0 - 20℃; for 2h; Inert atmosphere; Schlenk technique;	93%
With 1-hexyl-3-methyl-1-imidazolium bromide; copper(ll) bromide for 1h; regioselective reaction;	92%

: 119-61-9
benzophenone

: 88-17-5
2-(trifluoromethyl)benzenamine

: N-(Diphenylmethylene)-2-(trifluoromethyl)aniline

Conditions

Conditions	Yield
With tetraethoxy orthosilicate; sulfuric acid at 160℃; for 16h;	98%

: 1121-60-4
pyridine-2-carbaldehyde

: 88-17-5
2-(trifluoromethyl)benzenamine

: 386713-04-8
N-(2-pyridylmethylidene)-2-trifluoromethylaniline

Conditions

Conditions	Yield
With 4 A molecular sieve In benzene at 80℃; for 8h;	98%
In toluene for 24h; Reflux;	94%
With toluene-4-sulfonic acid In toluene at 70℃; for 48h; Molecular sieve;	91.9%

: 500-22-1
3-pyridinecarboxaldehyde

: 88-17-5
2-(trifluoromethyl)benzenamine

: N-(3-pyridylmethylidene)-2-trifluoromethylaniline

Conditions

Conditions	Yield
With 4 A molecular sieve In benzene at 80℃; for 8h;	98%

: 50-00-0
formaldehyd

: 88-17-5
2-(trifluoromethyl)benzenamine

: 103-85-5
monophenylthiourea

: 701277-33-0
1-phenyl-5-(2-trifluoromethyl-phenyl)-[1,3,5]triazinane-2-thione

Conditions

Conditions	Yield
In water for 0.0138889h; microwave irradiation;	98%

...Expand

: 98946-18-0
tert-Butyl 2,2,2-trichloroacetimidate

: 88-17-5
2-(trifluoromethyl)benzenamine

: 864365-12-8
tert-butyl-(2-trifluoromethyl-phenyl)-amine

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In cyclohexane at 20℃;	98%

: 673-32-5
1-Phenylprop-1-yne

: 88-17-5
2-(trifluoromethyl)benzenamine

: N-cinnamyl-2-(trifluoromethyl)aniline

Conditions

Conditions	Yield
With palladium diacetate; benzoic acid In toluene at 110℃; for 5h;	98%
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; benzoic acid In toluene at 110℃; for 1h; Inert atmosphere; chemoselective reaction;	98%

: 76-05-1
trifluoroacetic acid

: 88-17-5
2-(trifluoromethyl)benzenamine

: 2368-64-1
2,2,2-trifluoro-N-(2-(trifluoromethyl)phenyl)acetamide

Conditions

Conditions	Yield
With pyridine; dmap In dichloromethane at 0 - 20℃; for 15.5h; Inert atmosphere;	98%

: 693-13-0
diisopropyl-carbodiimide

: 88-17-5
2-(trifluoromethyl)benzenamine

: 2-(trifluoromethylphenyl)-1,3-diisopropylguanidine

Conditions

Conditions	Yield
With diethylzinc In hexane; toluene at 50℃; for 2h; Schlenk technique; Inert atmosphere;	98%

: 75-87-6
chloral

: 88-17-5
2-(trifluoromethyl)benzenamine

: 444-93-9
(E)-2-(hydroxyimino)-N-(2-(trifluoromethyl)phenyl)acetamide

Conditions

Conditions	Yield
With hydroxyammonium sulfate; sodium sulfate In ethanol at 60 - 80℃; for 6h;	97%

: 2094-72-6
1-Adamantanecarbonyl chloride

: 88-17-5
2-(trifluoromethyl)benzenamine

: N-[2-(trifluoromethyl)phenyl]adamantane-1-carboxamide

Conditions

Conditions	Yield
With triethylamine In acetone at 90℃; for 3h; Inert atmosphere;	97%

: 123-54-6
acetylacetone

: 88-17-5
2-(trifluoromethyl)benzenamine

: C12H11F3N2O2

Conditions

Conditions	Yield
Stage #1: 2-(trifluoromethyl)benzenamine With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 0.5h; Stage #2: acetylacetone With sodium acetate In ethanol; water at 0 - 20℃; for 4h;	97%

: 98-09-9
benzenesulfonyl chloride

: 88-17-5
2-(trifluoromethyl)benzenamine

: 86802-68-8
N-(2-(trifluoromethyl)phenyl)benzenesulfonamide

Conditions

Conditions	Yield
With pyridine In acetonitrile at 35 - 55℃; for 6.5h; Inert atmosphere; Large scale;	96.8%
With pyridine at 85℃; for 8h;	88%
With pyridine at 146℃; for 4h;	43%

: 108-24-7
acetic anhydride

: 88-17-5
2-(trifluoromethyl)benzenamine

: 344-62-7
N-[2-(trifluoromethyl)phenyl]acetamide

Conditions

Conditions	Yield
With 2,3,4,5,7,8,9,10-octahydropyrimido[1,2-a]azepin-1-ium acetate In neat (no solvent) at 50℃; for 0.5h; Green chemistry;	96%
at 80℃; for 5h; Large scale;	95%
Stage #1: acetic anhydride; 2-(trifluoromethyl)benzenamine at 20℃; for 1h; Stage #2: With water; sodium hydrogencarbonate	92%

: 50-00-0
formaldehyd

: 1736-71-6
2-trifluoromethylphenyl thiourea

: 88-17-5
2-(trifluoromethyl)benzenamine

: 701277-32-9
1-(2-trifluoromethylphenyl)-5-(2-trifluoromethylphenyl)-2-thioxo hexahydro-1,3,5-triazine

Conditions

Conditions	Yield
In water for 0.0125h; microwave irradiation;	96%

...Expand

: 88-17-5
2-(trifluoromethyl)benzenamine

: 68672-37-7
4-amino-3-(trifluoromethyl)phenyl thiocyanate

Conditions

Conditions	Yield
With bromine In methanol; dichloromethane	96%

: 3466-32-8
4-bromoohenyl methyl sulfone

: 88-17-5
2-(trifluoromethyl)benzenamine

: N-(4-(methylsulfonyl)phenyl)-2-(trifluoromethyl)aniline

Conditions

Conditions	Yield
With sodium phenoxide; C47H70BrO4PPdSi In tetrahydrofuran at 20℃; for 1h; Schlenk technique; Inert atmosphere; Sealed tube;	96%
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; 4-phenyl-N-methylpyridinium iodide; 4,4'-di-tert-butyl-2,2'-bipyridine; zinc In dimethyl sulfoxide at 80℃; for 8h; Reagent/catalyst; Inert atmosphere;	83%