CAS No.98-16-8,3-Aminobenzotrifluoride Suppliers

Dayang Chem (Hangzhou) Co.,Ltd.

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Jiangsu Huaen Energy Co., Ltd.

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EAST CHEMSOURCES LIMITED

3-Aminotrifluorotoluene Product Name: 3-Aminotrifluorotoluene Molecular Weight: 161.13 CAS NO: 98-16-8 EC NO: 202-643-4 Molecular Formula:

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Hebei yanxi chemical co.,LTD.

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/1654.html Product Name 3-Aminobenzotrifluoride CAS No. 98-16-8

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Henan Sinotech Import&Export Corporation

Chemical Name: M-aminobenzotrifluoride Synonym: 3-Aminotrifluorotoluene; 3-Trifluoromethylaniline; M-(Trifluoromethyl)aniline CAS No.: 98-16-8 Molecular Formula: C7H6F3N CAS: 98-16-8 Molecular formula:C7H6F3N Molecular weight:161.13

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Henan Wentao Chemical Product Co., Ltd.

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Hangzhou Keyingchem Co.,Ltd

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Zibo Hangyu Biotechnology Development Co., Ltd

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HANGZHOU YUNUO CHEMICAL CO.,LTD

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Henan Tianfu Chemical Co., Ltd.

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Zibo Dorne chemical technology co. LTD

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Wuhan Fortuna Chemical Co.,Ltd

1.Product name:3-Aminotrifluorotoluene 2.CAS:98-16-8 3.MF:C7H6F3N 4.MW:161.1244 5.Appearance:White crystalline powder 6.Assay:99%MIN Appearance:white powder Package:as celient requirement Port:ANY PORT OF CHINA

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Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)

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GIHI CHEMICALS CO.,LIMITED

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Aecochem Corp.

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Synthetic route

: 98-46-4
3-trifluoromethylnitrobenzene

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With hydrogenchloride; ammonium chloride; zinc In ethanol at 15 - 20℃; for 0.166667h; Irradiation;	100%
With hydrogen; nickel In methanol at 100 - 115℃; under 18751.9 - 30003 Torr; for 6h; Large scale;	99.9%
With hydrazine hydrate In ethanol for 2.5h; Reflux;	98.4%

: 401-81-0
m-trifluoromethylphenyl iodide

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With copper(I) oxide; ammonium hydroxide; C17H14N2O3; potassium hydroxide In ethanol at 60℃; for 24h; Schlenk technique; Inert atmosphere;	96%
With ammonium hydroxide; caesium carbonate In water for 1.5h; Reflux; Green chemistry;	90%
With ammonium hydroxide; caesium carbonate In acetonitrile for 2h; Reflux; Green chemistry;	90%
With ammonium hydroxide; potassium phosphate; copper(II) ferrite at 100℃; for 12h; Sealed tube; chemoselective reaction;	60%

: 401-78-5
3-bromo-1-trifluoromethylbenzene

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With ammonium hydroxide; L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate In 1-methyl-pyrrolidin-2-one at 110℃; for 12h;	95%
With ammonium hydroxide; copper(l) iodide; potassium carbonate; 4R-4-hydroxyproline In dimethyl sulfoxide at 50℃; for 24h;	90%

: 199188-30-2
3-(trifluoromethyl)phenyl trifluoromethanesulfonate

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
Stage #1: 3-(trifluoromethyl)phenyl trifluoromethanesulfonate With bis(bis(trimethylsilyl)amido)zinc(II); tri-tert-butyl phosphine; tetrabutylammomium bromide; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 50℃; for 6h; Stage #2: With hydrogenchloride In tetrahydrofuran; diethyl ether	91%

: 1423-26-3
(meta-(trifluoromethyl)phenyl)boronic acid

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With potassium carbonate; ammonium hydroxide In methanol at 60℃; for 21h;	84%
With N-Bromosuccinimide; CYANAMID; bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 20℃; for 1h; chemoselective reaction;	71%
With N-Bromosuccinimide; N-methoxylamine hydrochloride; bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 20℃;	66%

: 98-15-7
3-chlorotrifluoromethylbenzene

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With dicyclohexyl(2',4',6'-triisopropyl-5-methoxy-3,4,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; C50H70NO4PPdS; C50H70NO4PPdS; dicyclohexyl(2',4',6'-triisopropyl-4-methoxy-3,5,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 80℃; for 24h; Inert atmosphere;	81%

: 709-58-0
1-nitro-3-(trichloromethyl)benzene

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With ammonium bifluoride; aHF In dichloromethane 1.) 68-95 degC, 90-160 psig, 2.) 68-101 degC, 90-118 psig, 3.) 103-117 degC, 190-220 psig;	75%

: 1743-96-0
4-(pentafluoroethoxy)nitrobenzene

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With palladium 10% on activated carbon; hydrogen In methanol	71%

: 13712-75-9, 165618-44-0
3-methyl-2,4-diphenyloxazolium-5-olate

: 104143-76-2
4-[5-Methylene-3-(3-trifluoromethyl-phenyl)-4,5-dihydro-3H-[1,2,3]triazol-4-yl]-morpholine

A: 34660-89-4
N-benzoyl-N-methylphenylglycine morpholide

B: 98-16-8
3-trifluoromethylaniline

C: 1-methyl-2,5-diphenyl-3-pyrrolecarbaldehyde

D: 1-methyl-2,5-diphenyl-3-<<3-(trifluoromethyl)phenylimino>methyl>pyrrole

Conditions

Conditions	Yield
In acetonitrile for 0.5h; Ambient temperature; Further byproducts given;	A n/a B n/a C 65% D 10%

...Expand

: 98-17-9
3-Trifluoromethylphenol

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
Stage #1: 3-Trifluoromethylphenol With Nonafluorobutanesulfonyl fluoride; tris(trimethylsilyl)amine; potassium hexamethylsilazane In tetrahydrofuran at 60℃; for 5h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride In water at 20℃; for 0.0833333h; pH=3 - 4;	57%
Multi-step reaction with 2 steps 1.1: 86 percent / K3PO4 / toluene; H2O / 0 - 20 °C 2.1: P(t-Bu)3; Zn[N(SiMe3)2]2; Bu4NBr / Pd(dba)2 / tetrahydrofuran / 6 h / 50 °C 2.2: 91 percent / aq. HCl / tetrahydrofuran; diethyl ether View Scheme

: 98-56-6
4-chlorobenzotrifluoride

: 62-53-3
aniline

A: 98-16-8
3-trifluoromethylaniline

B: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
With 2,3,7,8-tetrafluoro-S-(trifluoromethyl)dibenzothiophenium trifluoromethanesulfonate In N,N-dimethyl-formamide at 30℃; for 3h; Reagent/catalyst; Inert atmosphere;	A 23% B 44%

...Expand

: 3-oxo-N-(3-trifluoromethylphenyl)butanethioamide

: 593-85-1
diguanidine carbonate

A: 6-methyl-4-[3-(trifluoromethyl)phenylamino]pyrimidin-2-amine

B: 593-87-3
guanidine acetic acid

C: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
at 140℃; for 3h;	A 40% B 28% C 26%

...Expand

: 98-46-4
3-trifluoromethylnitrobenzene

A: 98-16-8
3-trifluoromethylaniline

B: 38160-76-8
N-<3-(α,α,α-Trifluoromethyl)phenyl>hydroxylamine

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); hydrogen; palladium on activated charcoal	A n/a B 38%

: 98-46-4
3-trifluoromethylnitrobenzene

A: 98-16-8
3-trifluoromethylaniline

B: 2357-47-3
4-Fluoro-3-trifluoromethylaniline

Conditions

Conditions	Yield
With bismuth; hydrogen fluoride In dichloromethane Yield given;	A n/a B 13%
With bismuth; hydrogen fluoride In dichloromethane Yields of byproduct given;	A n/a B 13%

: 314-81-8
2-[3-(trifluoromethyl)phenyl]-1H-isoindole-1,3(2H)-dione

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With water; hydrazine hydrate

: 88-16-4
1-chloro-2-(trifluoromethyl)benzene

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With ammonia; sodium amide

: 110-96-3
diisobutylamine

: 403-96-3
1,3-bis(m-α,α,α-trifluorotolyl)urea

A: 1,1-Diisobutyl-3-(3-trifluoromethyl-phenyl)-urea

B: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
In 1,2-dichloro-benzene at 119.6℃; Equilibrium constant; Thermodynamic data; various temperatures; ΔHe, ΔSe;
In 1,2-dichloro-benzene at 141.9℃; Kinetics; Thermodynamic data; Mechanism; ΔH(excit.), ΔS(excit.); other temperature;

...Expand

: 403-96-3
1,3-bis(m-α,α,α-trifluorotolyl)urea

A: 98-16-8
3-trifluoromethylaniline

B: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
at 130 - 200℃; Thermodynamic data; ΔH; heat of dissociation;

: 117855-64-8
(3-Trifluoromethyl-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride

A: 3040-44-6
1-piperidinoethanol

B: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics;

: 97731-98-1
C9H10F3NS*ClH

A: 75-18-3
dimethylsulfide

B: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With iodide; hydrogen cation In water at 25℃; Rate constant; pH dependence (pH = 0.5-3.0), μ = 1.0 with KCl;

: 55642-42-7
bis(trifluoromethyl)tellurium

: 62-53-3
aniline

A: 455-14-1
4-trifluoromethylphenylamine

B: 98-16-8
3-trifluoromethylaniline

C: 88-17-5
2-(trifluoromethyl)benzenamine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 140℃; for 60h; Title compound not separated from byproducts;	A 24 % Spectr. B 21 % Spectr. C 21 % Spectr.

...Expand

11.11.11-trifluoro-3-nitro-toluene: 11.11.11-trifluoro-3-nitro-toluene

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With hydrogenchloride; ethanol; tin(ll) chloride

: 7664-41-7
ammonia

: sodium amide

: 88-16-4
1-chloro-2-(trifluoromethyl)benzene

: 98-16-8
3-trifluoromethylaniline

...Expand

: 7664-41-7
ammonia

: sodium amide

: 98-56-6
4-chlorobenzotrifluoride

A: 455-14-1
4-trifluoromethylphenylamine

B: 98-16-8
3-trifluoromethylaniline

...Expand

: 7647-01-0
hydrogenchloride

: 588-00-1
1,2-bis((3-trifluoromethyl)phenyl)diazene

tin (II)-chloride: tin (II)-chloride

: 98-16-8
3-trifluoromethylaniline

...Expand

: 1,1,1,3,3,3-hexamethyl-2-(3-trifluoromethyl-phenyl)-disilazane

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With hydrogenchloride In diethyl ether

: 13114-87-9
N-(3-trifluoromethylphenyl)urea

: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With sulfuric acid In methanol; water at 80 - 90℃; Kinetics; Further Variations:; Temperatures;

: 13114-87-9
N-(3-trifluoromethylphenyl)urea

A: 463-77-4
carbamic Acid

B: 98-16-8
3-trifluoromethylaniline

Conditions

Conditions	Yield
With sodium hydroxide In methanol; water at 90℃; Kinetics; Further Variations:; Temperatures; pH-values;

: 111-87-5
octanol

: 403-96-3
1,3-bis(m-α,α,α-trifluorotolyl)urea

A: 98-16-8
3-trifluoromethylaniline

B: (3-trifluoromethyl-phenyl)-carbamic acid octyl ester

Conditions

Conditions	Yield
at 118.85 - 152.25℃; Kinetics; Activation energy;

...Expand

: 98-16-8
3-trifluoromethylaniline

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 370-35-4
diethyl 2-({[3-(trifluoromethyl)phenyl]amino}methylidene)propanedioate

Conditions

Conditions	Yield
at 90 - 110℃; for 1h;	100%
In ethanol at 90℃; for 18h;	100%
In toluene at 110℃; for 24h;	98%

: 98-16-8
3-trifluoromethylaniline

: 4755-77-5
Ethyl oxalyl chloride

: 17738-86-2
ethyl 2-oxo-2-((3-(trifluoromethyl)phenyl)amino)acetate

Conditions

Conditions	Yield
With triethylamine In ethyl acetate at 0 - 19℃; for 2.5h; Product distribution / selectivity;	100%
With triethylamine In dichloromethane at 0℃; for 0.166667h; Product distribution / selectivity;	99%
With triethylamine In dichloromethane for 0.166667h; Cooling;	99%

: 98-16-8
3-trifluoromethylaniline

: 598-21-0
2-Bromoacetyl bromide

: 25625-57-4
2-bromo-N-(3′-(trifluoromethyl)phenyl)acetamide

Conditions

Conditions	Yield
In dichloromethane at 10 - 20℃; for 1.58333h;	100%
Stage #1: 3-trifluoromethylaniline; 2-Bromoacetyl bromide In dichloromethane at 10 - 20℃; for 1.58333h; Stage #2: With sodium hydrogencarbonate In dichloromethane for 0.666667h;	100%
Stage #1: 3-trifluoromethylaniline; 2-Bromoacetyl bromide In dichloromethane at 10 - 20℃; for 1.58333h; Stage #2: With sodium hydrogencarbonate In dichloromethane; water for 0.833333h;	100%

: 98-16-8
3-trifluoromethylaniline

: 407-25-0
trifluoroacetic anhydride

: 2946-73-8
2,2,2-trifluoro-N-(3-(trifluoromethyl)phenyl)acetamide

Conditions

Conditions	Yield
With triethylamine In 2-methyltetrahydrofuran	100%
Stage #1: 3-trifluoromethylaniline; trifluoroacetic anhydride With pyridine In dichloromethane at 0 - 20℃; Stage #2: With sodium hydrogencarbonate In dichloromethane	98%
In N,N-dimethyl-formamide for 48h; Ambient temperature;	70%
With triethylamine In tetrahydrofuran at 0 - 20℃;	51.1%
In dichloromethane

: 98-16-8
3-trifluoromethylaniline

: 160842-62-6
3-tert-Butyl-1-methyl-1H-pyrazole-5-carbonyl chloride

: 5-tert-Butyl-2-methyl-2H-pyrazole-3-carboxylic acid (3-trifluoromethyl-phenyl)-amide

Conditions

Conditions	Yield
With pyridine In dichloromethane Ambient temperature;	100%

: 7632-57-7
diphenylmethylenecyclopropene

: 98-16-8
3-trifluoromethylaniline

: [N,N-di-(1,1-diphenyl-1-butenyl)-3-(trifluoromethyl)]aniline

Conditions

Conditions	Yield
With tin(II) trifluoromethanesulfonate In 1,2-dichloro-ethane at 85℃; for 24h;	100%

: 98-16-8
3-trifluoromethylaniline

: 100-52-7
benzaldehyde

: [bis(p-tolyl)methylene]cyclopropane

: 7-trifluoromethyl-4,4-bis-(4-methylphenyl)-2-phenyl-1,2,3,4-tetrahydrospiro-(3,1'-cyclopropyl)-quinoline

Conditions

Conditions	Yield
Stage #1: 3-trifluoromethylaniline; benzaldehyde With magnesium sulfate In acetonitrile at 20℃; for 2h; Stage #2: [bis(p-tolyl)methylene]cyclopropane; Montmorillonite KSF In acetonitrile at 20℃; for 64h; aza-Diels-Alder reaction; Further stages.;	100%

...Expand

: 98-16-8
3-trifluoromethylaniline

: [bis(p-tolyl)methylene]cyclopropane

: [N,N-di-(4,4-di-p-tolylbut-3-enyl)-3-(trifluoromethyl)]aniline

Conditions

Conditions	Yield
With tin(II) trifluoromethanesulfonate In 1,2-dichloro-ethane at 85℃; for 5h;	100%
With tin(II) trifluoromethanesulfonate; carbon dioxide; perfluorotoluene at 65℃; under 75006 Torr; for 24h;	85%

: 13529-06-1
(5-trimethylsilanyl)furan-2-carbaldehyde

: 98-16-8
3-trifluoromethylaniline

: N-(5-trimethylsilyl-2-furylmethylidene)-3-trifluoromethylaniline

Conditions

Conditions	Yield
With 4 A molecular sieve In benzene at 20℃; for 20h;	100%

: 39716-58-0
pent-4-enoyl chloride

: 98-16-8
3-trifluoromethylaniline

: 632326-60-4
pent-4-enoic acid [3-(trifluoromethyl)phenyl]amide

Conditions

Conditions	Yield
With pyridine; dmap In dichloromethane at 0 - 20℃;	100%

: 1147550-11-5
ammonium thiocyanate

: 98-16-8
3-trifluoromethylaniline

: 953428-83-6
C17H13F3N2O3S

Conditions

Conditions	Yield
Stage #1: 2,3-dihydro-1,4-benzodioxine-6-carbonyl chloride; ammonium thiocyanate In iso-propanone at 20℃; for 0.25h; Heating / reflux; Stage #2: 3-trifluoromethylaniline In iso-propanone for 0.5h; Heating / reflux;	100%

: 100959-22-6
methyl 2-bromo-4-nitrobenzoate

: 98-16-8
3-trifluoromethylaniline

: 1019854-32-0
methyl 4-nitro-2-[(3-trifluoromethylphenyl)amino]benzoate

Conditions

Conditions	Yield
With caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium diacetate In toluene at 100℃; for 4h; Hartwig-Buchwald coupling;	100%

: 75-15-0
carbon disulfide

: 98-16-8
3-trifluoromethylaniline

: 637-19-4
1,3-bis(3-(trifluoromethyl)phenyl)thiourea

Conditions

Conditions	Yield
With dmap In ethanol for 6h; Reflux;	100%
With dmap In ethanol for 18h; Reflux;

: 2675-79-8
1-bromo-3,4,5-trimethoxybenzene

: 98-16-8
3-trifluoromethylaniline

: 1203581-78-5
N-(3-trifluoromethylphenyl)-3,4,5-trimethoxyaniline

Conditions

Conditions	Yield
With di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate In water at 20℃; for 3h; Inert atmosphere; Micellar solution;	100%

: 225385-03-5
6-bromo-4-chlorothiopheno[3,2-D]pyrimidine

: 98-16-8
3-trifluoromethylaniline

: 1228102-70-2
6-bromo-N-(3-(trifluoromethyl)phenyl)thieno[3,2-d]pyrimidin-4-amine

Conditions

Conditions	Yield
In 1,2-dichloro-ethane; tert-butyl alcohol for 20h; Reflux;	100%

: 98-16-8
3-trifluoromethylaniline

: 84358-13-4
N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid

: tert-butyl 4-((3-(trifluoromethyl)phenyl)carbamoyl)piperidine-1-carboxylate

Conditions

Conditions	Yield
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 50℃; for 16h;	100%

: 98-16-8
3-trifluoromethylaniline

: 2094-72-6
1-Adamantanecarbonyl chloride

: 42600-84-0
N-[3-(trifluoromethyl)phenyl]adamantane-1-carboxamide

Conditions

Conditions	Yield
With triethylamine In acetone at 90℃; for 3h; Inert atmosphere;	100%

: 108-24-7
acetic anhydride

: 98-16-8
3-trifluoromethylaniline

: 351-36-0
N-acetyl-3-trifluoromethylbenzenamine

Conditions

Conditions	Yield
In tetrahydrofuran at 60℃; for 1h; Concentration; Solvent; Temperature;	99.7%
With melamine-N2,N4,N6-trisulfonic acid In dichloromethane at 20℃; for 0.316667h;	95%
With dmap; triethylamine In dichloromethane at 20℃; for 12h;	86%

: 98-16-8
3-trifluoromethylaniline

: 351-36-0
N-acetyl-3-trifluoromethylbenzenamine

Conditions

Conditions	Yield
With acetic anhydride In acetic acid	99%

: 98-16-8
3-trifluoromethylaniline

: 140939-06-6
5-(4-Chloro-benzoyl)-2-phenyl-2H-pyrazole-3,4-dione

: 4-(4-chloro-phenyl)-2,4-dioxo-3-(phenyl-hydrazono)-N-(3-trifluoromethyl-phenyl)-butyramide

Conditions

Conditions	Yield
In toluene Ring cleavage; acylation; Heating;	99%

: 28539-02-8
1-Hydroxymethyl-1H-benzotriazole

: 98-16-8
3-trifluoromethylaniline

: benzotriazol-1-ylmethyl-(3-trifluoromethyl-phenyl)-amine

Conditions

Conditions	Yield
In ethanol Heating;	99%

: 50-00-0
formaldehyd

: 98-16-8
3-trifluoromethylaniline

: 1,3,5-tris(3-(trifluoromethyl)phenyl)-1,3,5-triazinane

Conditions

Conditions	Yield
In water for 0.05h; microwave irradiation;	99%
In water at 20℃; for 0.333333h; Ionic liquid; Green chemistry;	92%

: 98-16-8
3-trifluoromethylaniline

: 501-65-5
diphenyl acetylene

: 451-40-1
phenyl benzyl ketone

Conditions

Conditions	Yield
Stage #1: 3-trifluoromethylaniline; diphenyl acetylene; [(dppe)Pd(H2O)2](OTf)2 In 1,4-dioxane at 80℃; for 46h; Stage #2: With silica gel In dichloromethane at 20℃; for 2h;	99%

: 98-16-8
3-trifluoromethylaniline

: 36239-09-5
ethyl chlorocarbonylacetate

: 15386-86-4
ethyl 3-oxo-3-{[3-(trifluoromethyl)phenyl]amino}propanoate

Conditions

Conditions	Yield
With triethylamine In acetone at 20℃;	99%
With triethylamine In acetone at 0 - 20℃;	99%
With triethylamine In acetone at 20℃;	99%

: 916222-26-9
(6S)-4-methoxy-6-[(2,2,2-trifluoroacetyl)amino]-5,6,7,8-tetrahydronaphthalene-1-sulfonyl chloride

: 98-16-8
3-trifluoromethylaniline

: 916222-69-0
2,2,2-trifluoro-N-[(2S)-8-methoxy-5-({[3-(trifluoromethyl)phenyl]amino}sulfonyl)-1,2,3,4-tetrahydronaphthalen-2-yl]acetamide

Conditions

Conditions	Yield
With pyridine In dichloromethane for 16h;	99%

: 37517-81-0
3-chloro-3-oxopropanoic acid methyl ester

: 98-16-8
3-trifluoromethylaniline

: 106109-76-6
methyl 3-oxo-3-(3-(trifluoromethyl)phenylamino)propanoate

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 0.0833333h;	99%
With sodium hydrogencarbonate In Isopropyl acetate at 5 - 20℃; Product distribution / selectivity; Industry scale;	91%
With sodium hydrogencarbonate In Isopropyl acetate at -10 - 10℃;	91%
With triethylamine In acetone at 0℃; for 2h;	71%
With triethylamine In dichloromethane at 0 - 20℃; for 0.166667h;

: 1005785-02-3
2-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}thio)benzoic acid

: 98-16-8
3-trifluoromethylaniline

: 200731-31-3, 148893-10-1
HATU

: 1005787-55-2
2-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}thio)-N-[3-(trifluoromethyl)phenyl]benzamide

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide	99%

...Expand

: 98-16-8
3-trifluoromethylaniline

: 343338-97-6
5-acetyl-2-(trifluoro-methyl-sulfonyloxy)-benzoic acid,methyl ester

: 1359967-83-1
5-acetyl-2-(3-(trifluoromethyl)phenylamino)benzoic acid methyl ester

Conditions

Conditions	Yield
With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 20 - 120℃; Buchwald-Hartwig reaction; Inert atmosphere;	99%

: 98-16-8
3-trifluoromethylaniline

: 22001-17-8
3-trifluoromethylphenylazide

Conditions

Conditions	Yield
Stage #1: 3-trifluoromethylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.166667h; Stage #2: With sodium azide In water at 20℃;	99%
Stage #1: 3-trifluoromethylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 2h; Stage #2: With sodium azide In water at 0 - 20℃;	89%
Stage #1: 3-trifluoromethylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 2h; Stage #2: With sodium azide In water at 0℃; for 2h;	89%