1-Adamantanecarbonyl chloride Basic information Product Name: 1-Adamantanecarbonyl chloride Synonyms: 1-ADAMANTANECARBONYL CHLORIDE;1-ADAMANTANECARBOXYLIC ACID CHLORIDE;1-ADAMANTANECARBOXYLIC ACID CHLOROANHYDRIDE;ADAMANTANE-1-CARBONYL CHLORIDE
Cas:2094-72-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:0 Metric Ton
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Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:2094-72-6
Min.Order:1
Negotiable
Type:Other
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Cas:2094-72-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiry1-Adamantanecarbonyl chloride Basic information Product Name: 1-Adamantanecarbonyl chloride Synonyms: 1-Adamantanoic acid chloride;1-Adamantoyl chloride;1-Adamantyl carbonyl chloride;Ada
Cas:2094-72-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:2094-72-6
Min.Order:1 Kilogram
FOB Price: $50.0 / 80.0
Type:Trading Company
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Cas:2094-72-6
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:2094-72-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
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Cas:2094-72-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryCAS:2094-72-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, steroids, p
Cas:2094-72-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:1 Kilogram
FOB Price: $100.0 / 200.0
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:2094-72-6
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:2094-72-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryProduct name: 1-Adamantanecarbonyl Chloride CAS No.:2094-72-6 Molecule Formula:C11H15ClO Molecule Weight:198.69 Purity: 98.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTI
Cas:2094-72-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
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Cas:2094-72-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
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Cas:2094-72-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Metric Ton
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Type:Trading Company
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Cas:2094-72-6
Min.Order:0
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Type:Lab/Research institutions
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Cas:2094-72-6
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Conditions | Yield |
---|---|
With thionyl chloride at 80℃; for 2h; | 100% |
With oxalyl dichloride; N,N-dimethyl-formamide at 25℃; for 1.5h; | 100% |
With thionyl chloride at 80℃; for 3h; | 99% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) magnesium, 1,2-dibromoethane / 1.) diethyl ether, 35 deg C 2: 90 percent / SOCl2 / 1 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: sulfuric acid / hexane / 5 h / Cooling with ice 2: thionyl chloride / benzene / 5 h / 80 °C / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: magnesium; iodine / diethyl ether / 2 h / Inert atmosphere 1.2: 3.5 h / Inert atmosphere 2.1: thionyl chloride / 1 h / 80 °C View Scheme |
adamantoyltris(trimethylsilyl)germane
A
tris(trimethylsilyl)germyl chloride
C
chloroform
D
1-Adamantanecarbonyl chloride
Conditions | Yield |
---|---|
In tetrachloromethane byproducts: Me3SiCl, hexachloroethane; Irradiation (UV/VIS); NMR tubes contg. the acylgermane/CCl4 sealed under vac., irradiated (two 100W Hg lamps, λ>360 nm) for up to 3h, with cooling to -15°C), soln. remained colourless; not isolated, detected by NMR-spect.; | A >65 B 0% C <1 D >99 |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: bromine / 6 h / 85 °C 2.1: magnesium; iodine / diethyl ether / 2 h / Inert atmosphere 2.2: 3.5 h / Inert atmosphere 3.1: thionyl chloride / 1 h / 80 °C View Scheme | |
Multi-step reaction with 3 steps 1: bromine / 85 - 110 °C 2: sulfuric acid / tetrahydrofuran / 3 h / 5 - 10 °C 3: thionyl chloride / 2 h / 80 °C View Scheme | |
Multi-step reaction with 3 steps 1: bromine / 85 - 110 °C / Green chemistry 2: sulfuric acid / tetrahydrofuran / 3 h / 5 - 10 °C / Green chemistry 3: thionyl chloride / 2 h / 80 °C / Green chemistry View Scheme |
Conditions | Yield |
---|---|
In pyridine for 3h; Ambient temperature; | 100% |
1,3-dipropyl-5,6-diaminouracil
1-Adamantanecarbonyl chloride
sodium hydrogencarbonate
1,3-dipropyl-8-(1-adamantyl)xanthine
Conditions | Yield |
---|---|
In pyridine | 100% |
7-benzyl-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-4-amine
1-Adamantanecarbonyl chloride
C25H30N4O
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In chloroform at 160℃; for 0.116667h; Product distribution / selectivity; Microwave irradiation; | 100% |
4-aminobutyrylaldehyde diethylacetal
1-Adamantanecarbonyl chloride
N-(4,4-diethoxybutyl)adamantane-1-carboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
(S)-[1,1']-binaphthalenyl-2,2'-diol
1-Adamantanecarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at -10 - 20℃; | 100% |
With dmap; triethylamine In tetrahydrofuran at -5 - 20℃; for 24h; Inert atmosphere; | 95% |
With dmap; triethylamine In tetrahydrofuran at -10 - 20℃; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With triethylamine In chloroform at 20℃; for 0.5h; | 100% |
1-amino-4-[(tert-butyloxycarbonyl)amino]butane
1-Adamantanecarbonyl chloride
N-(4-tert-butoxycarbonylamino)butyl-1-adamantanecarboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 3h; | 100% |
3-trifluoromethylaniline
1-Adamantanecarbonyl chloride
N-[3-(trifluoromethyl)phenyl]adamantane-1-carboxamide
Conditions | Yield |
---|---|
With triethylamine In acetone at 90℃; for 3h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With pyridine; dmap In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
With pyridine; dmap In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
With pyridine; dmap In dichloromethane at 0 - 20℃; Inert atmosphere; |
3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one
1-Adamantanecarbonyl chloride
Conditions | Yield |
---|---|
With pyridine In 1,2-dichloro-ethane | 99.8% |
trimethylsilylazide
1-Adamantanecarbonyl chloride
1-adamantyl isocyanate
Conditions | Yield |
---|---|
zinc(II) iodide In tetrachloromethane for 6h; Heating; | 99% |
1-Adamantanecarbonyl chloride
Bis(trimethylsilyl)ethyne
ethynyl adamant-1-yl ketone
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane at -20℃; for 1.25h; | 99% |
methyl 3-acetyl-4-hydroxybenzoate
1-Adamantanecarbonyl chloride
adamantane-1-carboxylic acid 2-acetyl-4-(methoxycarbonyl)phenyl ester
Conditions | Yield |
---|---|
With pyridine; dmap at 20℃; for 18h; | 99% |
1-Adamantanecarbonyl chloride
(3-acetyl-4-hydroxyphenyl)acetic acid methyl ester
adamantane-1-carboxylic acid 2-acetyl-4-methoxycarbonylmethylphenyl ester
Conditions | Yield |
---|---|
With pyridine; dmap at 20℃; for 18h; | 99% |
1-Adamantanecarbonyl chloride
Nα,Nα-bis[(tert-butyloxycarbonyl)methyl]-L-lysine tert-butyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; | 99% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; | 77% |
Conditions | Yield |
---|---|
With triethylamine In acetone at 90℃; for 3h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With triethylamine In acetone at 90℃; for 3h; Inert atmosphere; | 99% |
(+)-endo-Fenchylamine
1-Adamantanecarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In toluene at 0 - 20℃; for 12h; | 99% |
1-Adamantanecarbonyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane at 20℃; for 0.5h; | 98.3% |
1-Adamantanecarbonyl chloride
A
1-Adamantyl bromide
B
2-<(trichloromethyl)thio>pyridine
Conditions | Yield |
---|---|
With Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; dmap at 105℃; for 0.5h; | A 98% B n/a |
1-Adamantanecarbonyl chloride
(R)-1-benzyl-3-aminopyrrolidine
(R)-N-(1-Benzylpyrrolidin-3-yl)-1-adamantanecarboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane Acylation; | 98% |
1-Adamantanecarbonyl chloride
(3S)-1-benzyl-3-pyrrolidinamine
(S)-N-(1-benzylpyrrolidin-3-yl)-1-adamantanecarboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane Acylation; | 98% |
With triethylamine In ethyl acetate; N,N-dimethyl-formamide |
1-Adamantanecarbonyl chloride
6-aminohexanoic acid
6-[(Adamantane-1-carbonyl)-amino]-hexanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran at 0℃; for 2h; | 98% |
(1S,2R)-(+)-norphedrine
1-Adamantanecarbonyl chloride
N-((1S,2R)-1-hydroxy-1-phenylpropan-2-yl)adamantane-1-carboxamide
Conditions | Yield |
---|---|
Stage #1: (1S,2R)-(+)-norphedrine; 1-Adamantanecarbonyl chloride With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; Cooling with ice; Stage #2: With sodium hydroxide In tetrahydrofuran; methanol; water at 20℃; for 4h; Alkaline aqueous solution; | 98% |
1-Adamantanecarbonyl chloride
(S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol
Conditions | Yield |
---|---|
98% |
5-fluoro-N1-[2-(morpholin-4-yl)ethyl]-1,2-phenylenediamine
1-Adamantanecarbonyl chloride
N-(1-adamantanecarbonyl)-4-fluoro-N'-[2-(morpholin-4-yl)ethyl]-1,2-phenylenediamine
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 60℃; for 1.5h; | 98% |
1-Adamantanecarbonyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane at 20℃; for 0.5h; | 98% |
1-Adamantanecarbonyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane at 20℃; for 0.5h; | 98% |
Conditions | Yield |
---|---|
Stage #1: 3-iodoindazole With potassium tert-butylate In tetrahydrofuran at 0℃; for 1h; Stage #2: 1-Adamantanecarbonyl chloride In tetrahydrofuran at 20℃; for 4h; | 98% |
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