SICHUAN ZHONGBANG with its subsidiaries LUZHOU FUBANG& LUZHOU DAZHOU are specializing in the research, development, manufacturing and trade of fine chemicals, pesticide intermediates and pharmaceutical intermediates.
DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:768-90-1
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance: White to yellow Powder Storage:Sealed, dry
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:768-90-1
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inquiryTIANFUCHEM--768-90-1--2-Adamantanol in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relationships
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
Cas:768-90-1
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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Cas:768-90-1
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inquiry1-Bromoadamantane CAS:768-90-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:768-90-1
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inquiry1.high quality: quality is life. quality is the most important element for all goods. we have a lab doing research in wuhan china. hplc and nmr is available if needed. 2.reasonable price: we provide high quality products wi
Cas:768-90-1
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inquiryOverview of Our Factories Our Factories production lines Our Factories R&D ability Our Factories warehouse Our Factorie
Cas:768-90-1
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Air/Courier Dang
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:768-90-1
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:768-90-1
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:768-90-1
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inquiryName 1-Bromoadamantane Cas 768-90-1
Cas:768-90-1
Min.Order:1 Gram
FOB Price: $63.0
Type:Lab/Research institutions
inquiryProduct name: 1-Bromoadamantane CAS No.:768-90-1 Molecule Formula:C10H15Br Molecule Weight:215.13 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TEST
Cas:768-90-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryConditions | Yield |
---|---|
With iron(III)-acetylacetonate; carbon tetrabromide at 120℃; for 2h; Sealed tube; Inert atmosphere; | 99% |
With hydrogen bromide at 130℃; for 2h; | 90% |
With boron tribromide for 0.5h; | 86% |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; carbon tetrabromide Reagent/catalyst; Sealed tube; Inert atmosphere; | A 99% B 23% |
With bromine; iron at 0 - 50℃; for 3h; | A n/a B 93% |
With iodine(I) bromide In tetrachloromethane for 3h; Heating; | A 75 % Chromat. B 25 % Chromat. |
With iodine(I) bromide In tetrachloromethane for 3h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With oxygen; 1,2-dibromomethane for 10h; Reflux; | 99% |
With iron(III)-acetylacetonate; carbon tetrabromide at 120℃; for 2h; Sealed tube; Inert atmosphere; | 99% |
With dibromo sulfoxide In toluene for 22h; | 96% |
Conditions | Yield |
---|---|
With bromine; Nitrogen dioxide In trifluoroacetic acid at 20℃; for 0.5h; | 98% |
With water; bromine for 0.166667h; | 93% |
With bromine at 85 - 110℃; Temperature; | 93% |
1-Adamantanecarbonyl chloride
A
1-Adamantyl bromide
B
2-<(trichloromethyl)thio>pyridine
Conditions | Yield |
---|---|
With Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; dmap at 105℃; for 0.5h; | A 98% B n/a |
1-Adamantyl bromide
Conditions | Yield |
---|---|
With bromine In tetrachloromethane at 20℃; for 12h; | 97% |
1-(Dibromoamino)adamantane
1-Adamantyl bromide
Conditions | Yield |
---|---|
In acetone at 250 - 260℃; | 94% |
In acetone at 250 - 260℃; also at 250 deg C, 6 Torr, without solvent; | 94% |
Conditions | Yield |
---|---|
With hydrogen bromide at 105℃; for 0.5h; | 92% |
With boron tribromide In hexane at 0℃; for 0.0833333h; | 90% |
4-(1-adamantyl)benzene-1,3-diol
A
1-Adamantyl bromide
B
2,4,6-tribromoresorcinol
C
2,6-Dibromo-4-(1-adamantyl)resorcinol
Conditions | Yield |
---|---|
With bromine In methanol; acetic acid for 1h; Ambient temperature; | A n/a B n/a C 91.5% |
Bromotrichloromethane
adamantane
acetonitrile
A
1-Adamantyl bromide
B
chloroform
C
N-(1-adamantyl)acetamide
Conditions | Yield |
---|---|
With water; molybdenum hexacarbonyl at 140℃; for 2h; | A n/a B n/a C 90% |
Conditions | Yield |
---|---|
With Ag(Phen)2OTf; dibromoisocyanuric acid In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere; Schlenk technique; | 89% |
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; caesium carbonate; Diethyl 2-bromomalonate In ethyl acetate at 20℃; for 4h; Solvent; Inert atmosphere; Irradiation; | 70% |
With Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; dmap 2.) reflux; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: (COBr)2 2: Fe / 1 h / Ambient temperature View Scheme |
1-nitroxyadamantane
1-Adamantyl bromide
Conditions | Yield |
---|---|
With sulfuric acid; potassium bromide for 1h; | 89% |
adamantane
acetonitrile
A
1-Adamantyl bromide
B
Bromoform
C
1-adamantanecarbonitrile
Conditions | Yield |
---|---|
With carbon tetrabromide; molybdenum hexacarbonyl at 140 - 160℃; for 6h; Reactivity; Mechanism; Reagent/catalyst; | A 15% B n/a C 85% |
adamantane
benzoyl chloride
A
1-Adamantyl bromide
B
2-adamantyl bromide
C
benzaldehyde
Conditions | Yield |
---|---|
With aluminum tri-bromide In various solvent(s) at 20℃; for 2h; | A 70% B 3% C 82% |
With aluminum tri-bromide In various solvent(s) at 20℃; for 2h; | A 70% B 3% C 82% |
1-(1-adamantyl)-3,4-dimethylbenzene
A
1-Adamantyl bromide
B
1,3-dibromoadamantane
C
1,2,3,4-tetrabromo-5,6-dimethylbenzene
Conditions | Yield |
---|---|
With bromine; iron for 3.5h; Product distribution; Ambient temperature; | A n/a B n/a C 82% |
1-chloroadamantane
A
1-Adamantyl bromide
B
2-adamantyl bromide
C
adamantane
D
1,3-dibromoadamantane
Conditions | Yield |
---|---|
With hydrogen bromide; ferric(III) bromide In dichloromethane at 25℃; for 0.3h; | A 78% B 3% C 9% D 9 % Chromat. |
With hydrogen bromide; ferric(III) bromide In dichloromethane at 25℃; for 0.3h; | A 78% B 3% C 9% D 3 % Chromat. |
adamantane
A
1-Adamantyl bromide
B
2-Adamantanone
C
1-chloroadamantane
D
2-adamantyl bromide
E
1-adamanthanol
F
1-adamantanol
Conditions | Yield |
---|---|
With Bromotrichloromethane; 3,3-dimethyldioxirane In acetone at 20℃; Product distribution; Mechanism; | A 12.2% B 1.8% C 0.7% D 2.3% E 77.2% F 1.1% |
With Bromotrichloromethane; 3,3-dimethyldioxirane In acetone for 1h; Mechanism; Product distribution; Ambient temperature; concentration depending investigated; |
adamantane
A
1-Adamantyl bromide
B
1-chloroadamantane
C
2-adamantyl bromide
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; Bromotrichloromethane; iron(III) chloride In pyridine; acetic acid at 60℃; for 18h; | A 69.2% B 4.1% C 26.7% |
With tert.-butylhydroperoxide; Bromotrichloromethane; iron(III) chloride In pyridine; acetic acid at 60℃; for 18h; Product distribution; Mechanism; various conditions; | A 69.2% B 4.1% C 26.7% |
(1s,3s)-adamantan-1-yl(phenyl)sulfide
1-Adamantyl bromide
Conditions | Yield |
---|---|
With bromine In dichloromethane at 20℃; for 1h; | 68% |
1-(Dibromoamino)adamantane
A
1-Adamantyl bromide
B
1,3-dibromoadamantane
Conditions | Yield |
---|---|
at 95 - 250℃; under 6 Torr; for 1h; | A 65% B n/a |
Conditions | Yield |
---|---|
Stage #1: adamantane With [2,2]bipyridinyl; N-Bromosuccinimide; manganese(II) acetate for 0.0833333h; Inert atmosphere; Stage #2: With trimethylsilylazide at 60℃; for 0.5h; Inert atmosphere; Sealed tube; regioselective reaction; | A 62% B 15% |
Stage #1: adamantane With [2,2]bipyridinyl; N-Bromosuccinimide; manganese(II) acetate for 0.0833333h; Inert atmosphere; Stage #2: With trimethylsilylazide at 60℃; for 18h; Inert atmosphere; Sealed tube; regioselective reaction; | A 16% B 62% |
C10H15Ge(CH3)3
A
1-Adamantyl bromide
B
1-adamantyldimethylbromogermane
Conditions | Yield |
---|---|
With bromine In tetrachloromethane soln. of Br2 added to soln. of 1-AdGeMe3; boiled (18 h, 78°C); solvent removed; recrystd. (hexane); elem.anal.; | A 54.7% B 28.7% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; bromine In water; 1,2-dichloro-ethane for 4h; | A 48.7% B 51.3% |
With Li2MnO3; bromine; oxygen at 100℃; under 760.051 Torr; for 24h; Photolysis; | A 42% B 5% |
With hydrogenchloride; oxygen; potassium bromide; sodium nitrite In chloroform; water at 20 - 30℃; under 760.051 Torr; for 24h; Sealed tube; Irradiation; | A 20% B 17% |
Conditions | Yield |
---|---|
With [(hydrotris(3,5-diphenyl-pyrazol-1-yl)borate)FeII(benzilate)]; tetrabutylammomium bromide; oxygen; pyridinium perchlorate In acetonitrile at 20℃; | A 7% B 48% |
With ruthenium hydroxide trichloride; carbon tetrabromide; water at 160℃; for 9h; Inert atmosphere; regioselective reaction; | A 30% B 30% |
adamantane
A
1-Adamantyl bromide
B
1-chloroadamantane
C
2-adamantyl bromide
D
1-adamanthanol
E
1-adamantanol
F
2-chloroadamantane
Conditions | Yield |
---|---|
With Bromotrichloromethane; 3,3-dimethyldioxirane In acetone at 20℃; for 3.5h; Rate constant; Product distribution; Kinetics; | A 42.3% B 9.2% C 10.5% D 33% E 2% F 2.5% |
Conditions | Yield |
---|---|
In dichloromethane at 250 - 260℃; 15-30percent SE-30 on Chromosorb W; | A 30% B n/a |
tetrabutylammomium bromide
3-chloro-benzenecarboperoxoic acid
A
1-Adamantyl bromide
B
2-adamantyl bromide
C
n-butyl 3-chlorobenzoate
Conditions | Yield |
---|---|
With adamantane In acetonitrile at 20℃; for 1h; Yields of byproduct given; | A n/a B n/a C 24% |
tetramethylammonium bromide
3-chloro-benzenecarboperoxoic acid
A
1-Adamantyl bromide
B
2-adamantyl bromide
C
methyl 3-chlorobenzoate
Conditions | Yield |
---|---|
With adamantane In acetonitrile at 20℃; for 1h; Yields of byproduct given; | A n/a B n/a C 19% |
Acetyl bromide
1-chloroadamantane
A
1-Adamantyl bromide
B
acetyl chloride
Conditions | Yield |
---|---|
With iron(III) chloride at 25℃; for 168h; Equilibrium constant; Thermodynamic data; ΔG; | |
With iron(III) chloride In chloroform at 25℃; for 168h; Equilibrium constant; Thermodynamic data; ΔG; |
Conditions | Yield |
---|---|
With molybdenum hexacarbonyl Sealed tube; regioselective reaction; | 100% |
With potassium carbonate; palladium on activated charcoal at 120℃; for 12h; | 91% |
With palladium 10% on activated carbon; potassium carbonate for 20h; Heating; | 82.65% |
Conditions | Yield |
---|---|
With triethylsilane; dilauryl peroxide; 1-dodecylthiol at 70℃; for 1h; | 100% |
With triethylsilane; dilauryl peroxide; 1-dodecylthiol In cyclohexane at 80℃; for 1h; | 100% |
With sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); cPS-SnBu2Cl In 1,2-dimethoxyethane at 80℃; for 0.5h; | 100% |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate Heating; | 100% |
With bromine for 0.05h; | 90% |
1-Adamantyl bromide
(2S,4R)-1-(tert-butoxycarbonyl)-4-((tert-butyldimethylsilyl)oxy)pyrrolidine-2-carboxylic acid
1-adamantyl (2S,4R)-1-(tert-butoxycarbonyl)-4-(tert-butyldimethylsilyloxy)pyrrolidine-2-carboxylate
Conditions | Yield |
---|---|
With silver(l) oxide In diethyl ether at 20℃; for 30h; | 100% |
Conditions | Yield |
---|---|
With triethylamine | 100% |
1-Adamantyl bromide
Conditions | Yield |
---|---|
In acetic acid Heating; | 100% |
Conditions | Yield |
---|---|
With molybdenum hexacarbonyl at 100℃; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; Time; Sealed tube; regioselective reaction; | 99% |
With potassium carbonate; palladium on activated charcoal at 120℃; for 12h; | 97% |
With iron pentacarbonyl; Bromotrichloromethane at 80℃; for 5h; Friedel-Crafts Alkylation; | 95% |
Conditions | Yield |
---|---|
In dibutyl ether at 85℃; for 1h; | 99% |
In dibutyl ether at 105℃; for 4.5h; | 80% |
In dibutyl ether at 70 - 90℃; Rate constant; Thermodynamic data; ΔE; |
1-Adamantyl bromide
ortho-cresol
4-((3r,5r,7r)-adamantan-1-yl)-2-methylphenol
Conditions | Yield |
---|---|
With molybdenum hexacarbonyl at 120℃; for 0.5h; Sealed tube; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In acetic anhydride; acetic acid; N,N-dimethyl-formamide at 0 - 10℃; for 4h; Substitution; Electrochemical reaction; | 98% |
With water; bromine for 1h; | 95.5% |
With hydrogenchloride In N,N-dimethyl-formamide at 105℃; for 0.5h; | 95% |
1-Adamantyl bromide
4-methylquinoline trifluoroacetate
4-methyl-2-(tricyclo[3.3.1.13,7]dec-1-yl)quinolone
Conditions | Yield |
---|---|
With {Au(dppm)}2Cl2 In methanol Inert atmosphere; UV-irradiation; | 98% |
With 2,2'-azobis(isobutyronitrile); 1,1,2,2-tetraphenyldisilane In ethanol for 24h; Product distribution; Heating; other reagents; | 93% |
With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane In benzene for 14h; Heating; | 90% |
With tetrakis(trimethylsilyl)silane In dichloromethane at 30℃; for 14h; Irradiation; | 83% |
Conditions | Yield |
---|---|
With hydrogen iodide; cetyltributylphosphonium bromide at 105℃; for 1.75h; | 98% |
With hydrogen iodide at 105℃; for 0.5h; | 90% |
Stage #1: 1-Adamantyl bromide With zinc In tetrahydrofuran for 2h; Reflux; Stage #2: With iodine In tetrahydrofuran at 20℃; | 79% |
With potassium iodide at 19.9℃; under 45003600 Torr; under shear deformation (360 deg); | 19% |
1-Adamantyl bromide
4,4'-bipyridine
1-Adamantan-1-yl-[4,4']bipyridinyl-1-ium; bromide
Conditions | Yield |
---|---|
With water at 180℃; for 4h; | 98% |
styrene
1-Adamantyl bromide
1-[(1E)-2-phenylethenyl]-tricyclo[3.3.1.13,7]decane
Conditions | Yield |
---|---|
Stage #1: 1-Adamantyl bromide With palladium diacetate; heptakis(6-amino-6-deoxy)-β-cyclodextrin In water; N,N-dimethyl-formamide for 0.5h; Stage #2: styrene With potassium carbonate In water; N,N-dimethyl-formamide at 80℃; for 8h; | 98% |
With (trimethylsilyl)methylmagnesium chloride; Co(1,3-bis(diphenylphosphino)hexane)Cl2 In diethyl ether at 20℃; for 8h; Heck reaction; | 87% |
With Co(1,3-bis(diphenylphosphino)hexane)Cl2; (trimethylsilyl)methylmagnesium chloride In diethyl ether at 20℃; for 8h; Heck reaction; | 87% |
With potassium carbonate; palladium on activated charcoal In N,N-dimethyl-formamide at 100 - 120℃; | 41% |
Conditions | Yield |
---|---|
With potassium carbonate; palladium on activated charcoal at 120℃; for 12h; | 98% |
With zinc(II) chloride Substitution; Heating; | 92% |
With zinc(II) chloride for 10h; Heating; | 90% |
With molybdenum hexacarbonyl at 120℃; for 2h; Sealed tube; regioselective reaction; | 72% |
Conditions | Yield |
---|---|
With triethylamine at 180℃; for 23h; | 98% |
With triethylamine | 93% |
With triethylamine In dichloromethane at 180℃; | 91% |
1-Adamantyl bromide
pentafluorophenyl potassium carboxylate
1-(perfluorophenyl)adamantane
Conditions | Yield |
---|---|
With copper(l) iodide In diethylene glycol dimethyl ether at 130℃; for 24h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With water at 180℃; for 6h; | 97% |
at 180℃; for 6h; | 97% |
at 180℃; for 24h; | 12% |
Conditions | Yield |
---|---|
With sodium nitrate; (HF)x*C5H5N In dichloromethane for 5h; Ambient temperature; | 97% |
With nitronium tetrafluoborate; pyridine polyhydrogen fluoride In dichloromethane for 3h; Ambient temperature; | 96% |
With n-Bu4PF at 150℃; for 5h; | 91% |
1-Adamantyl bromide
2-[(1-benzyloxycarbonylamino-ethyl)-hydroxy-phosphinoylmethyl]-4-phenyl-butyric acid ethyl ester
2-[(adamantan-1-yloxy)-(1-benzyloxycarbonylamino-ethyl)-phosphinoylmethyl]-4-phenyl-butyric acid ethyl ester
Conditions | Yield |
---|---|
With silver(l) oxide In chloroform for 0.5h; Heating; | 97% |
1-Adamantyl bromide
2-[(1-benzyloxycarbonylamino-ethyl)-hydroxy-phosphinoylmethyl]-5-phenyl-pentanoic acid ethyl ester
2-[(adamantan-1-yloxy)-(1-benzyloxycarbonylamino-ethyl)-phosphinoylmethyl]-5-phenyl-pentanoic acid ethyl ester
Conditions | Yield |
---|---|
With silver(l) oxide In chloroform for 0.5h; Heating; | 97% |
1-Adamantyl bromide
silver(I)-di(4-methylbenzolsulfonyl)amide
Conditions | Yield |
---|---|
In benzene at 20℃; for 96h; Substitution; | 97% |
1-Adamantyl bromide
trimethyleneglycol
3-(adamantane-1-yloxy)propan-1-ol
Conditions | Yield |
---|---|
With triethylamine Heating; | 97% |
1-Adamantyl bromide
(R,S)-2-isopropyl-3-((1-(N-(9-fluorenylmethoxycarbonyl)amino)methyl)phosphinic acid) propanoic acid allyl ester
Conditions | Yield |
---|---|
With silver(l) oxide In chloroform for 2h; Heating; | 97% |
With silver(l) oxide In chloroform for 2.83333h; Heating / reflux; | 97% |
1-Adamantyl bromide
trimethylstannane
A
adamantane
B
n-butyltrimethyltin
Conditions | Yield |
---|---|
With n-butyllithium In hexane 1-bromoadamantane (1 equiv.) and TMTH (1 equiv.) in hexane cooled to 0°C under Ar, n-BuLi (1 equiv., 2.40 M in hexane) added, stirred for 15 min, quenched with water; analyzed by GC; | A 97% B 95% |
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