CAS No.108-88-3,Toluene Suppliers,MSDS download

: 100-44-7
benzyl chloride

: 108-88-3
toluene

Conditions

Conditions	Yield
With hydrogen; Lindlar's catalyst In benzene under 760 Torr; for 0.5h; Ambient temperature;	100%
With sulfuric acid; aluminium; nickel dichloride In water at 25℃; Product distribution;	98%
With sodium tetrahydroborate; cetyltributylphosphonium bromide In water; toluene at 40℃; for 0h; Product distribution;	96%

: 100-51-6
benzyl alcohol

: 108-88-3
toluene

Conditions

Conditions	Yield
With hydrogenchloride; aluminium; nickel dichloride In ethanol at 25℃; Product distribution;	100%
With palladium dichloride In methanol at 40℃; for 24h; Green chemistry; chemoselective reaction;	99%
With palladium on activated charcoal; hydrogen In tetrahydrofuran at 25℃; under 760.051 Torr; for 1.5h;	99%

: 615-37-2
ortho-methylphenyl iodide

: 108-88-3
toluene

Conditions

Conditions	Yield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 12h; Inert atmosphere;	100%
With lithium aluminium tetrahydride In 1,2-dimethoxyethane at 35℃; for 5h; ultrasonic acceleration of reduction;	95%
With 2,2'-azobis(isobutyronitrile); poly(n-hexylsilane) In benzene-d6 at 82 - 85℃; for 3h; sealed;	99 % Spectr.

: 106-43-4
para-chlorotoluene

: 108-88-3
toluene

Conditions

Conditions	Yield
With water; sodium iodide; nickel dichloride; zinc; sonication In N,N,N,N,N,N-hexamethylphosphoric triamide at 60℃; for 3h;	100%
With water; sodium iodide; nickel dichloride; zinc; sonication In N,N,N,N,N,N-hexamethylphosphoric triamide at 60℃; for 3h; Product distribution;	100%
With palladium on ceria; sodium hydroxide In isopropyl alcohol at 40℃; for 24h; Temperature; Solvent; Irradiation; Inert atmosphere; Sealed tube;	97%

: 106-38-7
para-bromotoluene

: 108-88-3
toluene

Conditions

Conditions	Yield
With potassium hydroxide; isopropyl alcohol; polymer supported Na2PdCl4 at 82℃; for 0.666667h; Rate constant; further catalysts; influence of the nature of catalyst on the rate of dehalogenation;	100%
With tetrakis(triphenylphosphine) palladium(0); formaldehyd; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h;	99%
With lithium aluminium tetrahydride In 1,2-dimethoxyethane at 35℃; for 5h; ultrasonic acceleration of reduction;	97%

: 100-39-0
benzyl bromide

: 108-88-3
toluene

Conditions

Conditions	Yield
With sodium tetrahydroborate; cetyltributylphosphonium bromide In water; toluene at 18℃; for 0h; Product distribution;	100%
With ammonium chloride; zinc In tetrahydrofuran; water at 20℃; for 4h;	97%
With sodium tetrahydroborate In tetrahydrofuran for 0.0833333h; Ambient temperature;	90%

: 77924-17-5
1-Phenyl-5-p-tolyloxy-1H-tetrazole

A: 5097-82-5
1-phenyl-5-hydroxytetrazole

B: 108-88-3
toluene

Conditions

Conditions	Yield
With hydrazine hydrate; palladium on activated charcoal In ethanol; water; benzene for 3.5h; Ambient temperature;	A n/a B 100%
With hydrazine hydrate; palladium on activated charcoal In ethanol; benzene Mechanism; Ambient temperature;	A n/a B 100%
With sodium hypophosphite; palladium on activated charcoal In ethanol; benzene at 80℃; Relative steady-state rates of cleavage, relative extrapolated interceps;

: 108-86-1
bromobenzene

: (3-dimethylaminopropyl)dimethylgallium

: 108-88-3
toluene

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine)palladium dichloride In benzene at 80℃; for 7h;	100%

: 1122-91-4
4-bromo-benzaldehyde

: 108-88-3
toluene

Conditions

Conditions	Yield
With hydrogen; palladium on activated charcoal In water; isopropyl alcohol at 20℃; under 5171.62 Torr; for 1h;	100%

: cis-{(PhCH2)2Co(III)(2,2'-bipyridine)2}ClO4

: 108-88-3
toluene

Conditions

Conditions	Yield
With perchloric acid In acetonitrile Kinetics;	100%

: 60528-58-7
(η6-toluene)bis(η1-pentafluorophenyl)cobalt(II)

A: 434-90-2
decafluorobiphenyl

B: 7440-48-4
cobalt

C: 108-88-3
toluene

Conditions

Conditions	Yield
In neat (no solvent, solid phase) pyrolysis at 150°C;	A 93% B n/a C 100%

...Expand

: 6345-56-8
1-methyl-7-oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid anhydride

: 108-88-3
toluene

Conditions

Conditions	Yield
With zeolite Y with a silica-alumina at 250℃; for 5h; Temperature; Inert atmosphere;	100%

: 946-80-5
(benzyloxy)benzene

A: 108-88-3
toluene

B: 108-93-0
cyclohexanol

C: 108-95-2
phenol

Conditions

Conditions	Yield
With Ni0.85Rh0.15; hydrogen In water at 95℃; under 760.051 Torr; for 16h; Reagent/catalyst;	A 100% B 5% C 79%
With isopropyl alcohol at 150℃; under 7500.75 Torr; for 48h; Inert atmosphere; Autoclave;	A 100% B 12.2% C 87.5%
With isopropyl alcohol at 150℃; under 7500.75 Torr; for 3h; Catalytic behavior; Temperature; Inert atmosphere; Autoclave;	A 100% B 73.1% C 22.4%
With Ru0.6Ni0.4; hydrogen In water at 95℃; under 760.051 Torr; for 16h; Reagent/catalyst;	A 98% B 61% C 6%
With hydrogen In n-heptane at 140℃; under 750.075 Torr; for 6h; Catalytic behavior;	A 34 %Chromat. B 12 %Chromat. C 22 %Chromat.

...Expand

: 140-11-4
Benzyl acetate

A: 64-19-7
acetic acid

B: 108-88-3
toluene

Conditions

Conditions	Yield
With hydrogen In n-heptane at 160℃; under 750.075 Torr; for 6h; Catalytic behavior;	A 96 %Chromat. B 100%

: 100-52-7
benzaldehyde

: 108-88-3
toluene

Conditions

Conditions	Yield
With hydrogen In water; ethyl acetate at 50℃; under 15001.5 Torr; for 5h;	99%
With hydrogen In water at 25℃; for 1h;	99%
With palladium on activated charcoal; hydrogen In methanol at 25℃; under 760.051 Torr; for 0.833333h;	99%

: 946-80-5
(benzyloxy)benzene

A: 108-88-3
toluene

B: 108-95-2
phenol

Conditions

Conditions	Yield
With Ni0.85Ru0.15; hydrogen In water at 95℃; under 760.051 Torr; for 16h; Reagent/catalyst;	A 99% B 45%
With 0.5%Pd/TiO2; isopropyl alcohol In water at 24.84℃; for 2h; Inert atmosphere; Sealed tube; Irradiation;	A 99% B 99%
With formic acid In water at 120℃; Green chemistry;	A 98% B 96%

: 100-39-0
benzyl bromide

A: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

B: 108-88-3
toluene

Conditions

Conditions	Yield
With copper nickel; pyrographite In 1,2-dimethoxyethane at 85℃; for 20h;	A 99% B 1%
With titanium(III) citrate; Tris buffer; tetra(n-butyl)ammonium hydroxide; vitamin B-12 In ethanol for 1h; pH=8;	A 98% B 1%
With potassium phosphate; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; Irradiation;	A 85% B 6%

: 132636-69-2
3-(4-Chloro-2-methyl-phenoxy)-benzo[d]isothiazole 1,1-dioxide

A: 108-88-3
toluene

B: 81-07-2
saccharin

Conditions

Conditions	Yield
With sodium hypophosphite; palladium on activated charcoal In water; benzene for 3h; Heating;	A 99% B n/a

: 6630-18-8
4-methoxyphenyl benzyl ether

A: 150-76-5
4-methoxy-phenol

B: 108-88-3
toluene

Conditions

Conditions	Yield
With formic acid In water at 120℃; Green chemistry;	A 97% B 99%
With 9,10-dihydroanthracene at 224.84℃; Kinetics; Product distribution;
With hydrogen In hexane at 260℃; under 5250.53 Torr; for 10h; Autoclave;	A 93.6 %Chromat. B 82.9 %Chromat.
With isopropyl alcohol at 260℃; under 15001.5 Torr; for 4h; Autoclave; Inert atmosphere; Green chemistry;	A 85 %Chromat. B 88 %Chromat.

: 78709-76-9
{bis(triphenylphosphine)nitrogen}{HW(CO)5}

: 100-39-0
benzyl bromide

A: 15131-04-1
bromopentacarbonyl tungstate(0)(1-)

B: 108-88-3
toluene

Conditions

Conditions	Yield
In tetrahydrofuran Kinetics; 26.0°C, 20-fold excess of alkyl halide; second-order rate const. is given; anal. of the reaction mixt. by gas chromy.;	A n/a B 99%

...Expand

: 26138-28-3
phenylytterbium iodide

A: ytterbium(II) iodide

B: 108-88-3
toluene

Conditions

Conditions	Yield
With methyl iodide; bis(triphenylphosphine)nickel(II) chloride In tetrahydrofuran addn. of Ni-catalyst and alkyl halide to soln. of PhYbI (prepd. in situ from Yb metal and PhI in THF), agitation (25°C); GLC;	A n/a B 99%
With methyl iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran addn. of Ni-catalyst and alkyl halide to soln. of PhYbI (prepd. in situ from Yb metal and PhI in THF), agitation (25°C); GLC;	A n/a B 97%

: 538-86-3
benzyl methyl ether

: 108-88-3
toluene

Conditions

Conditions	Yield
With palladium dichloride In methanol at 40℃; for 12h; Inert atmosphere; Green chemistry; chemoselective reaction;	99%
With methanol; toluene-4-sulfonic acid at 25℃; for 7.5h; Reagent/catalyst; Inert atmosphere; Sealed tube; UV-irradiation;	95%
With samarium diiodide; water In tetrahydrofuran; decane at 20℃;
With diisobutylaluminium hydride; sodium t-butanolate; bis(1,5-cyclooctadiene)nickel(0); 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In tetrahydrofuran at 80℃; for 16h; Product distribution / selectivity; Inert atmosphere;	82 %Chromat.

: 946-80-5
(benzyloxy)benzene

A: 82166-21-0
methyl cyclohexane

B: 108-88-3
toluene

C: 108-93-0
cyclohexanol

Conditions

Conditions	Yield
With hydrogen In isopropyl alcohol at 120℃; for 2h;	A 28% B 72% C 99%
With Rh0.6Ni0.4; hydrogen In water at 95℃; under 760.051 Torr; for 16h; Reagent/catalyst;	A 35% B 63% C 95%
With 10% Pd/C; hydrogen In hexane at 160℃; under 30003 Torr; for 2h; Autoclave;
With isopropyl alcohol at 170℃; for 15h; Sealed tube;	A 0.68 mmol B 0.28 mmol C 0.94 mmol

...Expand

: 106-38-7
para-bromotoluene

: 67-63-0
isopropyl alcohol

: 108-88-3
toluene

Conditions

Conditions	Yield
With sodium hydroxide at 24.84℃; under 760.051 Torr; for 6h; Inert atmosphere; UV-irradiation; Sealed tube;	99%

: 95-49-8
2-methylchlorobenzene

: 67-63-0
isopropyl alcohol

: 108-88-3
toluene

Conditions

Conditions	Yield
With sodium hydroxide at 24.84℃; under 760.051 Torr; for 6h; Inert atmosphere; UV-irradiation; Sealed tube;	99%

: 613-62-7
2-benzyloxynaphthalene

A: 108-88-3
toluene

B: 135-19-3
β-naphthol

Conditions

Conditions	Yield
With 0.5%Pd/TiO2; isopropyl alcohol In water at 24.84℃; for 2h; Inert atmosphere; Sealed tube; Irradiation;	A 99% B 97%

: 588-67-0
benzyl 1-butyl ether

A: 108-88-3
toluene

B: 71-36-3
butan-1-ol

Conditions

Conditions	Yield
With 0.5%Pd/TiO2; isopropyl alcohol In water at 24.84℃; for 2h; Inert atmosphere; Sealed tube; Irradiation;	A 99% B 99%

: 52805-36-4
4-benzyloxybenzonitrile

A: 767-00-0
4-cyanophenol

B: 108-88-3
toluene

Conditions

Conditions	Yield
With 0.5%Pd/TiO2; isopropyl alcohol In water at 24.84℃; for 2h; Inert atmosphere; Sealed tube; Irradiation;	A 99% B 99%

: 103-16-2
4-Benzyloxyphenol

A: 556-48-9
1,4-Cyclohexanediol

B: 108-88-3
toluene

Conditions

Conditions	Yield
With hydrogen In n-heptane at 140℃; under 750.075 Torr; for 6h; Catalytic behavior;	A 99% B 99%

: 583-59-5
2-Methylcyclohexanol

A: 95-48-7
ortho-cresol

B: 108-88-3
toluene

Conditions

Conditions	Yield
platinum; potassium oxide at 360℃;	A 98% B 2%
platinum; potassium oxide at 360℃; Product distribution; other content of catalyst;	A 98% B 2%

: 38136-29-7
4-methylvaleroyl chloride

: 108-88-3
toluene

: 21847-98-3
4-methyl-1-(4'-methylphenyl)pentan-1-one

Conditions

Conditions	Yield
Friedel Crafts Acylation;	100%
With aluminium trichloride at 75 - 80℃; for 1h;	35%
With aluminium trichloride
Friedel-Crafts reaction;

: 108-88-3
toluene

: 447-31-4
Desyl chloride

: 50353-99-6
1,2-diphenyl-2-p-tolylethanone

Conditions

Conditions	Yield
With gallium(III) trichloride at 20℃; for 24h;	100%
With aluminium trichloride at 20℃; for 24h;	68%
With aluminium trichloride Behandeln bei Siedetemperatur;

: 108-88-3
toluene

: 100-39-0
benzyl bromide

Conditions

Conditions	Yield
With bromine In tetrachloromethane for 1.5h; Ambient temperature;	100%
With manganese(IV) oxide; bromine In dichloromethane at 0℃; for 1h; Product distribution; Further Variations:; Solvents; Temperatures; reaction time;	100%
With bromine; sodium t-butanolate In cyclohexane Heating;	100%

: 108-88-3
toluene

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With laccase from Coriolus versicolor MTCC-138; 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt In 1,4-dioxane for 0.5h; pH=4.5; Green chemistry; Enzymatic reaction;	100%
With nickel-doped graphene carbon nitride nanoparticles; air In ethanol at 25℃; for 8h; Reagent/catalyst; Solvent; Irradiation; Green chemistry;	98%
With water at 20℃; for 3h; Reagent/catalyst;	98%

: 108-88-3
toluene

: 82166-21-0
methyl cyclohexane

Conditions

Conditions	Yield
With hydrogen; [(norbornadiene)rhodium(I)chloride]2; phosphinated polydiacetylene In n-heptane at 30℃; under 60800 Torr; for 1.5h;	100%
With hydrogen; Ni-Tc on γ-Al2O3 at 175 - 250℃; under 760 Torr; Product distribution; dependence of catalytic activity on the reduction temperature; enhanced activity of bimetallic catalysts;	100%
With hydrogen; Rh on carbon In methanol at 20℃; under 760.051 Torr; for 0.5h;	100%

: 108-88-3
toluene

: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

Conditions

Conditions	Yield
With methyl cyanoformate; sodium decatungstate In acetonitrile at 8℃; for 90h; Irradiation;	100%
With di-tert-butyl peroxide; sodium acetate at 120℃; for 10h; Schlenk technique; Green chemistry;	94%
With di-tert-butyl peroxide; sodium acetate at 120℃; for 10h;	94%

: 112-85-6
n-docosanoic acid

: 108-88-3
toluene

: 101493-90-7
1-p-Tolyl-docosan-1-one

Conditions

Conditions	Yield
Ce3+ exchanged Y-fanjasite at 150℃; for 48h;	100%

: 1711-05-3
m-anisoyl chloride

: 108-88-3
toluene

: 82520-37-4
(4-methylphenyl)-(3-methoxyphenyl)methanone

Conditions

Conditions	Yield
Stage #1: m-anisoyl chloride; toluene With aluminum (III) chloride In dichloromethane at 20℃; for 4h; Stage #2: With hydrogenchloride In dichloromethane; water	100%
With aluminium trichloride	84%
With aluminium trichloride In nitromethane for 0.75h; Ambient temperature;	84%
With aluminium trichloride In 1,2-dichloro-benzene
With aluminium trichloride In dichloromethane at 20℃;

: 108-88-3
toluene

: 124-38-9
carbon dioxide

Conditions

Conditions	Yield
With α-manganese oxide; oxygen at 290℃; Temperature; [1,2]-Wittig Rearrangement; Inert atmosphere;	100%
With oxygen at 258℃; under 760.051 Torr; Kinetics; Reagent/catalyst; Temperature; Inert atmosphere;	100%
With oxygen at 230 - 240℃; for 0.5h; Reagent/catalyst; Temperature; Inert atmosphere;	99.9%

: 75-77-4
chloro-trimethyl-silane

: 108-88-3
toluene

: 183245-70-7
3-methyl-2-methylene-3-phenyloxetane

: 3-methyl-3,5-diphenyl-2-[(trimethylsilyl)oxy]-1-pentene

Conditions

Conditions	Yield
Stage #1: toluene; 3-methyl-3-phenyl-2-methyleneoxetane With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane at 0℃; for 1.5h; Stage #2: chloro-trimethyl-silane In hexane at 0℃; for 0.55h;	100%

...Expand

: 108-88-3
toluene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 195062-57-8
p-tolylboronic pinacol ester

Conditions

Conditions	Yield
[Ir(COD)(1,3-dicyclohexylimidazolidin-2-ylidene)2]CF3CO2 at 40℃; for 10h;	100%
(η4-1,5-cyclooctadiene)bis(1,3-dimethylimidazolin-2-ylidene)iridium(I) trifluoracetate In toluene byproducts: H2; (N2); using Schlenk techniques; dissolving of 2 mmol pinacolborane and 1.5 mol% of Ir(COD)(C3H2N2Me2)2CF3CO2 in toluene; stirring and heating at40°C for 12 h; monitoring by GC-MS; removal of solvent under vac. at room temp.; chromy. over silica gel, eluting with CH2Cl2;	100%
(η4-1,5-cyclooctadiene)(1,1'-dimethyl-3,3'-o-xylylene-diimidazolin-2,2'-diylidene)iridium(I) trifluoroacetate In toluene (N2); using Schlenk techniques; dissolving of 2 mmol pinacolborane and 1.5 mol% of Ir(COD)(1,1'-dimethyl-3,3'-o-xylylene-diimidazolin-2,2'-diylidene)2(CF3CO2) in toluene; stirring and heating at 40°C for 12 h; monitoring by GC-MS; removal of solvent under vac. at room temp.; chromy. over silica gel, eluting with CH2Cl2;	100%

: 199620-14-9, 13007-92-6
chromium(0) hexacarbonyl

: 108-88-3
toluene

: 12083-24-8
tricarbonyl(η(6)-toluene)chromium

Conditions

Conditions	Yield
With catalyst: dimethyl succinate In decalin byproducts: CO; refluxing for 2.3 h (catalyst: dimethyl succinate); freezing out at -18°C or quick chromy. of the decaline soln. on a SiO2 column;	100%
With catalyst: butyl acetate In decalin byproducts: CO; refluxing for 3 h (catalyst: butyl acetate); freezing out at -18°C or quick chromy. of the decaline soln. on a SiO2 column;	99%
With acetic acid In decalin refluxing of toluene with the Cr compd. (4:1) and 25 microliter AcOH for 4 h;	98.7%

: 51031-50-6
heptafluoropropane-2-sulphenic acid chloride

: 108-88-3
toluene

A: 754-62-1
bis(perfluoroisopropyl) disulfide

B: 68408-97-9
heptafluoropropane-2-thiol

C: 68409-03-0
benzyl perfluoroisopropyl sulfide

D: 100-44-7
benzyl chloride

Conditions

Conditions	Yield
	A n/a B n/a C 4% D 100%
	A n/a B n/a C 4% D 100%

...Expand

: 32308-83-1
nonafluoro-tert-butanesulfenyl chloride

: 108-88-3
toluene

A: 32308-82-0
nonafluoro-tert-butanethiol

B: 100-44-7
benzyl chloride

Conditions

Conditions	Yield
	A 100% B 100%
	A 100% B 100%

...Expand

: 10170-69-1
dimanganese decacarbonyl

: 62637-93-8
trimethylamine-N-oxide dihydrate

: 108-88-3
toluene

: {{Mn(μ3-OH)(CO)3}4}*2toluene

Conditions

Conditions	Yield
In tetrahydrofuran; toluene stirring Mn2(CO)10 with Me3NO*2H2O in THF (18 h), solvent removal; recrystn. (hot toluene);	100%
In toluene byproducts: trimethylammonium carbonate; treatment of Mn2(CO)10 with 6 equivs. of Me3NO, boiling of product in MePh; hot filtration, crystn. (5°C); second crop from mother liquor; elem. anal.;	98%

...Expand

: 86197-44-6
bis(pentafluorophenyl)(η6-anisole)cobalt(II)

: 108-88-3
toluene

: 60528-58-7
(η6-toluene)bis(η1-pentafluorophenyl)cobalt(II)

Conditions

Conditions	Yield
In chloroform-d1 byproducts: anisole; mol. ratio 1/10; not isolated, detected by NMR;	100%
In chloroform-d1 byproducts: anisole; mol. ratio 1/1; not isolated, detected by NMR;	85%

: 121-00-6
3-tert-Butyl-4-hydroxyanisole

: 7550-45-0
titanium tetrachloride

: 108-88-3
toluene

: trichloromono(2-tert-butyl-4-methylphenoxide)titanium(IV)*0.0625(toluene)

Conditions

Conditions	Yield
In toluene byproducts: HCl; under N2; 2-tert-butyl-4-methylphenol in toluene added to TiCl4 (molar ratio 1:1) in toluene; refluxed for 13 h; filtered; solvent removed; dried under vac. for 4 h; elem. anal.;	100%

...Expand

: 1109-15-5
tris(pentafluorophenyl)borate

: 75-24-1
trimethylaluminum

: 108-88-3
toluene

: tris(pentafluorophenyl)aluminum*(toluene)0.5

Conditions

Conditions	Yield
In hexane	100%
In hexane; toluene B(C6F5)3 and AlMe3 in 1:3 toluene/hexanes mixt.;	99%
In hexane; toluene (inert atm.); reaction of borane deriv. with trimethylaluminium in hexane/toluene (3:1);	99%

...Expand

: [Rh(C8H12)(PO2C12H4C16H36)2C8H12O5](1+)*BF4(1-)*0.5CH2Cl2=[Rh(C8H12)(PO2C12H4C16H36)2C8H12O5]BF4*0.5CH2Cl2

: 108-88-3
toluene

: [Rh(C7H8)(PO2C12H4C16H36)2C8H12O5](1+)*BF4(1-)*C7H8=[Rh(C7H8)(PO2C12H4C16H36)2C8H12O5]BF4*C7H8

Conditions

Conditions	Yield
In toluene 100 mL vessel filled with a soln. of Rh(C8H12)diphosphiteBF4 in toluene, placed into an autoclave, autoclave purged 3 times with H2 and pressurised to the appropriate pressure (5 bar), after react. time of 3 h at room temp. autoclave depressurised; concentration to dryness, elem. anal.;	100%

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