As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:556-48-9
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryStock products, own laboratory Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to qu
Purity greater than 99.5% All over the years, backed by strong technical team, high efficiency management and perfect after-sales service, we have sold our products in over 20 cities and provinces around China. Advanced equipments, complete testing
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:556-48-9
Min.Order:1
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Type:Other
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:556-48-9
Min.Order:1 Kilogram
FOB Price: $1.0 / 3.0
Type:Trading Company
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:556-48-9
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiry1,4-Cyclohexanediol Basic information Product Name: 1,4-Cyclohexanediol Synonyms: QUINITOL;1,4-HEXANEDIOL;1,4-DIHYDROXYCYCLOHEXANE;1,4-CYCLOHEXANEDIOL;1,4-BIS(HYDROXY)-CYCLOHEXANE;HEXAHY
Cas:556-48-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:556-48-9
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:556-48-9
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam
Cas:556-48-9
Min.Order:1 Kilogram
FOB Price: $7.0 / 10.0
Type:Trading Company
inquiryProduct name: 1,4-Cyclohexanediol CAS NO.: 556-48-9 English name: 1,4-Cyclohexanediol; Hexahydrohydroquinone; CHDM; Quinitol Purity: 99.50% Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Applic
Cas:556-48-9
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:556-48-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:556-48-9
Min.Order:10 Gram
FOB Price: $1.52
Type:Trading Company
inquiryProduct Name: 1,4-Cyclohexanediol CAS: 556-48-9 MF: C6H12O2 MW: 116.16 EINECS: 209-126-2 Mol File: 556-48-9.mol 1,4-Cyclohexanediol Structure 1,4-Cyclohexanediol Chemical Properties Melting point 98-100 °C (lit.) Boiling
1,4-Cyclohexanediol CAS:556-48-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:556-48-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:556-48-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:556-48-9
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiry1,4-Cyclohexanediol CAS: 556-48-9 Specification Item Standard Test Results Identification A.H-NMR:Comply with the structure Complies B.LC-MS:Comply with the
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out
Cas:556-48-9
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:556-48-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:556-48-9
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:556-48-9
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:556-48-9
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white to off-white crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medicine ,
Product name: 1,4-Cyclohexanediol CAS No.:556-48-9 Molecule Formula:C6H12O2 Molecule Weight:116.16 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:556-48-9
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:556-48-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With hydrogen In water at 30℃; under 7500.75 Torr; for 7h; Autoclave; | 99.1% |
With hydrogen In water at 80℃; under 15001.5 Torr; for 6h; | 99% |
With potassium hydroxide; samarium diiodide In tetrahydrofuran; water for 0.05h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran at 20℃; | 99% |
With sodium tetrahydroborate; TiO(acac)2 In tetrahydrofuran for 0.17h; Heating; | 93% |
With sodium tetrahydroborate; Dowex1-x8 In tetrahydrofuran for 0.34h; Heating; | 90% |
Conditions | Yield |
---|---|
With hydrogen In n-heptane at 140℃; under 750.075 Torr; for 6h; Catalytic behavior; | A 99% B 99% |
(4-hydroxycyclohexyl) 4-methylbenzoate
1,4-Cyclohexanediol
Conditions | Yield |
---|---|
With methanol; samarium diiodide In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide Reflux; | 98% |
With methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide In tetrahydrofuran Inert atmosphere; Reflux; | 98% |
1,4-bis-trimethylsiloxycyclohexane
1,4-Cyclohexanediol
Conditions | Yield |
---|---|
With water; p-toluenesulfonyl chloride at 20℃; for 0.0833333h; | 91% |
With aminosulfonic acid; water at 20℃; for 4.5h; | 91% |
With water; boric acid at 20℃; for 24h; | 85% |
4-(4-methylbenzoyloxy)cyclohexyl 4-(trifluoromethyl)benzoate
1,4-Cyclohexanediol
Conditions | Yield |
---|---|
With tetrabutylammonium tetrafluoroborate In 1-methyl-pyrrolidin-2-one; isopropyl alcohol at 90℃; Electrochemical reaction; | 65% |
Conditions | Yield |
---|---|
In isopropyl alcohol | 53% |
4,4'-dihydroxydiphenyl ether
A
cyclohexane
B
1,4-Cyclohexanediol
C
cyclohexanol
Conditions | Yield |
---|---|
With isopropyl alcohol at 150℃; for 6h; Sealed tube; | A 10.5 %Chromat. B 8.4% C 76.2 %Chromat. |
Conditions | Yield |
---|---|
With water; sodium hydrogencarbonate unter Durchleiten von CO2; cis-quinitol; |
(1S,4R)-Cyclohex-2-ene-1,4-diol
A
4-hydroxy-2-cyclohexenone
B
1,4-Cyclohexanediol
C
4-hydroxycyclohexanone
Conditions | Yield |
---|---|
ruthenium In tetrahydrofuran at 65℃; for 15h; Yield given. Yields of byproduct given; | |
ruthenium In tetrahydrofuran at 60℃; for 15h; Yield given. Yields of byproduct given; |
4-hydroxycyclohexanone
A
1,4-Cyclohexanediol
B
cyclohexanone
C
cyclohexanol
Conditions | Yield |
---|---|
With hydrogen; palladium In tert-butyl alcohol at 30℃; Yield given. Yields of byproduct given; | |
With hydrogen; palladium In tert-butyl alcohol at 30℃; Product distribution; further catalyst, further 4-substituted cyclohexanone; |
acetaldehyde
cyclohexa-1,3-diene
A
1,2-Cyclohexanediol
B
cyclohexane-1,3-diol
C
1,4-Cyclohexanediol
D
(1R*,1'RS*)-1-cyclohex-2-enylethanol
E
3-cyclohexen-1-ol
Conditions | Yield |
---|---|
With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide Product distribution; other cyclic dienes and hydroborating agents; |
Conditions | Yield |
---|---|
With hydrogen; silica gel; nickel In isopropyl alcohol at 100℃; under 4650.4 Torr; Product distribution; Kinetics; various catalyst, var. temp., var. of hydrogen pressure, var. of substrate concentr.; | A n/a B 87 % Chromat. |
With hydrogen; palladium/alumina at 130℃; under 22502.3 Torr; Conversion of starting material; | |
With Zr -F-100 In isopropyl alcohol at 82℃; for 6h; Reagent/catalyst; | |
With nicotinamide adenine dinucleotide phosphate; isopropyl alcohol In aq. phosphate buffer at 30℃; for 12h; pH=7; Enzymatic reaction; |
1,4-Cyclohexanedione
A
1,4-Cyclohexanediol
B
4-hydroxycyclohexanone
C
cyclohexanone
D
cyclohexanol
Conditions | Yield |
---|---|
With hydrogen; palladium In tert-butyl alcohol at 30℃; Product distribution; further catalyst; | |
With hydrogen; palladium In tert-butyl alcohol at 30℃; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With hydrogen; nickel at 170℃; trans-quinitol; |
cyclohexanone
A
Adipic acid
B
succinic acid
C
1,4-Cyclohexanediol
D
1,4-Cyclohexanedione
Conditions | Yield |
---|---|
With peracetic acid; Ru-carbon In ethyl acetate at 20℃; for 1h; Further byproducts given; | A 48 % Chromat. B 26 % Chromat. C n/a D 8 % Chromat. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: concentrated sulfuric acid View Scheme | |
Multi-step reaction with 2 steps 1: concentrated sulfuric acid 2: NaHCO3; water / unter Durchleiten von CO2 View Scheme |
methanol
A
3,4,5,6-tetrahydro-2H-pyran-2-one
B
hexanedioic acid dimethyl ester
C
methyl 6-hydroxycaproate
D
Dimethyl glutarate
E
methyl 5-hydroxypentanoate
F
1,2-Cyclohexanediol
G
1,4-Cyclohexanediol
H
Dimethyl succinate
Conditions | Yield |
---|---|
With sulfuric acid |
hydroquinone
A
1,4-Cyclohexanediol
B
4-hydroxycyclohexanone
C
1,4-Cyclohexanedione
Conditions | Yield |
---|---|
With hydrogen; Pd/hydrophilic-C at 100℃; under 7500.75 Torr; for 20h; |
cyclohexane
A
Adipic acid
B
6-Hydroxyhexanoic acid
C
1,4-Cyclohexanediol
Conditions | Yield |
---|---|
With oxygen at 160℃; under 7500.75 Torr; |
Conditions | Yield |
---|---|
With carbon dioxide; hydrogen at 50℃; under 30003 - 90009 Torr; for 4h; Supercritical conditions; | |
With hydrogen In water at 25℃; under 750.075 Torr; for 7h; Autoclave; | |
With hydrogen In dichloromethane at 50℃; under 7500.75 Torr; for 1h; |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 160℃; under 11251.1 Torr; |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 160℃; under 11251.1 Torr; |
Conditions | Yield |
---|---|
With rhodium contaminated with carbon; water; hydrogen at 80℃; for 18h; Supercritical conditions; Autoclave; |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 150℃; under 9000.9 Torr; |
hydroquinone
A
1,4-Cyclohexanediol
B
1,4-Cyclohexanedione
C
phenol
Conditions | Yield |
---|---|
With hydrogen In water at 119.84℃; under 4500.45 Torr; Kinetics; |
hydroquinone
A
1,4-Cyclohexanediol
B
4-hydroxycyclohexanone
C
cyclohexanone
D
cyclohexanol
Conditions | Yield |
---|---|
With hydrogen In water at 25℃; under 760.051 Torr; for 15h; Schlenk technique; Green chemistry; |
Conditions | Yield |
---|---|
With [Cu3(μ3-5-(4-pyridyl)tetrazolate)4(μ2-N3)2(DMF)2]n·(DMF)2n; dihydrogen peroxide In neat (no solvent) at 20℃; under 760.051 Torr; for 24h; Green chemistry; |
1,4-Cyclohexanediol
1,4-cyclohexanediol-O,O-d2
Conditions | Yield |
---|---|
With water-d2 for 6h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 99% |
With pyridine; dmap In dichloromethane at 25℃; for 4h; | 30% |
With pyridine In dichloromethane at 25℃; for 4h; | 30% |
With pyridine In chloroform at 0 - 20℃; for 6h; |
Conditions | Yield |
---|---|
With MgLa mixed oxides at 129.85℃; for 0.75h; | 98% |
aluminum oxide; cesium fluoride at 129.85℃; for 0.5h; | 97% |
With MgLa mixed oxide at 125℃; for 0.75h; | 97% |
With immobilized 1,5,7-triazabicyclo[4.4.0]dec-5-ene on magnetic γ-Fe2O3 nanoparticles at 125℃; for 10h; | 94% |
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In neat (no solvent) at 20℃; for 1h; Milling; | 97% |
With ruthenium(IV) oxide; sodium dihydrogenphosphate; sodium chloride In water at 10 - 15℃; electrooxidation; | 94% |
With m-iodosylbenzoic acid; ruthenium trichloride In water; acetonitrile at 20℃; for 10h; | 84% |
1,4-Cyclohexanediol
1,1,1,3,3,3-hexamethyl-disilazane
1,4-bis-trimethylsiloxycyclohexane
Conditions | Yield |
---|---|
iodine In dichloromethane at 20℃; for 0.0666667h; Substitution; | 97% |
With boric acid In acetonitrile at 20℃; for 2h; | 97% |
With aminosulfonic acid In acetonitrile at 20℃; for 2h; | 95% |
Stage #1: 1,4-Cyclohexanediol With Iron(III) nitrate nonahydrate; sodium iodide In dichloromethane at 20℃; Stage #2: 1,1,1,3,3,3-hexamethyl-disilazane In dichloromethane at 20℃; for 0.0416667h; | 90% |
With p-toluenesulfonyl chloride In dichloromethane at 20℃; for 0.5h; | 85% |
1,4-Cyclohexanediol
4-chlorocyclohexanol
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; N,N-dimethyl-formamide In dichloromethane at 25℃; for 0.25h; | 95% |
With hydrogenchloride at 100℃; im geschlossenen Gefaess; | |
With hydrogenchloride |
1,4-Cyclohexanediol
acetic anhydride
1,4-diacetoxycyclohexane
Conditions | Yield |
---|---|
at 90℃; for 2h; | 95% |
With nickel dichloride at 20℃; for 0.5h; Neat (no solvent); | 92% |
With N-Bromosuccinimide In dichloromethane at 20℃; for 12h; | 84% |
3,4-dihydro-2H-pyran
1,4-Cyclohexanediol
A
1,4-Bis--cyclohexan
B
4-(2-Tetrahydropyranyloxy)-1-cyclohexanol
Conditions | Yield |
---|---|
With Dowex 50W x 2 (50-100 mesh) In toluene at 30℃; for 1.5h; | A 3% B 95% |
With iodine In tetrahydrofuran at 67℃; for 0.0472222h; Irradiation; | A 15% B 77% |
aluminum(III) sulfate; silica gel In hexane for 8h; Ambient temperature; | A 9 % Chromat. B 71 % Chromat. |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 10 - 20℃; for 6h; | 94.7% |
1,4-Cyclohexanediol
Conditions | Yield |
---|---|
With γ-Fe2O3-immobilized 1,5,7-triazabicyclo[4.4.0]dec-5-ene nanoparticles (MNPs-TBD) at 125℃; for 10h; | 94% |
3,4-dihydro-2H-pyran
1,4-Cyclohexanediol
4-(2-Tetrahydropyranyloxy)-1-cyclohexanol
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In tetrahydrofuran for 6h; Ambient temperature; | 93% |
With lithium trifluoromethanesulfonate In 1,2-dichloro-ethane for 5.5h; Heating; | 93% |
With pyridinium p-toluenesulfonate In dichloromethane at 10 - 20℃; for 7h; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
With sodium bromate; sodium hydrogensulfite In water; acetonitrile at 20℃; for 6h; Oxidation; | A 1% B 93% |
With sodium bromate; sodium hydrogensulfite In water; acetonitrile at 20℃; for 2h; Oxidation; | A 78% B 10% |
With 2O34W9Zn(12-)*W(6+)*3Zn(2+)*2H2O; dihydrogen peroxide In water; acetonitrile at 135℃; under 2250.23 Torr; for 0.25h; Microwave irradiation; | A n/a B 58% |
Conditions | Yield |
---|---|
With p-toluenesulfonyl chloride at 20℃; for 0.633333h; neat (no solvent); | 93% |
With Iron(III) nitrate nonahydrate; sodium iodide at 20℃; for 0.833333h; neat (no solvent); | 92% |
1,4-Cyclohexanediol
4-hydroxycyclohexanone
Conditions | Yield |
---|---|
With sodium bromate; ammonium cerium(IV) nitrate In water; acetonitrile | 92% |
With sodium bromate; ammonium cerium (IV) nitrate In water; acetonitrile for 2.5h; Reflux; | 91% |
With calcium hypochlorite; potassium bromide In water; acetic acid at 0℃; for 3h; | 88% |
1,4-Cyclohexanediol
cyclohexa-1,4-diene
Conditions | Yield |
---|---|
With 1,1,1-trichloro-3,3,3-trifluoro-propan-2-one; toluene-4-sulfonic acid In benzene for 6h; Heating; | 92% |
5-Norbornene-2-carboxaldehyde
1,4-Cyclohexanediol
Conditions | Yield |
---|---|
sodium hydride at 20℃; for 10h; | 92% |
1,4-Cyclohexanediol
7-oxa-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde
Conditions | Yield |
---|---|
sodium hydride at 20℃; for 10h; | 92% |
Conditions | Yield |
---|---|
at 160℃; for 5h; Molecular sieve; Inert atmosphere; | 88.4% |
Conditions | Yield |
---|---|
With p-toluenesulfonyl chloride at 20℃; for 0.383333h; neat (no solvent); | 88% |
With triethylamine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; |
1.3-propanedithiol
1,4-Cyclohexanediol
1,5-dithiaspiro<5.5>undecan-9-ol
Conditions | Yield |
---|---|
Stage #1: 1,4-Cyclohexanediol With sodium bromate; ammonium cerium (IV) nitrate In water; acetonitrile for 1h; Reflux; Stage #2: 1.3-propanedithiol With boron trifluoride diethyl etherate In dichloromethane at 0℃; for 0.25h; | 88% |
1,4-Cyclohexanediol
tert-butyldimethylsilyl chloride
4-((tert-butyldimethylsilyl)oxy)cyclohexan-1-ol
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran at 20℃; for 16h; | 86.7% |
With 1H-imidazole In tetrahydrofuran; N,N-dimethyl-formamide at 0℃; | 66% |
With 1H-imidazole In tetrahydrofuran; N,N-dimethyl-formamide at 0℃; | 62% |
Conditions | Yield |
---|---|
at 150℃; for 4h; Molecular sieve; Inert atmosphere; | 86.6% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In toluene at 150℃; for 4h; Inert atmosphere; | 84.1% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 40℃; for 18h; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 24h; | 84% |
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