Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:583-59-5
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Min.Order:100 Kilogram
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryChemical Name 2-Methylcyclohexanol Synonyms o-methyl-cyclohexano;2-methyl-1-cyclohexanol;2-methylcyclohexan-1-ol;2-methylcyclohexyl alcohol;O-METHYLCYCLOHEXANOL CAS No. 583-5
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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Min.Order:100 Gram
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inquiry2-Methylcyclohexanol cas 583-59-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low priceAppearance:Colourless viscous liquid with an aromatic odour Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
Conditions | Yield |
---|---|
With zinc hydride In tetrahydrofuran for 24h; Ambient temperature; | 100% |
With sodium isopropylate; acetonitrile In isopropyl alcohol at 80℃; for 1h; Catalytic behavior; | 99% |
gadolinium(III) isopropoxide In isopropyl alcohol at 30℃; for 1h; | 98% |
2-(2-methyl-cyclohexyloxy)-tetrahydro-pyran
2-Methylcyclohexanol
Conditions | Yield |
---|---|
silica-supported prop-1-ylsulfonic acid In methanol | 99.6% |
With sulfuric acid; silica gel In methanol for 0.25h; Heating; | 80% |
With H14[NaP5W30O110] In methanol for 2h; Heating; | 97 % Chromat. |
Conditions | Yield |
---|---|
With hydrogen In water at 20℃; under 7500.75 Torr; for 6h; Autoclave; | 99.1% |
With hydrogen at 100℃; under 3750.38 Torr; for 3h; Reagent/catalyst; Pressure; Temperature; | 99% |
With nickel(II) oxide; hydrogen; palladium In hexane at 80℃; under 7500.75 Torr; for 10h; | 98% |
Conditions | Yield |
---|---|
With [{2-(2-pyridyl)benzimidazole}RuCl2(PPh3)2]; potassium hydroxide at 82℃; for 4h; | 97% |
With potassium hydroxide for 4h; Ambient temperature; | 8% |
Mechanism; Product distribution; Irradiation; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; triethylamine In water; acetonitrile Irradiation; | 94% |
With cobalt(II) tetrafluoroborate hexahydrate; hydrogen; zinc trifluoromethanesulfonate; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In 1,4-dioxane at 60℃; under 30003 Torr; for 20h; Autoclave; regioselective reaction; | 88 %Chromat. |
With ammonia borane; C28H28Cl2CoNP2; erbium(III) triflate In tetrahydrofuran at 55℃; for 8h; | 89 %Chromat. |
1,2-epoxy-3-methyl-cyclohexane
A
2-Methylcyclohexanol
B
m-methylcyclohexanol
Conditions | Yield |
---|---|
With Li(1+)*C12H28AlO3(1-) In tetrahydrofuran; hexane at 0℃; for 0.17h; Yields of byproduct given. Title compound not separated from byproducts; | A 93% B n/a |
With Li(1+)*C12H28AlO3(1-) In tetrahydrofuran; hexane at 0℃; for 0.17h; | A 93% B n/a |
Conditions | Yield |
---|---|
Stage #1: 1-methylcyclohex-1-ene With 1-bromo-butane; sodium tetrahydroborate; Aliquat 336 at 20℃; for 16h; Addition; Hydroboration; Stage #2: With sodium hydroxide; dihydrogen peroxide at 40℃; for 1h; Oxidation; | 78% |
With sodium tetrahydroborate; (2,3,7,8,12,13,17,18-octaethylporphyrinato)rhodium(III) chloride; oxygen In tetrahydrofuran at 20 - 25℃; for 50h; Product distribution; Mechanism; other olefins, diene and acetylenes, other rhodium porphyrin, other conc. of catalyst; | |
With sodium tetrahydroborate; oxygen; (2,3,7,8,12,13,17,18-octaethylporphyrinato)rhodium(III) chloride In tetrahydrofuran Ambient temperature; 48-130 h; Yield given; |
2-Trimethylsilanylmethyl-cyclohexanol
2-Methylcyclohexanol
Conditions | Yield |
---|---|
With potassium tert-butylate; 18-crown-6 ether In water; dimethyl sulfoxide at 80℃; for 12h; | 78% |
2-(6-Methyl-1-oxa-4-aza-spiro[4.5]dec-4-yl)-ethanol
A
2-Methylcyclohexanol
B
2-(7-Methyl-4,5,6,7-tetrahydro-indol-1-yl)-ethanol
C
2,2'-iminobis[ethanol]
Conditions | Yield |
---|---|
With potassium hydroxide Heating; CH3ONa as reagent; | A n/a B 59% C n/a |
1,5-bis(bromomagnesio)hexane
formic acid ethyl ester
2-Methylcyclohexanol
Conditions | Yield |
---|---|
In tetrahydrofuran | 57% |
Conditions | Yield |
---|---|
With Cu2(OTf)2; (-)-(aR)-[1,1'-binaphthalene]-8,8'-diyl dimethylphosphoramidite In tetrahydrofuran at -78 - 20℃; Ring cleavage; methylation; | 45% |
Conditions | Yield |
---|---|
With [(hydrotris(3,5-diphenyl-pyrazol-1-yl)borate)FeII(benzilate)]; oxygen; scandium tris(trifluoromethanesulfonate) In benzene at 20℃; Inert atmosphere; | A 13% B 45% |
With [(hydrotris(3,5-diphenyl-pyrazol-1-yl)borate)FeII(benzilate)]; oxygen; pyridinium perchlorate In acetonitrile; benzene at 20℃; for 0.25h; Catalytic behavior; Reagent/catalyst; | A 15% B 44% |
With 2,6-dimethylpyridine; Cumene hydroperoxide; [FeII(1,1’-(((pyridin-2-ylmethyl)azanediyl)bis(ethane-2,1-diyl))bis(3-(tert-butyl)urea))(H2O)(trifluoromethanesulfonate)](trifluoromethanesulfonate) In acetonitrile at -20.16 - 9.84℃; for 1h; Catalytic behavior; Inert atmosphere; |
methyl cyclohexane
A
p-methylcyclohexanol
B
2-Methylcyclohexanol
C
1-Methylcyclohexanol
D
m-methylcyclohexanol
Conditions | Yield |
---|---|
With iodosylbenzene; 5,10,15,20-tetraphenyl-21 H,23-H-porphine manganese(III)chloride In benzene for 2h; Ambient temperature; pAr = 1 atm; Further byproducts given. Title compound not separated from byproducts; | A 18% B 20% C 24% D 3% |
With iodosylbenzene; 5,10,15,20-tetraphenyl-21 H,23-H-porphine manganese(III)chloride In benzene for 2h; Ambient temperature; pAr= 1 atm; Further byproducts given. Title compound not separated from byproducts; | A 18% B 20% C 24% D 3% |
With peracetic acid; tris(μ-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate In acetonitrile at 30℃; for 1h; Yield given. Further byproducts given. Yields of byproduct given; |
2-Methylcyclohexanol
Conditions | Yield |
---|---|
With tetrahydrofuran; titanium(III) chloride; lithium for 40h; Heating; | 20% |
Conditions | Yield |
---|---|
at 24.9℃; Equilibrium constant; other temperatures; calculated values; | A 17% B 8.6% |
at 240 - 320℃; an metallbeschichtetem opt.-akt. Quarz; |
methyl magnesium iodide
trans-2-chlorocyclohexanol
A
2-Methylcyclohexanol
B
1-cyclopentylethan-1-ol
Conditions | Yield |
---|---|
With diethyl ether dl-trans-1-methyl-cyclohexanol-(2); |
Conditions | Yield |
---|---|
With ethanol; sodium | |
With diisobutylaluminium hydride In hexane; dichloromethane at -78℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With manganese containing nickel catalyst at 170℃; Hydrogenation.unter Druck; d-cis-1-methyl-cyclohexanol-(2); | |
With manganese containing nickel catalyst at 170℃; Hydrogenation.unter Druck; l-cis-1-methyl-cyclohexanol-(2); |
2,2-bis(4-hydroxy-3-methylphenyl)propane
A
2-Methylcyclohexanol
B
4-isopropyl-2-methylcyclohexanol
Conditions | Yield |
---|---|
in Gegenwart eines Kupfer, Kobalt und Mangan enthaltenen Nickelkatalysators.Hydrogenation; |
diethyl ether
methyllithium
cyclohexane-1,2-epoxide
2-Methylcyclohexanol
2-Methylcyclohexanone
A
2-Methylcyclohexanol
B
3-methyl-2-oxo-cyclohexanecarbaldehyde
Conditions | Yield |
---|---|
With diethyl ether; sodium; formic acid ethyl ester dl-trans-1-methyl-cyclohexanol-(2); |
Conditions | Yield |
---|---|
With CuO/Cr2O3 at 250℃; Hydrogenation; |
1,2-epoxy-1-methylcyclohexane
A
2-Methylcyclohexanol
B
1-Methylcyclohexanol
Conditions | Yield |
---|---|
With sodium tert-pentoxide; sodium hydride; nickel dichloride In 1,2-dimethoxyethane at 65℃; for 40h; Yield given. Yields of byproduct given; |
1,2-epoxy-1-methylcyclohexane
A
2-Methylcyclohexanol
B
1-Methylcyclohexanol
(1S,2S)-2-Isopropoxy-2-methyl-cyclohexanol
(1R,2R)-2-Isopropoxy-1-methyl-cyclohexanol
Conditions | Yield |
---|---|
In isopropyl alcohol Irradiation; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With dihydrogen peroxide In acetonitrile Irradiation; Yield given. Yields of byproduct given; |
2-methyl-2-cyclohexen-1-one
A
2-Methylcyclohexanol
B
2-methylcyclohex-2-en-1-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate; alpha cyclodextrin In water Product distribution; influence of other cyclodextrin on the reduction; | |
With sodium tetrahydroborate; β‐cyclodextrin In water for 24h; | A 35 % Chromat. B 65 % Chromat. |
With sodium tetrahydroborate In water Ambient temperature; | A 22 % Chromat. B 78 % Chromat. |
With sodium tetrahydroborate; alpha cyclodextrin In water for 24h; | A 10 % Chromat. B 90 % Chromat. |
2-methyl-2-cyclohexen-1-one
A
2-Methylcyclohexanol
B
2-methylcyclohex-2-en-1-ol
C
2-Methylcyclohexanone
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; cryptand 211 In tetrahydrofuran for 0.0833333h; Ambient temperature; Yield given. Yields of byproduct given; | |
With lithium aluminium tetrahydride In tetrahydrofuran for 0.0166667h; Ambient temperature; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With hydrogen; nickel In methanol at 170℃; under 114000 Torr; for 24h; Yield given; |
cyclohexane
methyl cyclohexane
A
p-methylcyclohexanol
B
2-Methylcyclohexanol
C
1-Methylcyclohexanol
D
m-methylcyclohexanol
E
2-Methylcyclohexanone
F
3-Methylcyclohexanone
Conditions | Yield |
---|---|
5,10,15,20-tetraphenyl-21 H,23-H-porphine manganese(III)chloride for 2h; Product distribution; Mechanism; Ambient temperature; variations of reagents, pO2, protective atmosphere; |
methyl cyclohexane
A
2-Methylcyclohexanol
B
1-Methylcyclohexanol
C
1-methylcyclohexan-4-one
D
3-Methylcyclohexanone
Conditions | Yield |
---|---|
With hydrogenchloride; oxygen; sodium L-ascorbate; 5,10,15,20-tetraphenyl-21 H,23-H-porphine manganese(III)chloride In benzene Ambient temperature; pH=8.5, pO2= 1 atm; Further byproducts given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium tungstate In tert-butyl alcohol at 90℃; for 0.5h; | 100% |
With jones reagent; silica gel In dichloromethane for 0.0833333h; | 99% |
With silica-supported Jones reagent In dichloromethane for 0.00269444h; | 99.7% |
3,4-dihydro-2H-pyran
2-Methylcyclohexanol
2-(2-methyl-cyclohexyloxy)-tetrahydro-pyran
Conditions | Yield |
---|---|
silica-supported prop-1-ylsulfonic acid In acetonitrile for 0.166667h; | 99.8% |
With sulfuric acid; silica gel for 0.0166667h; Irradiation; microwave; | 80% |
With H14[NaP5W30O110] In dichloromethane for 1h; Heating; | 94 % Chromat. |
Conditions | Yield |
---|---|
platinum; potassium oxide at 360℃; | A 98% B 2% |
platinum; potassium oxide at 360℃; Product distribution; other content of catalyst; | A 98% B 2% |
2-Methylcyclohexanol
p-toluenesulfonyl chloride
Toluene-4-sulfonic acid 2-methyl-cyclohexyl ester
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In ethyl acetate at 0 - 20℃; for 96h; | 95% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In acetonitrile for 2h; | 91% |
2-Methylcyclohexanol
2,2,6-trichloro-6-methylcyclohexanone
Conditions | Yield |
---|---|
With chlorine In N,N-dimethyl-formamide at 35 - 45℃; for 3h; | 91% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 100 - 124℃; for 3h; Temperature; | 89.8% |
With sulfuric acid at 100 - 110℃; |
2-Methylcyclohexanol
chloroacetic acid
(2-methylcyclohexyl)oxyacetic acid
Conditions | Yield |
---|---|
Stage #1: 2-Methylcyclohexanol With lithium In tetrahydrofuran for 16h; Inert atmosphere; Reflux; Stage #2: chloroacetic acid In tetrahydrofuran for 6h; Inert atmosphere; Reflux; | 89% |
2-Methylcyclohexanol
1,1,1,3,3,3-hexamethyl-disilazane
Trimethyl-(2-methyl-cyclohexyloxy)-silane
Conditions | Yield |
---|---|
With potassium fluoride incorporated on clinoptilolite nanoparticles In dichloromethane at 20℃; for 1.25h; chemoselective reaction; | 86% |
With sulfonic acid functionalized silica In dichloromethane at 20℃; for 1h; | 90 % Chromat. |
With [Ti(IV)(salophen)(OTf)2] In dichloromethane at 20℃; for 0.25h; | 98 %Chromat. |
2-Methylcyclohexanol
tert-Butyl 8-chloro-2,3-dihydropyrido[3,2-f][1,4]oxazepine-4(5H)-carboxylate
tert-butyl 8-[(2-methylcyclohexyl)oxy]-2,3-dihydropyrido[3,2-f][1,4]oxazepine-4(5H)-carboxylate
Conditions | Yield |
---|---|
Stage #1: 2-Methylcyclohexanol With sodium hydride In toluene at 70℃; for 0.25h; Inert atmosphere; Stage #2: tert-Butyl 8-chloro-2,3-dihydropyrido[3,2-f][1,4]oxazepine-4(5H)-carboxylate; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 100℃; for 2h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With pyridine In diethyl ether at 18 - 23℃; | 80% |
2-Methylcyclohexanol
ethyl 6-benzyl-2-(benzyloxy)-4-hydroxynicotinate
ethyl 6-benzyl-2-(benzyloxy)-4-(2-methylcyclohexyloxy)nicotinate
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 20h; | 80% |
2-Methylcyclohexanol
3,3,4-trichloro-3-butenoyl chloride
Conditions | Yield |
---|---|
With pyridine In diethyl ether at 20 - 23℃; for 22h; | 77% |
2-Methylcyclohexanol
ethyl 2-(benzyloxy)-4-hydroxy-6-phenethylnicotinate
ethyl 2-(benzyloxy)-4-(2-methylcyclohexyloxy)-6-phenethyl nicotinate
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 20h; | 76% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; Mitsunobu Displacement; | 51% |
2-Methylcyclohexanol
2-Chlorocyclohexanone
6-methyl-1,2,3,4-tetrahydrodibenzo[b,d]furan
Conditions | Yield |
---|---|
With titanium tetrachloride In 2,2,2-trifluoroethanol Inert atmosphere; Reflux; | 76% |
chloro-trimethyl-silane
2-Methylcyclohexanol
Trimethyl-(2-methyl-cyclohexyloxy)-silane
Conditions | Yield |
---|---|
With urea at 20℃; for 4h; | 73.4% |
2-Methylcyclohexanol
2,2,2-trichloroethyl heptanoate
Heptanoic acid (R)-2-methyl-cyclohexyl ester
Conditions | Yield |
---|---|
With porcine pancreatic lipase In n-heptane at 60℃; for 96h; | 72% |
Conditions | Yield |
---|---|
In hexane at -40 - 20℃; for 3h; Inert atmosphere; Schlenk technique; | 72% |
Conditions | Yield |
---|---|
With sulfuric acid at 20℃; Inert atmosphere; | 70% |
With sulfuric acid |
Conditions | Yield |
---|---|
With cerium(III) chloride heptahydrate; tetrabutyl-ammonium chloride In acetonitrile for 19h; Inert atmosphere; Irradiation; | 68% |
Conditions | Yield |
---|---|
With 1,3-dicyclohexylimidazol-2-ylidene at 25℃; for 0.25h; | 67% |
Conditions | Yield |
---|---|
With sulfuric acid at 25 - 30℃; | 66% |
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