As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:583-61-9
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryFactory supply 2,3-Lutidine Cas 583-61-9 with competitive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed addit
Cas:583-61-9
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
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2,3-Lutidine Basic information Product Name: 2,3-Lutidine Synonyms: LUT;2,3-DIMETHYLPYRIDINE;23L;2,3-LUTIDINE;2,3-dimethyl-pyridin;pyridine,2,3-dimethyl-;2,3-LUTIDI
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:583-61-9
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:583-61-9
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inquiryName 2,3-Lutidine Synonyms 2,3-DIMETHYLPYRIDINE(2,3-LUTIDINE);a,b-Dimethylpyridine;2,3-Lutidine (8CI);Pyridine, 2,3-dimethyl- (9CI);2,3-Lutidine, 98+% 100ML;2,3- twoMethy
1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:583-61-9
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:583-61-9
Min.Order:1 Kilogram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:583-61-9
Min.Order:1 Kilogram
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Type:Trading Company
inquiry2,3-Lutidine CAS:583-61-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:583-61-9
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:583-61-9
Min.Order:1 Kilogram
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiry2,3-Dimethylpyridine CAS:583-61-9 Specification Item Specification Appearance Clear Colorless to Slightly Yellow Liquid Assay 98%min Density 0.945 g/mL at 25 °C (lit.) Boiling Point
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:583-61-9
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:583-61-9
Min.Order:10 Gram
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inquiryadvantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
Cas:583-61-9
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Product name: 2,3-Lutidine CAS No.:583-61-9 Molecule Formula:C22H17IN2 Molecule Weight:436.29 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
2-Methyl-3-acetoxymethylpyridin
2,3-Lutidine
Conditions | Yield |
---|---|
With hydrogen; Pd-BaSO4 In ethanol for 0.5h; Ambient temperature; | 99.2% |
2,3-Lutidine
Conditions | Yield |
---|---|
Stage #1: N-(3-methyl-2-methyl-2H-pyridin-1-yl)-N-methyl-benzamidine With manganese triacetate; acetic acid at 60℃; for 2h; Stage #2: With water; acetic acid at 80℃; | 81% |
5-chloro-5,6-dimethyl-2,3,4,5-tetrahydropyridine
2,3-Lutidine
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran Heating; | 80% |
butanone
A
2,3-Lutidine
B
2,3,6-trimethylpyridine
C
2,3,4-lutidine
Conditions | Yield |
---|---|
With ammonia; chromium(III) oxide; aluminium at 350℃; | A 30.7% B 46.2% C 23% |
butanone
A
2,6-dimethylpyridine
B
2,3-Lutidine
C
2,3,6-trimethylpyridine
D
2,3,4-lutidine
Conditions | Yield |
---|---|
With ammonia; chromium(III) oxide; aluminium at 375℃; | A 6.8% B 24.6% C 45.4% D 25.7% |
With ammonia; chromium(III) oxide; aluminium at 425℃; | A 25.3% B 34.5% C 13.8% D 13.8% |
With ammonia; chromium(III) oxide; aluminium at 450℃; | A 21.8% B 22.4% C 29.4% D 11.7% |
With ammonia; chromium(III) oxide; aluminium at 300 - 450℃; Product distribution; |
3-Methylpyridine
A
pyridine
B
α-picoline
C
2,3-Lutidine
D
2,4-lutidine
E
2,5-dimethylpyridine
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; nickel at 330℃; under 750.06 Torr; Product distribution; | A 0.3% B 0.5% C 5.3% D 8% E 30.9% |
formaldehyd
acetaldehyde
acetone
A
2,3-Lutidine
B
3-ethylpyridine
C
2,3,4-lutidine
D
3-Methylpyridine
Conditions | Yield |
---|---|
With diammonium phosphate In ethanol; water at 234℃; for 1h; | A 25% B 8% C 13% D 22% |
α-picoline
A
pyridine
B
2,6-dimethylpyridine
C
2,3-Lutidine
D
2,5-dimethylpyridine
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; nickel at 330℃; under 750.06 Torr; Product distribution; | A 14.9% B 11.4% C 3% D 1.6% |
5,6-dimethyl-1,2,3,4-tetrahydro-pyridine
2,3-Lutidine
Conditions | Yield |
---|---|
With magnesium hydrosilicate; hydrogen; palladium at 280℃; |
6-chloro-2,3-dimethylpyridine
2,3-Lutidine
Conditions | Yield |
---|---|
With ethanol; palladium Hydrogenation; |
1-Methyl-3-acetylpiperidine
2,3-Lutidine
Conditions | Yield |
---|---|
With selenium at 300℃; |
4,6-dichloro-2,3-dimethyl-pyridine
2,3-Lutidine
Conditions | Yield |
---|---|
With methanol; potassium acetate; palladium Hydrogenation; |
2,3-bis(chloromethyl)-pyridine
2,3-Lutidine
Conditions | Yield |
---|---|
With methanol; palladium on activated charcoal; Lindlar's catalyst Hydrogenation; |
methanol
3-Methylpyridine
lead(IV) tetraacetate
acetic acid
A
2,3-Lutidine
B
2,5-dimethylpyridine
Conditions | Yield |
---|---|
at 110℃; |
4-methyl-5-oxohexanal
2,3-Lutidine
Conditions | Yield |
---|---|
With ethanol; water; hydroxylamine anschliessend Erwaermen mit wss. Salzsaeure; |
2,3-Lutidine
Conditions | Yield |
---|---|
bei der Zinstaub-Destillation; |
Conditions | Yield |
---|---|
With ammonia at 400℃; Leiten ueber mit Cadmiumphosphat impraegnierte Fullererde; |
2,3-Lutidine
Conditions | Yield |
---|---|
With methyllithium; calcium carbonate bei der Destillation; |
2,3-Lutidine
Conditions | Yield |
---|---|
With zinc durch Destillation; |
Conditions | Yield |
---|---|
bei der Destillation; |
5,6-dimethyl-1,2,3,4-tetrahydro-pyridine
2,3-Lutidine
Conditions | Yield |
---|---|
at 290℃; |
Conditions | Yield |
---|---|
at 300℃; unter Druck; |
3-methyl-cyclohexanone oxime
A
2,3-Lutidine
B
methyl cyclohexane
C
toluene
Conditions | Yield |
---|---|
levorotatory 1-methyl-cyclohexane oxime-(3); |
Conditions | Yield |
---|---|
With dimethyltitanocene at 20℃; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: Tf2O / CH2Cl2 / -40 - 20 °C 1.2: 80 percent / CH2Cl2 / -70 °C 2.1: Mn(OAc)3*2H2O; AcOH / 2 h / 60 °C 2.2: 81 percent / H2IO6; AcOH; H2O / 80 °C View Scheme |
[2,5-Dichloro-1,2-dimethyl-pent-(E)-ylidene]-isopropyl-amine
2,3-Lutidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 28 percent / NaN3 / dimethylsulfoxide / 20 h / 55 °C 2: 48 percent / SnCl2 / methanol / 5 h / 20 °C 3: 80 percent / KOBu-t / tetrahydrofuran / Heating View Scheme |
2,3-Lutidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 48 percent / SnCl2 / methanol / 5 h / 20 °C 2: 80 percent / KOBu-t / tetrahydrofuran / Heating View Scheme |
(2-methylpyridin-3-yl)methanol
2,3-Lutidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / 1.) room temp., 15 h, 2.) reflux, 2 h 2: 99.2 percent / H2 / Pd/BaSO4 / ethanol / 0.5 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 94 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 0.5 h / 40 °C 2: 91 percent / 1.) room temp., 15 h, 2.) reflux, 2 h 3: 99.2 percent / H2 / Pd/BaSO4 / ethanol / 0.5 h / Ambient temperature View Scheme |
2,3-Lutidine
2,3-dimethylpyridine 1-oxide
Conditions | Yield |
---|---|
With sodium tungstate; dihydrogen peroxide In water at 55℃; for 3h; Temperature; | 99% |
With 3-chloro-benzenecarboperoxoic acid In Isopropyl acetate at 10 - 35℃; for 5.83333h; Green chemistry; | 98.9% |
With △-Na8H[PW9O34]·19H2O; dihydrogen peroxide In water at 20℃; for 24h; Green chemistry; | 94% |
2,3-Lutidine
di-tert-butyl dicarbonate
Conditions | Yield |
---|---|
Stage #1: 2,3-Lutidine With chloro(1,5-cyclooctadiene)rhodium(I) dimer; borane-ammonia complex In 2,2,2-trifluoroethanol at 20℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube; Stage #2: di-tert-butyl dicarbonate With triethylamine In 2,2,2-trifluoroethanol at 20℃; Inert atmosphere; Schlenk technique; Sealed tube; | 99% |
2,3-Lutidine
bis(2,3-dimethylpyridino)tetra(μ2-O,O'-trimethylacetato)dicobalt(II)
Conditions | Yield |
---|---|
In acetonitrile under Ar atm. soln. 2,3-Me2C5H3N in MeCN was added to (Co(Me3CCOO)2)n and strirred at 80°C for 15 min; soln. was concd. at 0.1 Torr and 20°C and allowed to crystallize at 20°C for 12 h, ppt. was washed with cold benzene and dried under Ar stream; elem. anal.; | 98% |
2,3-Lutidine
Ni2(μ-H2O)(μ-OOC-tert-Bu)2(OOC-tert-Bu)2(tert-BuCOOH)4
bis(2,3-dimethylpyridino)tetra(μ2-O,O'-trimethylacetato)dinickel(II)
Conditions | Yield |
---|---|
In benzene under Ar atm. soln. 2,3-Me2C5H3N in benzene was added to Ni6(Me3CCOO)2)12 and strirred at 70°C for 15 min; soln. was concd. at 0.1 Torr and 20°C and allowed to crystallize at 20°C for 12 h, ppt. was washed with cold benzene and dried under Ar stream; elem. anal.; | 98% |
2,3-Lutidine
benzoyl chloride
2,3-dimethyl-N-benzoyliminopyridinium ylide
Conditions | Yield |
---|---|
Stage #1: 2,3-Lutidine With O-(2,4-dinitrophenyl)hydroxylamine In tetrahydrofuran; water at 40℃; for 12h; Stage #2: benzoyl chloride With sodium hydroxide In tetrahydrofuran at 20℃; for 4h; | 96% |
2,3-Lutidine
3-((3-methylpyridin-2-yl)methyl)-2-tosylisoindolin-1-one
Conditions | Yield |
---|---|
With scandium tris(trifluoromethanesulfonate) In α,α,α-trifluorotoluene at 120℃; for 24h; Inert atmosphere; screw-cap vial; | 95% |
Conditions | Yield |
---|---|
With triphenylcarbenium tetra(pentafluorophenyl)borate; C63H83N2O2ScSi2 In toluene at 40℃; for 48h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 95% |
Conditions | Yield |
---|---|
Stage #1: 2,3-Lutidine With boron trifluoride diethyl etherate In tetrahydrofuran for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: tert-butyl (E)-cinnamyl carbonate With C49H50IrNO4P(1+)*CF3O3S(1-); lithium hexamethyldisilazane In tetrahydrofuran at 30℃; for 8h; Inert atmosphere; Schlenk technique; enantioselective reaction; | 94% |
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; C42H51N3PSc In chlorobenzene at 100℃; for 8h; diastereoselective reaction; | 94% |
2,3-Lutidine
mesitylenesulfonylhydroxylamine
2,3-dimethylpyridin-1-ium-1-amine 2,4,6-trimethylbenzenesulfonate
Conditions | Yield |
---|---|
In dichloromethane for 0.5h; cooling; | 93% |
Conditions | Yield |
---|---|
In not given | 93% |
Conditions | Yield |
---|---|
at 80℃; for 0.333333h; | 93% |
Conditions | Yield |
---|---|
Stage #1: 2,3-Lutidine With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at 25℃; for 0.25h; Inert atmosphere; Stage #2: meta-bromotoluene With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 1-ethyl-2-pyrrolidinone; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere; | 91% |
2,3-Lutidine
ethyl-3,3,3-trifluoropyruvate
ethyl 3,3,3-trifluoro-2-hydroxy-2-(3-methylpyridin-2-ylmethyl)propanoate
Conditions | Yield |
---|---|
With ytterbium(III) triflate In 1,4-dioxane at 90℃; for 12h; | 91% |
With iron(II) acetate In 1,4-dioxane at 120℃; for 24h; Schlenk technique; Inert atmosphere; | 24% |
Conditions | Yield |
---|---|
With (C5Me4SiMe3)Sc(CH2C6H4NMe2-o)2; trityl tetrakis(pentafluorophenyl)borate In toluene at 70℃; for 36h; Glovebox; Schlenk technique; Sealed tube; stereoselective reaction; | 91% |
2,3-Lutidine
5-methyl-indole-2,3-dione
3-hydroxy-3-((3-methylpyridin-2-yl)methyl)indolin-2-one
Conditions | Yield |
---|---|
In water for 1h; Reagent/catalyst; Reflux; | 91% |
Conditions | Yield |
---|---|
Stage #1: 2,3-Lutidine With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: benzoic acid methyl ester In tetrahydrofuran; hexane at 0℃; for 3h; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; C42H51N3PSc In chlorobenzene at 100℃; for 9h; Inert atmosphere; Schlenk technique; Glovebox; | 91% |
2,3-Lutidine
[zinc(II)(μ2-κ1O:κ1O'-O2C(t-Bu))2(2,3-lutidine)]2
Conditions | Yield |
---|---|
In methanol soln. of C5H3NMe2 in MeOH added to soln. of Zn salt in MeOH, stirred at room temp. for 12 h; volatiles removed under vac., crystd. by diffusing CHCl3 over MeOH soln.at room temp. for 4 d; elem. anal.; | 90% |
2,3-Lutidine
1-bromo-4-methoxy-benzene
2-(4-methoxybenzyl)-3-methylpyridine
Conditions | Yield |
---|---|
Stage #1: 2,3-Lutidine With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at 25℃; for 0.25h; Inert atmosphere; Stage #2: 1-bromo-4-methoxy-benzene With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 1-ethyl-2-pyrrolidinone; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere; | 90% |
2,3-Lutidine
2-oxo-2H-chromene-3-carboxylic acid
4-((3-methylpyridin-2-yl)methyl)chroman-2-one
Conditions | Yield |
---|---|
In 1,4-dioxane at 120℃; for 48h; | 90% |
2,3-Lutidine
1-cyanoethyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 48h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl acetamide at 150℃; for 16h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | 90% |
Conditions | Yield |
---|---|
With n-butyllithium | 89% |
Conditions | Yield |
---|---|
Stage #1: 2,3-Lutidine With n-butyllithium; N-ethyl-N,N-diisopropylamine; sodium t-butanolate In tetrahydrofuran; hexane at -78℃; Stage #2: Dimethyldisulphide In tetrahydrofuran; hexane at -78℃; Further stages.; | 89% |
2,3-Lutidine
ruthenium(II) phthalocyanine
(phthalocyaninato)(2,3-lutidine)2-ruthenium(II)
Conditions | Yield |
---|---|
In neat (no solvent) under N2; refluxed for 5 h; addn. of hexane to hot soln.; slowly cooled down to room temp.; filtered; washed (MeOH); chromy. (Al2O3, CHCl3); dried (70°C); elem. anal.; UV; IR; | 89% |
2,3-Lutidine
2-oxo-2H-thiochromene-3-carboxylic acid
4-((3-methylpyridin-2-yl)methyl)thiochroman-2-one
Conditions | Yield |
---|---|
In 1,4-dioxane at 120℃; for 48h; | 89% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; oxygen; sodium formate; silver nitrate In water at 80℃; for 4h; Schlenk technique; regioselective reaction; | 89% |
With dipotassium peroxodisulfate; oxygen; sodium acetate; silver nitrate In water at 80℃; for 4h; Green chemistry; | 89% |
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