CAS No.109-06-8,2-Picoline Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t

2-Picoline suppliers in China

Cas:109-06-8

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2-picoline supplier in China

Cas:109-06-8

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Jinan Finer Chemical Co., Ltd

Product informations Product Name 2-Picoline CAS No. 109-06-8 Appearance

2-Picoline

Cas:109-06-8

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Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

2-picoline

Cas:109-06-8

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Hefei TNJ chemical industry co.,ltd

1.strict Quality control: Strictly in accordance with Chinese GMP(2010 version), guidelines issued by FDA,EDQM, and ICH relevant regulations, we have established a sound quality assurance system, implementing regular supervision and management in

2-Picoline

Cas:109-06-8

Min.Order:7000 Kilogram

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory supply 2-picoline

Cas:109-06-8

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

α-Picoline

Cas:109-06-8

Min.Order:5 Kiloliter

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Henan Tianfu Chemical Co., Ltd.

2-Picoline Basic information Product Name: 2-Picoline Synonyms: ALPHA-PICOLINE;ALPHAP;2-METHYLPYRIDINE;2-PICOLINE;.alpha.-Methylpyridine;2-methyl-pyridin;ai3-2409;alpha-Methylpyridine

2-Picoline 109-06-8

Cas:109-06-8

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Henan Sinotech Import&Export Corporation

Product:2-Picoline CASNO.:109-06-8 Molecular formula:C6H7N Molecular weight:93.13 EINECS: 203-643-7 Diagnosis-related group: Pesticide intermediates. Plant growth regulator intermediates Appearance:Colorless Liquid Storage: Store in cool an

2-Picoline

Cas:109-06-8

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Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

99% 2-Picoline 109-06-8 Pesticide Intermediate

Cas:109-06-8

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Baoji Guokang Healthchem co.,ltd

About us Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad.

2-Picoline

Cas:109-06-8

Min.Order:1 Kilogram

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Triumph International Development Limilted

Appearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:packaged in foil bags or tins Application:Use only for laboratory research Transportation:Sea,Air，DHL/TNT/FEdex/UPS/EMS Por

2-Picoline

Cas:109-06-8

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2-Picoline

Cas:109-06-8

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Picoline

Cas:109-06-8

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

2-METHYL PYRIDINE

Cas:109-06-8

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

2-Picoline

Cas:109-06-8

Min.Order:1 Gram

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2-picoline

Cas:109-06-8

Min.Order:10 Gram

FOB Price: $100.0

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

METHYL PYRIDINE

Cas:109-06-8

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Antimex Chemical Limied

ProName: 2-Picoline suppliers in China CasNo: 109-06-8 Molecular Formula: C6H7N Appearance: colourless to yellow liquid with an un... Application: Used as medicine, pesticide intermedia... DeliveryTime: prompt PackAge

2-Methylpyridine CAS 109-06-8

Cas:109-06-8

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Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

Pyridine, 2-methyl-CAS NO.: 109-06-8

Cas:109-06-8

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Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

2-Picoline

Cas:109-06-8

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Hangzhou ZeErRui Chemical Co., Ltd.

Name: 2-Picoline. Synonyms:2-Methylpyidine;2-PICOLINE98%;2-methylpyridine(2-Picoline);2-Picoline,98+%;Pyridine,Reagent;2-methylpyridine，2-pieoline;2-Picoline(2-Methylpyridine);NSC-3409 CAS No: 109-06-8. Molecular formula: C6H7N. Molecular w

2-Picoline manufacture

Cas:109-06-8

Min.Order:10 Gram

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Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an

2-Methylpyridine

Cas:109-06-8

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SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

SAGECHEM/2-Methylpyridine

Cas:109-06-8

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Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)

Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti

2-Methylpyridine

Cas:109-06-8

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colourless to yellow liquid with an unpleasant smell Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharma

2-Picoline

Cas:109-06-8

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Nanjing Yuance Industry&Trade Co., Ltd.

Product Name3-Amino-4-(trifluoromethyl)pyridine CAS 175204-80-5 MF C6H5F3N2 MW 162.11 Product Name3-Amino-4-(trifluoromethyl)py…

2-Picoline

Cas:109-06-8

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Hangzhou Dingyan Chem Co., Ltd

Hangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special chemicals and other fine chemicals. We could give you: 1.Best qualit

2-Picoline

Cas:109-06-8

Min.Order:1 Gram

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Hubei Vanz Pharm Co.,Ltd

ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai

2-Methylpyridine

Cas:109-06-8

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

2-Picoline

Cas:109-06-8

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Synthetic route

: (C5H5)2Zr(NC5H3CH3)(NC5H4CH3)(1+)*B(C6H5)4(1-)=(C5H5)2Zr(NC5H3CH3)(NC5H4CH3)B(C6H5)4

: 187737-37-7
propene

A: 109-06-8
α-picoline

B: (C5H5)2ZrCH2CH(CH3)NC5H3CH3(1+)*B(C6H5)4(1-)=(C5H5)2ZrCH2CH(CH3)NC5H3CH3B(C6H5)4

Conditions

Conditions	Yield
<10 min, 23°C, 1 atm.; monitored by NMR;	A n/a B 100%

...Expand

: 931-19-1
2-methylpyridine N-oxide

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With benzyl alcohol at 120℃; for 6h; Inert atmosphere;	99%
With cis-Cyclooctene; trans-dioxo(5,10,15,20-tetramesitylporphirinato)ruthenium(VI) In benzene at 80℃; for 15h;	96%
With diphosphorus tetraiodide In dichloromethane Heating; 10-20 min;	95%

: 75-05-8
acetonitrile

: 74-86-2
acetylene

: 109-06-8
α-picoline

Conditions

Conditions	Yield
at 150℃; for 22h; Autoclave;	94.3%
With decaethylene glycol mono n-hexadecyl ether; cyclopentadienyl-cyclooctadienyl-cobalt(I) In water for 4h; Ambient temperature; Irradiation;	18%
(η5-cyclopentadienyl)-η4-cycloocta-1,5-dienecobalt(I) at 40℃; for 2h; Irradiation; Yield given;
trimethylsilyl modified Cp-CO catalyst at 130 - 152℃; under 15001.2 Torr; for 2h;
η5-cyclopentadienylbis(ethene)cobalt at 40℃; for 3h; Product distribution; in the dark; variation of reaction time, temperature, catalyst. The influence of light and irradiation was investigated.;

: 5315-25-3
2-bromo-6-methylpyridine

A: 109-06-8
α-picoline

B: 4411-80-7
6,6'-dimethyl-2,2'-bipyridine

Conditions

Conditions	Yield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 18h; Inert atmosphere;	A 93.1% B 6.9%

: 110-86-1
pyridine

A: 110-89-4
piperidine

B: 109-06-8
α-picoline

C: 24362-44-5
1,5-di-(1-piperidyl)pentane

Conditions

Conditions	Yield
With hydrogen; Ni-Cr catalyst at 160℃; under 30400 Torr; for 8h; Product distribution; temperatures from 140 to 192 deg C, pressure 20 to 65 atm, reaction time 5 - 8 h;	A 91.8% B n/a C 0.1%

...Expand

: 110-86-1
pyridine

: 67-56-1
methanol

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With Fe-MnOx-Yb at 475℃; Gas phase;	89.5%
nickel(II) nitrate for 8h; Ambient temperature; Irradiation;	37.1%
With nano-diatomite modified magnesium aluminum hydrotalcite at 140 - 500℃; Temperature;

: 1452-77-3
pyridine-2-carboxylic acid amide

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With samarium diiodide; phosphoric acid In tetrahydrofuran for 0.000555556h; Ambient temperature;	88%

: 126963-92-6
benzyltri(2-(6-methylpyridyl))phosphonium bromide

A: 109-06-8
α-picoline

B: 4411-80-7
6,6'-dimethyl-2,2'-bipyridine

C: C19H19N2OP

Conditions

Conditions	Yield
With hydrogenchloride In water for 10h; Heating;	A 68% B 87% C n/a
With hydrogenchloride In water for 10h; Product distribution; Heating; variation of pH, temp. and time;	A 68% B 87% C n/a
With hydrogenchloride In water for 10h; Heating;	A 68% B 68% C n/a

...Expand

: 14402-20-1
N-cetyl-α-methylpyridinium iodide

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With triethylammonium hydrogensulfite at 150℃; for 30h; Mechanism;	86%

: 38700-15-1
triphenyl-(2-pyridylmethyl)phosphonium chloride

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With potassium tert-butylate; benzyl alcohol In tetrahydrofuran at 40℃; for 6h; Inert atmosphere;	80%

: 13115-43-0
2-pyridineacetic acid

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With potassium carbonate In chloroform at 20℃; for 24h; Irradiation; Inert atmosphere;	79%

: 110-86-1
pyridine

: 71-23-8
propan-1-ol

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With Raney nickel at 180℃; under 51716.2 Torr; for 0.5h; Concentration; Flow reactor; Green chemistry; regioselective reaction;	78%

: 110-86-1
pyridine

: 112-30-1
1-Decanol

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With Ra-Ni for 212h; Reflux; regioselective reaction;	71%

: C21H18N6O3

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With bis(1,5-cyclooctadiene)nickel (0); sodium isopropylate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 2-methyltetrahydrofuran at 80℃; for 12h; Green chemistry;	71%
With bis(tricyclohexylphosphine)nickel(II) dichloride; potassium iodide; zinc In 1,4-dioxane; methanol at 60℃; for 20h; Inert atmosphere; chemoselective reaction;

: 5029-67-4
2-iodopyridine

: 31729-70-1
bis(iodozinc)methane

: 109-06-8
α-picoline

Conditions

Conditions	Yield
Stage #1: 2-iodopyridine; bis(iodozinc)methane With triphenylphosphine; nickel dichloride In tetrahydrofuran at 40℃; Stage #2: With hydrogenchloride In tetrahydrofuran; water Reagent/catalyst; chemoselective reaction;	71%

: 1121-60-4
pyridine-2-carbaldehyde

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With hydrogen In para-xylene at 120℃; under 750.075 Torr; for 24h; Glovebox; Sealed tube; chemoselective reaction;	71%

: {C6H6NCr(H2O)5}(2+)

A: 109-06-8
α-picoline

B: 4916-40-9
1,2-bis(pyridin-2-yl)ethane

Conditions

Conditions	Yield
In perchloric acid addn. of Na2CO3;;	A 70% B 30%
In perchloric acid

: 1121-60-4
pyridine-2-carbaldehyde

A: 109-06-8
α-picoline

B: 586-98-1
2-Hydroxymethylpyridine

Conditions

Conditions	Yield
With hydrogen; GIPKh-105 copper-chromium catalyst at 200℃; Product distribution; Mechanism; other isomeric pyridinecarboxaldehydes; var. temp.;	A 14% B 66%

: 4377-33-7
2-chloromethylpyridine

: 100-52-7
benzaldehyde

A: 109-06-8
α-picoline

B: 2294-74-8
1-phenyl-2-pyridin-2-yl-ethanol

Conditions

Conditions	Yield
With dipotassium hydrogenphosphate; silver nitrate; zinc In water at 30℃; for 1h;	A 51% B 66%

...Expand

: 586-98-1
2-Hydroxymethylpyridine

: 109-06-8
α-picoline

Conditions

Conditions	Yield
With [IrCl(CO)(PPh3)2]; hydrazine hydrate; potassium hydroxide In methanol at 160℃; for 3h; Wolff-Kishner Reduction; Sealed tube;	62%
With [IrCl(CO)(PPh3)2]; hydrazine hydrate; potassium hydroxide In methanol at 160℃; for 3h; Sealed tube;	62%
With hydrazine hydrate; C23H40MnNO2P2; potassium tert-butylate In tert-butyl alcohol at 115℃; for 48h; Wolff-Kishner Reduction; Green chemistry;	26%

: 75-07-0
acetaldehyde

A: 110-86-1
pyridine

B: 109-06-8
α-picoline

C: 108-89-4
picoline

Conditions

Conditions	Yield
With ammonia; Pb(5.3percent)/borotitano silicate at 420℃; for 1h; Product distribution / selectivity; Molecular sieve;	A 2.4% B 61.3% C 21.6%
With ammonia; Pb/SnS-1B at 395℃; Product distribution / selectivity;	A 1% B 53.4% C 22.3%
With ammonia; titanium-silicate catalyst (sample C) at 250 - 400℃; Conversion of starting material;	A 0.88% B 53.44% C 20.55%

...Expand

: 50-00-0
formaldehyd

: 75-07-0
acetaldehyde

A: 110-86-1
pyridine

B: 109-06-8
α-picoline

C: 108-89-4
picoline

D: 108-99-6
3-Methylpyridine

Conditions

Conditions	Yield
With Pb-ZSM-5 zeolite; ammonia In gas	A 60% B 7% C 4% D 8%
With Co-ZSM-5 zeolite; ammonia In gas	A 57% B 6% C 8% D 7%
With Ag-ZSM-5 zeolite; ammonia In gas	A 42% B 3% C 6% D 11%
With pentasil zeolite H-ZSM-5; ammonia In gas at 450℃; Product distribution; synthesis of pyridine bases over ion-exchanged pentasil zeolite; var. zeolites, var. Si/Al atomic ratio;	A 42% B 3% C 5% D 11%

...Expand

: 1452-77-3
pyridine-2-carboxylic acid amide

A: 109-06-8
α-picoline

B: 109-05-7, 3000-79-1
2-Methylpiperidin

Conditions

Conditions	Yield
With hydrogenchloride; samarium for 0.166667h; Ambient temperature;	A 13% B 60%

: 110-86-1
pyridine

: 74-88-4
methyl iodide

A: 109-06-8
α-picoline

B: 100-71-0
2-Ethylpyridine

Conditions

Conditions	Yield
With n-butyllithium; 2-(N,N-dimethylamino)ethanol 1.) hexane, -78 deg C, 1 h, 2.) THF, -78 deg C, 1 h;	A 60% B 16 % Chromat.

...Expand

: 67-64-1
acetone

: 74-86-2
acetylene

A: 109-06-8
α-picoline

B: 108-48-5
2,6-dimethylpyridine

C: 108-75-8
2,4,6-trimethyl-pyridine

D: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With ammonia; MG-4 at 375℃; under 760 Torr;	A 6.3% B 7.3% C 58.3% D 5.9%
With ammonia; MG-4 at 375℃; under 760 Torr; Product distribution; other catalysts;	A 6.3% B 7.3% C 58.3% D 5.9%
With ammonia; MG-4 at 350℃; under 760 Torr;	A 6.2% B 15.6% C 36.4% D 6.8%

...Expand

: α-pyridylmethylenetriphenylphosphorane

: 100-51-6
benzyl alcohol

A: 109-06-8
α-picoline

B: 538-49-8, 714-08-9, 1519-59-1
2-styrylpyridine

Conditions

Conditions	Yield
With potassium tert-butylate In tetrahydrofuran at 40℃; for 6h;	A 58% B 26%

...Expand

: 3678-63-5
4-chIoro-2-methylpyridine

: 73183-34-3
bis(pinacol)diborane

A: 109-06-8
α-picoline

B: 660867-80-1
2-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

Conditions

Conditions	Yield
With bis(1,3-dimesityl-1H-imidazol-2(3H)-ylidene)nickel(0); potassium methanolate In hexane at 25℃; for 6h; Inert atmosphere; Irradiation;	A 10 %Chromat. B 55%

...Expand

: 931-19-1
2-methylpyridine N-oxide

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

A: 109-06-8
α-picoline

B: C9H12N2OS

C: C9H12N2OS

Conditions

Conditions	Yield
In acetonitrile at 81℃; for 4h;	A 52% B 3% C 5%

...Expand

: {C6H6NCr(H2O)5}(2+)

A: 109-06-8
α-picoline

B: 2-{α-D1}-methylpyridine

Conditions

Conditions	Yield
With water-d2 In water-d2	A 50% B 50%
With D2O In water-d2

: 109-06-8
α-picoline

: 100-44-7
benzyl chloride

: 13686-87-8
1-benzyl-2-methylpyridinium chloride

Conditions

Conditions	Yield
In toluene at 110℃; for 19h;	100%
In acetone for 8h; Heating;	51%

: 109-06-8
α-picoline

: 931-19-1
2-methylpyridine N-oxide

Conditions

Conditions	Yield
With dihydrogen peroxide; Na12[WZn3(H2O)2(ZnW9O34)2] at 75℃; for 7h;	100%
With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; acetonitrile In tert-butyl alcohol at 20℃; for 18h; Green chemistry; chemoselective reaction;	99%
With dihydrogen peroxide In acetic acid at 70 - 75℃; for 24h; Oxidation;	98%

: 109-06-8
α-picoline

: 100-39-0
benzyl bromide

: 2654-66-2
1-Benzyl-6-methylpyridinium bromide

Conditions

Conditions	Yield
	100%
In acetone Reflux;	100%
In toluene for 14h; Inert atmosphere; Reflux;	72%

: 109-06-8
α-picoline

: 100-47-0
benzonitrile

: N-((E)-1-Phenyl-2-pyridin-2-yl-vinyl)-benzamide

Conditions

Conditions	Yield
With phenyllithium In diethyl ether for 2.5h; Heating;	100%

: 109-06-8
α-picoline

: 565-80-0
2,4-dimethylpentan-3-one

: 941279-81-8
2,4-dimethyl-3-(pyridin-2-ylmethyl)pentan-3-ol

Conditions

Conditions	Yield
Stage #1: α-picoline With tert.-butyl lithium In tetrahydrofuran; pentane at -30℃; Stage #2: 2,4-dimethylpentan-3-one In tetrahydrofuran; pentane at -30 - 20℃; Stage #3: With water In tetrahydrofuran; pentane	100%
Stage #1: α-picoline With n-butyllithium In tetrahydrofuran; hexane at -78 - -50℃; for 1h; Inert atmosphere; Stage #2: 2,4-dimethylpentan-3-one In tetrahydrofuran; hexane at -50℃; for 2h; Inert atmosphere;	91%
Stage #1: α-picoline With n-butyllithium In tetrahydrofuran; hexane at -78 - -50℃; for 1h; Inert atmosphere; Stage #2: 2,4-dimethylpentan-3-one In tetrahydrofuran; hexane at -50℃; for 2h; Inert atmosphere; Stage #3: With water In tetrahydrofuran; hexane Inert atmosphere;	90%

: 109-06-8
α-picoline

: 345298-30-8
di-μ-chloro-dichloro-bis[η5-(perfluorobutyl)tetramethylcyclopentadienyl]-dirhodium(III)

: 933802-63-2
dichloro-(perfluorohexyl)tetramethylcyclopentadienyl-(2-methylpyridine)-rhodium(III)

Conditions

Conditions	Yield
In chloroform (Ar); methylpyridine was added to soln. of Rh complex in CHCl3; mixt. was stirred for 2 h at room temp.; evapd.; dried (vac.);	100%

: 109-06-8
α-picoline

: 119-60-8
dicyclohexyl ketone

: 102658-00-4
1,1-dicyclohexyl-2-(pyridin-2-yl)ethanol

Conditions

Conditions	Yield
Stage #1: α-picoline With n-butyllithium In tetrahydrofuran; hexane at -78 - -20℃; Inert atmosphere; Stage #2: dicyclohexyl ketone In tetrahydrofuran; hexane at -20℃; Inert atmosphere; Stage #3: With water; ammonium chloride In tetrahydrofuran; hexane	100%

: 109-06-8
α-picoline

: 1765-40-8
(bromomethyl)pentafluorobenzene

: 1229616-85-6
N-(pentafluorobenzyl)-2-methylpyridinium bromide

Conditions

Conditions	Yield
In chloroform at 20℃; for 24h;	100%

: 109-06-8
α-picoline

: 83766-52-3
4-heptadecafluorooctylaniline

: N-(4-heptadecafluoroctylphenyl)-2-pyridinethiocarbamide

Conditions

Conditions	Yield
With sodiumsulfide nonahydrate; sulfur for 72h; Reflux;	100%

: 109-06-8
α-picoline

: 627-32-7
1-iodopropan-3-ol

: 1-(3-hydroxypropyl)-2-methylpyridin-1-ium iodide

Conditions

Conditions	Yield
In 1,4-dioxane at 101℃; for 16h; Inert atmosphere;	100%

: 109-06-8
α-picoline

: (pyridin-2-yl-methyl)potassium

Conditions

Conditions	Yield
Stage #1: α-picoline With potassium tert-butylate at -35℃; for 0.333333h; Stage #2: With n-butyllithium In hexane at -35 - 20℃; for 4h;	100%
With n-butyllithium; potassium tert-butylate In hexane at 20℃; for 1h; Schlenk technique; Glovebox;	63%

: 109-06-8
α-picoline

: μ2-chlorido[3-(2-(piperidinyl)pyrimidin-4-yl-5-ido)-1-mesityl-1Himidazolylidene]palladium(II) dimer

: chlorido[3-(2-(piperidinyl)pyrimidin-4-yl-5-ido)-1-mesityl-1H-imidazolylidene](2-methylpyridine)palladium(II)

Conditions

Conditions	Yield
for 0.0833333h; Reflux;	100%

: 109-99-9
tetrahydrofuran

: 109-06-8
α-picoline

: [IPr2*NN]Cu(η2-C6H6)

: [IPr2*NN]Cu(N-2-picoline)

Conditions

Conditions	Yield
at 20℃; for 0.166667h; Glovebox; Inert atmosphere;	100%

...Expand

: 109-06-8
α-picoline

: 589-15-1
1-bromomethyl-4-bromobenzene

: 1-(4-bromobenzyl)-2-methylpyridinium bromide

Conditions

Conditions	Yield
In acetonitrile at 20℃; for 24h;	100%

: 109-06-8
α-picoline

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 7496-82-4
2-(4-methoxyphenyl)-indolizine

Conditions

Conditions	Yield
Stage #1: α-picoline; 2-Bromo-4'-methoxyacetophenone In acetone for 1h; Heating; Stage #2: With potassium carbonate for 5h;	99%

: 109-06-8
α-picoline

: 15743-13-2
tetrachloro-cyclopent-4-ene-1,3-dione

: 2,2,4-Trichloro-5-hydroxy-cyclopent-4-ene-1,3-dione; compound with 2-methyl-pyridine

Conditions

Conditions	Yield
In formic acid at 100℃; Product distribution; CH3CO2H,CF3CO2H;	99%
With acetic acid Ambient temperature;	87.4%

: 109-06-8
α-picoline

: 105-36-2
ethyl bromoacetate

: 55814-02-3
1-(2-ethoxy-2-oxoethyl)-2-methylpyridin-1-ium bromide

Conditions

Conditions	Yield
In ethanol at 60 - 80℃; for 20h;	99%
In tetrahydrofuran at 80℃; for 12h; Inert atmosphere;	92%
for 16h; Reflux;	90%

: 109-06-8
α-picoline

: 26127-08-2
(1R,2S,5R)-1-(chloromethoxy)-2-isopropyl-5-methylcyclohexane

: 1-[(1R,2S,5R)-(-)-menthoxymethyl]-2-methylpyridinium chloride

Conditions

Conditions	Yield
In hexane at 20℃; Menschutkin quaternization;	99%

: 109-06-8
α-picoline

: 7466-50-4
phenanthrene-3-carbaldehyde

: 1-(3-phenanthryl)-2-pyridin-2-ylethanol

Conditions

Conditions	Yield
Stage #1: α-picoline With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -5℃; for 0.5h; Stage #2: phenanthrene-3-carbaldehyde In tetrahydrofuran; hexane at 20℃; for 0.5h; Further stages.;	99%

: 109-06-8
α-picoline

: 68558-86-1
thallium(I) pentafluorobenzoate

: 41575-66-0
(SP-4-3)-dichlorido(N,N-dimethyl-ethane-1,2-diamine)platinum(II)

: 363-72-4
Pentafluorobenzene

: 117533-75-2
b-chloro-c(N),d(N')-{N,N-dimethyl-N'-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato(1-)}-a-(2-methylpyridine)platinum(II)

B: 124-38-9
carbon dioxide

Conditions

Conditions	Yield
In further solvent(s) Heating under stirring (110-115°C, N2, 120 min, 2-methylpyridine).; Cooling, evapn. to dryness (vacuum), washed (ether, petrol), dried, extraction with acetone, filtn. of TlCl, evapn. to dryness, washed (cold ethanol), elem. anal.;	A 28% B 99%

...Expand

: 109-06-8
α-picoline

: Fe(octaphenyltetraazaporphinate)

: Fe(octaphenyltetraazaporphinate)(2-methylpyridine)2

Conditions

Conditions	Yield
In neat (no solvent) standing in vapor of amine (room temp., 2 days);	99%
In benzene addn. of amine to Fe-complex; distn. off of excess amine and solvent (after 24 h), drying (vac., room temp.);

: 109-06-8
α-picoline

: 202280-80-6, 1046824-89-8
trans-[Pd(AsPh3)2(3,5-dichlorotrifluorophenyl)2]

: 202280-69-1
cis-[Pd(2-picoline)2(3,5-dichlorotrifluorophenyl)2]

Conditions

Conditions	Yield
In dichloromethane excess of picoline, stirring for 30 min; evapn., washing (hexane), drying; elem. anal.;	99%

: 109-06-8
α-picoline

: trans-(C6F5)2Pd{As(C6H5)3}2

: 202280-73-7
cis-[Pd(2-picoline)2(C6F5)2]

Conditions

Conditions	Yield
In dichloromethane excess of picoline, stirring for 30 min; evapn., washing (hexane), drying; elem. anal.;	99%

: 109-06-8
α-picoline

: 185226-19-1, 70424-04-3
trans-chloromethylbis(dimethylsulfoxide)platinum(II)

: 185042-99-3
cis(C,N)-chloromethyl(dimethyl sulfoxide)(2-methylpyridine)platinum(II)

Conditions

Conditions	Yield
In dichloromethane stirring stoich. amts. for 30 min; addn. of pentane, pptn. on cooling, collection (filtration), washing (cold pentane), drying (vac.); elem. anal.;	99%

: 109-06-8
α-picoline

: 623-03-0
4-Cyanochlorobenzene

: 32315-10-9
bis(trichloromethyl) carbonate

: 1202924-71-7
3-(4-chlorophenyl)pyrido[1,2-c]pyrimidin-1-one

Conditions

Conditions	Yield
Stage #1: α-picoline With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -70℃; for 1h; Inert atmosphere; Stage #2: 4-Cyanochlorobenzene In tetrahydrofuran; hexane at -70 - 20℃; Inert atmosphere; Stage #3: bis(trichloromethyl) carbonate With triethylamine In tetrahydrofuran; hexane at 20℃; for 2h; Inert atmosphere;	99%

...Expand

: 109-06-8
α-picoline

: 35815-10-2
bis(allyl)calcium

: bis(pyridin-2-ylmethyl)calcium

Conditions

Conditions	Yield
at 20℃; for 504h; Inert atmosphere;	99%

: 109-06-8
α-picoline

: 111-66-0
oct-1-ene

: 2-methyl-6-(octan-2-yl)pyridine

Conditions

Conditions	Yield
With C50H63NO2Zr; trityl tetrakis(pentafluorophenyl)borate In chlorobenzene at 100℃; for 6h; Inert atmosphere; Glovebox;	99%
With tris(pentafluorophenyl)borate; C42H51N3PSc In chlorobenzene at 100℃; for 15h; Inert atmosphere; Schlenk technique; Glovebox;	82%
With C23H29N2Sc; triphenylcarbenium tetra(pentafluorophenyl)borate at 70℃; Schlenk technique; Inert atmosphere;

: 109-06-8
α-picoline

: 592-41-6
1-hexene

: 143814-41-9
6-methyl-2-(1-methylpentyl)pyridine

Conditions

Conditions	Yield
With C50H63NO2Zr; trityl tetrakis(pentafluorophenyl)borate In chlorobenzene at 100℃; for 6h; Inert atmosphere; Glovebox;	99%
With tris(pentafluorophenyl)borate; C42H51N3PSc In chlorobenzene at 100℃; for 15h; Inert atmosphere; Schlenk technique; Glovebox;	81%
With C23H29N2Sc; triphenylcarbenium tetra(pentafluorophenyl)borate at 70℃; Schlenk technique; Inert atmosphere;