As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:105-36-2
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inquiryProduct description: Product name Ethyl bromoacetate CAS number 105-36-2 Assay ≥99.5% Appearance Colorless transparent liquid Capacity 500mt/year Application Pharmaceutical/p
Cas:105-36-2
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inquiryhigh quality Appearance:Colorless liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Ethyl bromoacetate Molecular weight: 167.00238 Appearance: Melting point: -38°C Boiling point: 159°C Flash point: 47°C
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:105-36-2
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inquiryEthylbromoacetate 3-Bromo-1-propanol Basic information Product Name: 3-Bromo-1-propanol Synonyms: TRIMETHYLENE BROMOHYDRIN;3-BROMO-1-PROPANOL;3-HYDROXYPROPYL BROMIDE;1-Bromo-3-hydroxyp
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inquiryChemical Name: Hexanoyl chloride CAS No.:142-61-0 Molecular Formula:C6H11ClO Molecular weight: 134.6 Appearance: Clear to slightly yellow liquid Appearance:Colorless liquid Storage:Preserve in well-closed, light-resistant and airtight conta
Cas:105-36-2
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inquiryethyl bromoacetate CAS:105-36-2 Specification mp -38 °c bp 159 °c(lit.) density 1.506 g/ml at 25 °c(lit.) vapor pressure 2.6 mm hg ( 25 °c) refractive index n20/d 1.451(
Price, service, company and transport advantage : 1. best service, high quality and reasonable price 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's customers' r
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:105-36-2
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:105-36-2
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inquiryProduct name: Ethyl Bromoacetate CAS No.:105-36-2 Molecule Formula:C4H7BrO2 Molecule Weight:167.00 Purity: 99.0% Package: 200kg/drum Description:Colorless clear liquid Manufacture Standards:Enterprise Standard TEST
Cas:105-36-2
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:105-36-2
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inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:105-36-2
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Superior quality, moderate price & quick delivery. Appearance:Colorless or light yellow liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmac
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:105-36-2
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Cas:105-36-2
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:105-36-2
Min.Order:1 Kilogram
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Type:Trading Company
inquiryConditions | Yield |
---|---|
With bromine; phosphorus tribromide for 0.5h; Hell-Volhard-Zelinsky reaction; Heating; | 100% |
With phosphorus tribromide 1.) r.t., 5 min; reflux, 3 h, 2.) r.t., overnight; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With thionyl chloride In diethyl ether at 0 - 20℃; | 95% |
With sulfuric acid for 24h; Reflux; | 85% |
at 100℃; |
C10H25N3O2PS(1+)
ethyl bromoacetate
Conditions | Yield |
---|---|
With bromide In N,N-dimethyl-formamide | 95% |
Conditions | Yield |
---|---|
With 1-bromo-butane; [HB(3,5-(CF3)2Pz)3]Ag(THF) | 78% |
With chloroform; hydrogen bromide |
Conditions | Yield |
---|---|
With tetraethylammonium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dichloromethane at 20℃; for 0.166667h; regioselective reaction; | 65% |
Conditions | Yield |
---|---|
Stage #1: ethanol With triethylamine In dichloromethane at 0℃; for 0.166667h; Stage #2: 2-Bromoacetyl bromide In dichloromethane at 0 - 25℃; for 5h; | 42% |
diethyl 2-amino-6-[(hydroxycarbamoyl)-methyl]-azulene-1,3-dicarboxylate sodium
B
ethyl bromoacetate
Conditions | Yield |
---|---|
A 24% B n/a |
bromoacetic acid tert-butyl ester
(+)-(S)-isopropyl-p-toluenesulphinamide
A
ethyl bromoacetate
Conditions | Yield |
---|---|
With n-butyllithium Product distribution; 1.) THF, -30 deg C, 15 min, 2.) THF, 0 deg C, 5 h; further temperatures; further alkylating agents; regio and stereochemistry of alkylation; | A 3% B n/a |
Conditions | Yield |
---|---|
bei der Einwirkung von UV-Licht; |
Conditions | Yield |
---|---|
Photolysis; |
ethyl bromide
thiocyanato-acetic acid ethyl ester
A
ethyl isothiocyanate
B
ethyl bromoacetate
Conditions | Yield |
---|---|
at 120℃; |
diethyl ether
bromocyane
ethyl N,N-diethylglycinate
B
Diethylcyanamide
C
ethyl bromoacetate
Acetyl bromide
ethyl 2-ethoxyethanoate
A
ethyl bromide
B
acetoxy-acetic acid ethyl ester
C
ethyl acetate
D
ethyl bromoacetate
Conditions | Yield |
---|---|
at 190℃; |
Conditions | Yield |
---|---|
With ethanol |
ethanol
bromo-acetic acid-(1-bromo-ethyl ester)
A
diethyl acetal
B
ethyl bromide
C
ethyl bromoacetate
D
crotonaldehyde
ethanol
A
ethyl bromide
B
ethyl bromoacetate
C
Bromoacetaldehyde diethyl acetal
D
bromoacetaldehyde
1,1,2,2-tetrabromoethene
sodium ethanolate
A
3,4-dibromobut-3-en-2-ol
B
ethyl bromoacetate
Conditions | Yield |
---|---|
With phosphorus pentabromide | |
With phosphorus tribromide In dichloromethane for 0.5h; Cooling with ice; |
Conditions | Yield |
---|---|
With pyridine; bromine durch folgende Veresterung mit Aethanol in Gegenwart von konz. H2SO4 in siedendem Benzol; |
Conditions | Yield |
---|---|
at 130 - 135℃; |
Conditions | Yield |
---|---|
With phosphorus; bromine Abdestillieren des ueberschuessigen Broms und Giessen des Reaktionsprodukts in Alkohol; | |
With bromine; acetic anhydride at 100℃; und Behandlung des Reaktionsprodukts mit Alkohol auf dem Wasserbad; |
Conditions | Yield |
---|---|
With phosphorus; bromine bei der Einw. von absol. Aethanol auf das Reaktionsgemisch; |
diazoacetic acid ethyl ester
(E)-1-Bromo-2-butene
A
ethyl bromoacetate
B
Ethyl 2-bromo-3-methyl-4-pentenoate
Ethyl 2-(bromomethyl)-3-methylcyclopropanecarboxylate
Ethyl 2-(bromomethyl)-3-methylcyclopropanecarboxylate
Conditions | Yield |
---|---|
dirhodium tetraacetate at 4℃; Yield given. Yields of byproduct given; |
ethyl 2-(tributylstannyl)acetate
acetophenone
A
ethyl acetate
B
ethyl bromoacetate
C
α-bromoacetophenone
Conditions | Yield |
---|---|
With tributyltin iodide; bromine Product distribution; 1.) DMSO, 75 deg C, 36 h; | A 82 % Chromat. B 10 % Chromat. C 75 % Chromat. |
Conditions | Yield |
---|---|
In ethanol Further byproducts given. Yields of byproduct given; | A 7 % Spectr. B 20 % Spectr. C n/a D n/a |
diazoacetic acid ethyl ester
chloroform
hydrogen bromide
ethyl bromoacetate
Conditions | Yield |
---|---|
In benzene for 0.5h; Reflux; | 100% |
In toluene for 8h; | 92% |
In benzene for 0.5h; Alkylation; Heating; | 91% |
4-hydroxy-benzaldehyde
ethyl bromoacetate
ethyl 2-(4-formylphenoxy)acetate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 24h; Reflux; | 100% |
Stage #1: 4-hydroxy-benzaldehyde With potassium carbonate; sodium iodide In acetonitrile for 0.5h; Heating; Stage #2: ethyl bromoacetate In acetonitrile for 18h; Heating; | 98% |
With potassium carbonate In acetone at 20℃; for 2h; | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 14h; Reflux; Inert atmosphere; | 100% |
With potassium carbonate In acetone for 4h; Reflux; Inert atmosphere; | 98% |
With potassium carbonate In acetone for 14h; Reflux; | 96% |
ethyl bromoacetate
phenyl isopropyl ketone
(+/-)-Ethyl 3-hydroxy-4-methyl-3-phenylpentanoate
Conditions | Yield |
---|---|
With iodine; zinc In 1,4-dioxane for 0.583333h; Reformatsky reaction; ultrasound irradiation; | 100% |
86% | |
With zinc; benzene |
ethyl bromoacetate
triethyl phosphite
diethoxyphosphoryl-acetic acid ethyl ester
Conditions | Yield |
---|---|
at 60 - 80℃; for 0.5h; Arbusov reaction; | 100% |
at 150℃; for 3h; | 99% |
for 0.0333333h; Michaelis-Arbuzov reaction; microwave irradiation; | 98% |
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
In acetone |
ethyl bromoacetate
Cyclopropylamine
[(cyclopropyl)amino]acetic acid ethyl ester
Conditions | Yield |
---|---|
In ethanol for 1h; | 100% |
With triethylamine In diethyl ether at 20℃; | 100% |
In ethanol at 0 - 20℃; for 18h; | 99% |
Conditions | Yield |
---|---|
With sodium azide In water; acetone at 20℃; for 0.5h; | 100% |
With sodium azide In water; acetone at 20℃; for 24h; | 100% |
With sodium azide In water; acetone at 0 - 63℃; for 4h; | 100% |
Conditions | Yield |
---|---|
With silver nitrate In acetonitrile at 20℃; for 12h; | 100% |
With trinitromethane; silver(l) oxide In acetonitrile |
Conditions | Yield |
---|---|
With triphenyl phosphite; potassium carbonate; (BrBu2Te)2O In toluene at 80℃; for 42h; Wittig-type olefination; | 100% |
With lithium hydroxide; triphenylphosphine; lithium chloride In water Wittig reaction; Heating; | 99% |
With lithium hydroxide; triphenylphosphine; lithium chloride In water for 0.25h; Wittig reaction; Heating; | 97% |
Indole-3-carboxaldehyde
ethyl bromoacetate
(3-formylindol-1-yl)acetic acid ethyl ester
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 15 - 20℃; for 16.5h; | 100% |
Stage #1: Indole-3-carboxaldehyde With sodium hydride In N,N-dimethyl-formamide Stage #2: ethyl bromoacetate In N,N-dimethyl-formamide at 20℃; for 16h; | 100% |
With sodium hydride In DMF (N,N-dimethyl-formamide) at 15 - 20℃; for 16.5h; | 100% |
Conditions | Yield |
---|---|
Stage #1: indole-2,3-dione With calcium hydride In N,N-dimethyl-formamide at 100℃; for 1h; Stage #2: ethyl bromoacetate In N,N-dimethyl-formamide at 100℃; for 4h; | 100% |
Stage #1: indole-2,3-dione With aluminum oxide; potassium fluoride In acetonitrile for 0.0833333h; Stage #2: ethyl bromoacetate In acetonitrile for 21h; Reflux; | 97% |
With KF-Celite In 2-methyltetrahydrofuran for 4h; Reflux; chemoselective reaction; | 93% |
4-chlorobenzaldehyde
ethyl bromoacetate
ethyl (E)-3-(4-chlorophenyl)prop-2-enoate
Conditions | Yield |
---|---|
With triphenyl phosphite; poly(ethylene glycol) di(2-(n-butyltelluro)ethyl) ether; potassium carbonate In toluene at 80℃; | 100% |
Stage #1: ethyl bromoacetate With triphenyl phosphite; PEG-Te-Bu In toluene at 80℃; for 0.166667h; Stage #2: With potassium carbonate In toluene for 0.0166667h; Stage #3: 4-chlorobenzaldehyde In toluene for 7h; Wittig-type olefination; Further stages.; | 98% |
With N1,N3,N5-tris(4-(diphenylarsino)phenyl)benzene-1,3,5-tricarboxamide; potassium carbonate In neat (no solvent) at 80℃; for 0.5h; Wittig Olefination; stereoselective reaction; | 96% |
4-nitrobenzaldehdye
ethyl bromoacetate
ethyl (E)-3-(4-nitrophenyl)-2-propenoate
Conditions | Yield |
---|---|
With polyethyleneimine supported triphenylphosphine In chloroform at 65℃; Wittig Olefination; Inert atmosphere; | 100% |
With Rasta resin-PPh3-NBniPr2 In dichloromethane at 20℃; for 19h; Wittig reaction; Molecular sieve; optical yield given as %de; | 99% |
With triphenylphosphine; nanocrystalline aerogel prepared MgO In N,N-dimethyl-formamide at 20℃; for 3h; Wittig reaction; | 98% |
ethyl 3-oxo-3-phenylpropionate
ethyl bromoacetate
diethyl 2-benzoylsuccinate
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol cooling; | 100% |
With potassium carbonate; sodium iodide at 65℃; for 2h; | 63% |
With sodium hydride 1.) THF, RT, 2.) THF, RT, 1 h; Yield given. Multistep reaction; | |
With potassium carbonate In acetone for 20h; Reflux; |
Conditions | Yield |
---|---|
With triphenyl phosphite; potassium carbonate; (BrBu2Te)2O In toluene at 80℃; for 36h; Wittig-type olefination; | 100% |
Stage #1: ethyl bromoacetate With triphenyl phosphite; PEG-Te-Bu In toluene at 80℃; for 0.166667h; Stage #2: With potassium carbonate In toluene for 0.0166667h; Stage #3: benzaldehyde In toluene for 18h; Further stages.; | 98% |
With triphenyl phosphite; poly(ethylene glycol) di(2-(n-butyltelluro)ethyl) ether; potassium carbonate In toluene at 80℃; | 98% |
benzene-1,2-diol
ethyl bromoacetate
ethyl 2-<2-<(ethoxycarbonyl)methoxy>phenoxy>acetate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 120h; | 100% |
With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In acetonitrile for 8h; Heating; | 95% |
With potassium carbonate In N,N-dimethyl-formamide at 75 - 80℃; for 1.5h; | 90% |
4-methoxy-aniline
ethyl bromoacetate
diethyl 2,2’-((4-methoxyphenyl)azanediyl)diacetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 60℃; for 16h; | 100% |
With N-ethyl-N,N-diisopropylamine In acetonitrile at 60℃; for 18h; | 100% |
With N-ethyl-N,N-diisopropylamine In acetonitrile at 60℃; for 16h; | 100% |
5,11,17,23-tetra-t-butyl-25,26,27,28-tetrahydroxycalix-4-arene
ethyl bromoacetate
5,11,17,23-tetra-tert-butyl-[25,26,27,28-(ethylethanoate)oxy]-calix[4]arene
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 70℃; for 3h; | 100% |
With caesium carbonate In acetone at 56℃; for 1h; | 100% |
With potassium carbonate In acetone for 120h; Heating; | 88% |
p-(tert-butyl)hexahomotrioxacalix[3]arene
ethyl bromoacetate
7,15,23-tri-tert-butyl-25,26,27-tris(ethoxycarbonylmethoxy)-2,3,10,11,18,19-hexahomo-3,11,19-trioxacalix[3]arene
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 56℃; for 6h; | 100% |
With sodium hydride In tetrahydrofuran at 67℃; distribution of cone and partial-cone conformers; other bases, solvents, temperatures and reaction times; | |
With potassium carbonate In acetone for 12h; Heating; |
1-methyl-4-(2-hydroxy-3-methoxyphenyl)-3-(3-oxo-3-ethoxypropyl)pyridinuim iodide
ethyl bromoacetate
4-<2-(2-ethoxy-2-oxoethoxy)3-3-methoxyphenyl>-1-methyl-3-(3-oxo-3-ethoxypropyl)pyridinium iodide
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 1h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 1h; |
Conditions | Yield |
---|---|
With pyridine In ethanol for 2h; Ambient temperature; | 100% |
With triethylamine In tetrahydrofuran at 20℃; for 4h; | 99% |
With 1-pentyl-3-methylimidazolium bromide at 25 - 30℃; for 0.166667h; | 98% |
ethyl bromoacetate
2-Mercaptobenzothiazole
ethyl 2-(benzo[d]thiazol-2-ylthio)acetate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere; | 100% |
With potassium carbonate In acetone for 3h; Heating; | 95% |
With potassium carbonate In acetonitrile at 20℃; for 3h; Inert atmosphere; | 74% |
ethyl bromoacetate
(1aS,3aS,4R,8aR)-1a,4-Dimethyl-octahydro-1-oxa-cyclopropa[c]azulen-8-one
((1aR,3aR,4S,7R,8aS)-1a,4-Dimethyl-8-oxo-octahydro-1-oxa-cyclopropa[c]azulen-7-yl)-acetic acid ethyl ester
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diisopropylamine In tetrahydrofuran | 100% |
ethyl bromoacetate
2-((isopropylamino)methylene)malononitrile
3-amino-4-cyan-1-(2-propyl)-pyrrol-2-carbonsaeureethylester
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100℃; for 5h; | 100% |
With sodium ethanolate; potassium carbonate 1.) DMF, 80 deg C, 30 min, 2.) DMF, ethanol, 60 deg C, 30 min; Yield given. Multistep reaction; |
ethyl bromoacetate
triphenylphosphine
(carbethoxymethyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In xylene for 0.00833333h; Heating; microwave irradiation; | 100% |
In ethyl acetate Reflux; | 100% |
In benzene at 20℃; | 100% |
ethyl bromoacetate
Diethyl methylmalonate
triethyl propane-1,2,2-tricarboxylate
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 2h; Ambient temperature; | 100% |
ethyl bromoacetate
2-<(4'-hydroxyphenyl)methyl>-3-methyl-4-acetoxy-5-propyl-7-chlorobenzofuran
2-<<4'-(carbethoxymethoxy)phenyl>methyl>-3-methyl-4-acetoxy-5-propyl-7-chlorobenzofuran
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 0.5h; Heating; | 100% |
With potassium carbonate In hexane; acetone |
ethyl bromoacetate
3,5-dihydroxybenzoic acid benzyl ester
benzyl 3,5-bis(ethoxycarbonylmethoxy)benzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 4.5h; Heating; | 100% |
ethyl bromoacetate
tert-butyl ((trans)-7-methyl-2-oxoazepan-3-yl)carbamate
((3S,7S)-3-tert-Butoxycarbonylamino-7-methyl-2-oxo-azepan-1-yl)-acetic acid ethyl ester
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran for 0.5h; Ambient temperature; | 100% |
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