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Cas:2678-54-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Cas:2678-54-8
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
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Min.Order:5 Kiloliter
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Type:Manufacturers
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1,1-diethoxyethylene CAS:2678-54-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:10 Kilogram
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inquiryAppearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
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Min.Order:100 Metric Ton
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inquiryProName: KETENEDIETHYLACETAL CasNo: 2678-54-8 Appearance: detailed see specifications Application: An important raw material and intermed... DeliveryTime: prompt PackAge: according to the clients requirement Port: Shanghai ProductionCapacity
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Min.Order:1 Gram
FOB Price: $6.0 / 9.0
Type:Trading Company
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Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:2678-54-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Metric Ton
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Type:Trading Company
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Cas:2678-54-8
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Min.Order:0
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Type:Lab/Research institutions
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Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 130 - 140℃; under 100 Torr; | 92% |
With potassium tert-butylate for 0.1 - 0.183333h; Cooling with ice; | 72% |
With potassium tert-butylate at 20℃; Reflux; Inert atmosphere; | 69.9% |
ketene diethyl acetal
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium tert-butylate In tetrahydrofuran at 0℃; for 2h; Elimination; | 70% |
β-(1,1-diethoxy-ethoxy)-chalcone
A
ketene diethyl acetal
B
1,3-diphenylpropanedione
Conditions | Yield |
---|---|
at 140℃; under 38 Torr; |
Conditions | Yield |
---|---|
With aluminium tert-butyl oleate at 180℃; |
potassium tert-butylate
1,1-diethoxy-2-iodoethane
ketene diethyl acetal
1,1-diethoxy-2-iodoethane
ketene diethyl acetal
Conditions | Yield |
---|---|
With potassium tert-butylate | |
With potassium tert-butylate |
ketene diethyl acetal
Conditions | Yield |
---|---|
With sodium methylate for 0.666667h; Ambient temperature; Yield given; |
ketene diethyl acetal
Conditions | Yield |
---|---|
With sodium; benzene |
tert-Amyl alcohol
tert-butyl methyl ether
ethylene glycol
chloroacetaldehyde diethyl acetal
ketene diethyl acetal
Conditions | Yield |
---|---|
With potassium hydroxide In Dimethyl ether |
tert-Amyl alcohol
ethylene glycol
chloroacetaldehyde diethyl acetal
ketene diethyl acetal
Conditions | Yield |
---|---|
With potassium hydroxide In Dimethyl ether; tert-butyl methyl ether |
N-propylsulfonylchloralimine
ketene diethyl acetal
Conditions | Yield |
---|---|
In dichloromethane Ambient temperature; | 100% |
ketene diethyl acetal
Conditions | Yield |
---|---|
dirhodium tetraacetate In dichloromethane at 20℃; for 2h; | 100% |
ketene diethyl acetal
(2-ethynylcyclohex-1-en-1-yl)(phenyl)methanone
Conditions | Yield |
---|---|
chromium(0) hexacarbonyl In tetrahydrofuran at 20℃; for 2h; | 99% |
With pentacarbonyl(tetrahydrofuran)chromium(0) In tetrahydrofuran at 20℃; for 2h; | 99% |
ketene diethyl acetal
methyl 6-ethoxynicotinate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 60℃; for 0.5h; Diels-Alder reaction; Inert atmosphere; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With (2,4,5-trifluorophenyl)boronic acid In tert-butyl methyl ether at 50℃; for 14h; | 98% |
4-methyl-benzaldehyde
ketene diethyl acetal
ethyl (E)-3-(4-methylphenyl)acrylate
Conditions | Yield |
---|---|
With (2,4,5-trifluorophenyl)boronic acid In tert-butyl methyl ether at 50℃; for 14h; | 97% |
ketene diethyl acetal
4-bromo-benzaldehyde
ethyl (E)-3-(4-bromophenyl)-2-propenoate
Conditions | Yield |
---|---|
With (2,4,5-trifluorophenyl)boronic acid In tert-butyl methyl ether at 50℃; for 14h; | 97% |
(S)-5-methoxycarbonylmethyl-6,6-dimethyl-2-cyclohexen-1-one
ketene diethyl acetal
4-carbomethoxymethyl-7,7-diethoxy-3,3-dimethylbicyclo<4.2.0>octan-2-one
Conditions | Yield |
---|---|
for 3h; Ambient temperature; Irradiation; | 96% |
ketene diethyl acetal
Hexafluoroacetone
4,4-diethoxy-1,1,1-trifluoro-2-trifluoromethyl-but-3-en-2-ol
Conditions | Yield |
---|---|
In methanol at 20℃; | 95% |
ketene diethyl acetal
6-[(benzyloxycarbonyl)amino]-3-(methylthio)-1,2,4,5-tetrazine
Conditions | Yield |
---|---|
In 1,4-dioxane at 100℃; for 2h; Diels-Alder reaction; | 95% |
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 24h; Diels-Alder reaction; regioselective reaction; | 95% |
Conditions | Yield |
---|---|
In toluene at 150℃; for 17h; Diels-Alder Cycloaddition; Inert atmosphere; regioselective reaction; | 95% |
1,1,3-trichloro-1,3,3-trifluoroacetone
ketene diethyl acetal
1,1-Diethoxy-4,4-difluoro-4-chloro-3-fluorodichloromethyl-1-buten-3-ol
Conditions | Yield |
---|---|
for 18h; Ambient temperature; | 94% |
ketene diethyl acetal
4-methoxy-benzaldehyde
ethyl (E)-3-(4-methoxyphenyl)prop-2-enoate
Conditions | Yield |
---|---|
With (2,4,5-trifluorophenyl)boronic acid In tert-butyl methyl ether at 50℃; for 14h; | 94% |
1-naphthaldehyde
ketene diethyl acetal
(E)-ethyl 3-(naphthalen-1-yl)acrylate
Conditions | Yield |
---|---|
With (2,4,5-trifluorophenyl)boronic acid In tert-butyl methyl ether at 50℃; for 14h; | 93% |
1-(2-diazo-1,3-dioxobutyl)-2-pyrrolidinone
ketene diethyl acetal
Conditions | Yield |
---|---|
dirhodium tetraacetate In benzene for 2h; Heating; | 92% |
5-(4-chlorophenyl)-2,3-dihydrofuran-2,3-dione
ketene diethyl acetal
[5-(4-Chloro-phenyl)-2-hydroxy-3-oxo-2,3-dihydro-furan-2-yl]-acetic acid ethyl ester
Conditions | Yield |
---|---|
In dichloromethane at 40℃; for 1h; | 91% |
ketene diethyl acetal
Conditions | Yield |
---|---|
In toluene for 1.5h; Heating; | 91% |
ketene diethyl acetal
5-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-2-cyclohexen-1-one
4-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-7,7-diethoxybicyclo<4.2.0>octane-2-one
Conditions | Yield |
---|---|
In benzene for 3.5h; Irradiation; | 90% |
ketene diethyl acetal
diethyl Fumarate
trans-3,3-diethoxy-1,2-cyclobutanedicarboxylic acid diethyl ester
Conditions | Yield |
---|---|
With diisobutylaluminum chloride; N-ethyl-N,N-diisopropylamine In toluene at -40℃; | 90% |
In tert-butyl alcohol at 84℃; for 72h; | 54% |
In tert-butyl alcohol at 84℃; for 72h; | 53% |
Stage #1: ketene diethyl acetal With diethylaluminium chloride In toluene at -45℃; for 0.166667h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In toluene at -45℃; for 0.166667h; Inert atmosphere; Stage #3: diethyl Fumarate In toluene at -45℃; for 3h; Inert atmosphere; | 42.3% |
ketene diethyl acetal
5-(4-bromo-phenyl)-furan-2,3-dione
[5-(4-Bromo-phenyl)-2-hydroxy-3-oxo-2,3-dihydro-furan-2-yl]-acetic acid ethyl ester
Conditions | Yield |
---|---|
In dichloromethane at 40℃; for 1h; | 90% |
N-[(4-methylbenzene-1-sulfonyl)(phenyl)methyl]formamide
ketene diethyl acetal
3-formylamino-3-phenyl-propionic acid ethyl ester
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane for 24h; Heating; | 90% |
With caesium carbonate In dichloromethane for 24h; Product distribution / selectivity; Heating / reflux; | 90% |
With triethylamine In dichloromethane for 24h; Product distribution / selectivity; Heating / reflux; | 80% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 24h; Product distribution / selectivity; Heating / reflux; | 48% |
ethyl acetoacetate
ketene diethyl acetal
Ethyl 2-acetyl-3-ethoxybut-2-enoate
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 22 - 90℃; for 8.5h; | 89% |
5-chloro-2,2-dimethyl-1,3-dioxin-4-one
ketene diethyl acetal
5-chloro-2,2-diethoxy-2,3-dihydropyran-4-one
Conditions | Yield |
---|---|
In toluene for 0.666667h; Product distribution / selectivity; Heating / reflux; | 89% |
ketene diethyl acetal
cyclohexanecarbaldehyde
(E)-3-cyclohexyl-acrylic acid ethyl ester
Conditions | Yield |
---|---|
With (2,4,5-trifluorophenyl)boronic acid In tert-butyl methyl ether at 50℃; for 14h; | 89% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In cyclohexane at 20℃; for 0.0833333h; Inert atmosphere; | 89% |
nitropentafluoroacetone
ketene diethyl acetal
4,4-diethoxy-1,1-difluoro-1-nitro-2-trifluoromethyl-but-3-en-2-ol
Conditions | Yield |
---|---|
at -30°C, then at 20°C 2 h; | 88% |
at -30°C, then at 20°C 2 h; | 88% |
ketene diethyl acetal
Conditions | Yield |
---|---|
In acetonitrile at 20 - 50℃; for 19h; Cycloaddition; | 87% |
3-bromo-1-trifluoromethylbenzene
ketene diethyl acetal
1,1-diethoxy-6-(trifluoromethyl)benzocyclobutene
Conditions | Yield |
---|---|
With sodium amide In tetrahydrofuran for 22h; Heating; | 87% |
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