As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
Cas:66-77-3
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inquiryThe company is committed to research, develop, produce and sale fine chemicals and pharmaceutical intermediates. The company is the leading producer of 1-Chloromethyl Naphthalene in China,The company has a professional production, strict quality mana
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:66-77-3
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inquirySpecifications 1. 66-77-3 2. Assay: 99% min 3. Pharmaceutical intermediate 4. 1-Naphthaldehyde 5. High Quality 1-Naphthaldehyde Synonyms 1-Naphthaldehyde (alpha);
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1-Naphthaldehyde CAS 66-77-3 1-Naphthalenecarboxaldehyde CAS no 66-77-3 Naphthalene-1-carbaldehyde alpha-Naphthylaldehyde 1-Naphthaldehyde Manufacturer High quality Best price In stock factory CAS 66-77-3 1-Naphthaldehyde COA TDS price MSDS
Cas:66-77-3
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inquiryProduct Name: 1-Naphthaldehyde Synonyms: alpha-Naphthal;alpha-Naphthylaldehyde;alpha-Naphthylcarboxaldehyde;-Naphthaldehdye;naphthalene-1-carbaldehyde;Naphthalene-1-carboxaldehyde;ALPHA-NAPHTHALDEHYDE;AKOS BBS-00003152 CAS: 66-77
Cas:66-77-3
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:66-77-3
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:66-77-3
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inquiryProduct name 1-Naphthaldehyde Product category Naphthalene series CAS NO. 66-77-3 Structural formula Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg
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Cas:66-77-3
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Cas:66-77-3
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inquiryBeluga chemical professional supply High-quality naphthal CAS 66-77-3 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in China and expor
Cas:66-77-3
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:66-77-3
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:66-77-3
Min.Order:10 Gram
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inquiry66-77-3Appearance:white powder Storage:keep cold Package:according to customers' requirements Application:Pharmaceutical intermediates 66-77-3 Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or according to
moderate price & quick delivery. Appearance:Yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used as Pharmaceutical Intermediate
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:66-77-3
Min.Order:1 Kilogram
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inquiryProduct name: 1-Naphthalenecarboxaldehyde CAS No.: 66-77-3 Molecule Formula:C11H8O Molecule Weight:156.18 Purity: 98.0% Package: 200kg/drum Description:Light yellow liquid Manufacture Standards:Enterprise Standard
Cas:66-77-3
Min.Order:1 Kilogram
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
1-Naphthaldehyde Basic information Applications Appearance Dangerous Goods Info Product Name: 1-Naphthaldehyde Synonyms: alpha-Naphthal;alpha-Naphthylaldehyde;alpha-Naphthylcarboxaldehyde;-Naphthaldehdye;naphthalene-1-carbaldehyde;Naphthalene-
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:66-77-3
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Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Conditions | Yield |
---|---|
With oxygen; perruthenate modified mesoporous silicate MCM-41 In toluene at 80℃; for 1h; Oxidation; | 100% |
With C23H35N3O3(1+)*Br(1-); copper In chlorobenzene at 80℃; for 15h; | 99% |
With 1-hydroxy-1H-1,2,3-benziodoxathiole 1,3,3-trioxide; Oxone; cetyltrimethylammonim bromide In water at 20℃; for 2h; Green chemistry; chemoselective reaction; | 99% |
2,2-dimethyl-5-(naphthalen-1-ylmethylene)-1,3-dioxane-4,6-dione
1-naphthaldehyde
Conditions | Yield |
---|---|
With copper(II) acetate dihydrate; manganese(III) triacetate dihydrate In acetic acid at 50℃; for 24h; Inert atmosphere; | 100% |
diacetoxy(1-naphthyl)methane
1-naphthaldehyde
Conditions | Yield |
---|---|
With bismuth(III) chloride In chloroform for 0.333333h; deprotection; Heating; | 99% |
With tin(ll) chloride In acetonitrile at 25℃; for 0.0333333h; Hydrolysis; | 99% |
With H6P2W18O62 In toluene at 100℃; for 0.0833333h; | 99% |
Conditions | Yield |
---|---|
With 1-dodecyl-3-methylimidazolium iron chloride; periodic acid at 30℃; for 1.5h; | 97% |
With 4-methylmorpholine N-oxide; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride; potassium iodide at 100℃; for 0.0333333h; Microwave irradiation; Ionic liquid; | 91% |
With sodium nitrate; acetic acid In water for 3h; Reflux; | 87% |
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) In benzene for 0.166667h; Ambient temperature; | 97% |
With tri-n-butyl-tin hydride In 1-methyl-pyrrolidin-2-one at 20℃; Inert atmosphere; | 90% |
With polymethylhydrosiloxane; trifuran-2-yl-phosphane; tetrabutyl ammonium fluoride; potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) In tetrahydrofuran; water at 20℃; for 1h; | 86% |
1-naphtylaldehyde oxime
1-naphthaldehyde
Conditions | Yield |
---|---|
With molybdenum(V) chloride; zinc In acetonitrile at 20℃; for 0.116667h; | 97% |
With ammonium peroxydisulfate; Montmorillonite K10; silver nitrate In hexane at 50℃; for 2.5h; | 95% |
With iodine In acetonitrile for 4h; deoximation; Heating; | 93% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In ethanol for 4h; Reflux; Green chemistry; | 96% |
With sodium periodate In dichloromethane at 40 - 50℃; Ionic liquid; | 82% |
With sodium periodate In N,N-dimethyl-formamide at 150℃; for 0.583333h; | 80% |
2-(naphth-1-yl)-1,3-dioxolane
1-naphthaldehyde
Conditions | Yield |
---|---|
With lithium tetrafluoroborate In acetonitrile for 48h; Ambient temperature; | 96% |
With ammonium cerium(IV) nitrate In methanol; water at 20℃; for 0.166667h; Ring cleavage; | 95% |
With polyaniline-sulfate salt; water for 2h; Heating; | 90% |
With sodium tetrahydroborate; nickel(II) chloride hexahydrate In methanol for 3h; Reflux; chemoselective reaction; | 86% |
With Pyrene-1-carboxylic acid; C33H22NO4(1-)*Na(1+) In dimethylsulfoxide-d6; water-d2 at 85℃; for 6h; Reagent/catalyst; | 23 %Spectr. |
Conditions | Yield |
---|---|
With Bis(N-methylpiperazinyl) aluminum hydride In tetrahydrofuran for 24h; Heating; | 95% |
With 9-borabicyclo[3.3.1]nonane dimer; lithium dihydrido borata-bicyclo[3.3.0]nonane In tetrahydrofuran for 6h; Ambient temperature; | 80% |
With 9-borabicyclo[3.3.1]nonane dimer; tert.-butyl lithium 1.) THF, room temp.; 2.) THF, pentane, -20 deg C, 10 min and room temp., 6 h; Yield given. Multistep reaction; | |
With ThxBHO-s-Bu In tetrahydrofuran at 25℃; for 96h; Yield given; | |
Multi-step reaction with 2 steps 1.1: thionyl chloride / N,N-dimethyl-formamide; dichloromethane / 4 h / Reflux 1.2: 12 h / 20 °C 2.1: sodium hydride; sodium iodide / mineral oil; tetrahydrofuran / 85 °C / Inert atmosphere; Sealed tube View Scheme |
acetic acid
1-Methylnaphthalene
A
naphthalen-1-ylmethyl acetate
B
1-naphthaldehyde
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In water at 85℃; for 2h; | A 3% B 95% |
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In water; acetic acid at 85℃; for 2h; | A 3% B 95% |
With *5H2O; lithium chloride In acetic acid at 100℃; for 27h; | A 35% B 39% |
1-[bis(N,N-diethyldithiocarbamato)methyl]naphthalene
1-naphthaldehyde
Conditions | Yield |
---|---|
With nitric acid In water at 20℃; | 95% |
Conditions | Yield |
---|---|
In diethyl ether for 0.25h; Ambient temperature; | 94% |
Conditions | Yield |
---|---|
With sodium hydride; sodium iodide In tetrahydrofuran at 40℃; chemoselective reaction; | 93% |
With sodium hydride; sodium iodide In tetrahydrofuran; mineral oil at 85℃; Inert atmosphere; Sealed tube; | 88% |
With lithium diethoxyaluminum hydride |
Conditions | Yield |
---|---|
With 1H-imidazole; sodium periodate In water; acetonitrile at 20℃; for 30h; | 93% |
With 1H-imidazole; sodium periodate; [Mn(III)-salophen]Cl In water; acetonitrile at 20℃; for 0.25h; | 90% |
With 1H-imidazole; sodium periodate; {Mn(III)[5,10,15,20-tetrakis(4-H2N-Ph)porphyrin]}polystyrene In acetonitrile at 20℃; for 6h; | 89% |
1-(naphthalen-1-ylmethylene)-2-phenylhydrazine
1-naphthaldehyde
Conditions | Yield |
---|---|
With caro's acid; silica gel for 0.0416667h; Oxidation; Irradiation; | 93% |
dicobalt octacarbonyl
1-naphthyl triflate
1-naphthaldehyde
Conditions | Yield |
---|---|
With triethylsilane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium acetate In acetonitrile at 25℃; for 16h; Schlenk technique; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With carbon tetrabromide; oxygen In acetonitrile at 20℃; for 2h; Irradiation; Green chemistry; | 92% |
With nickel-doped graphene carbon nitride nanoparticles; air In ethanol at 25℃; for 8h; Irradiation; Green chemistry; | 89% |
With air; titanium(IV) oxide; silver sulfate In acetonitrile for 5h; Ambient temperature; Irradiation; | 26% |
Conditions | Yield |
---|---|
In diethyl ether for 0.5h; Ambient temperature; | 92% |
1-naphthaldehyde semicarbazone
1-naphthaldehyde
Conditions | Yield |
---|---|
With magnesium hydrogen sulfate; water; silica gel In hexane at 20℃; for 0.5h; | 92% |
With tetrachlorosilane; silica gel In hexane; water for 2h; Heating; | 92% |
With ammonium dichromate(VI); water; silica gel; zirconium(IV) chloride at 80℃; for 1.08333h; | 85% |
With potassium permanganate; silica gel In water at 20℃; for 0.25h; | 78% |
With sulfuric acid; silica gel In hexane for 0.166667h; |
Conditions | Yield |
---|---|
With copper(l) iodide; oxygen In dimethyl sulfoxide at 120℃; for 15h; Reagent/catalyst; Solvent; chemoselective reaction; | 92% |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / tetrahydrofuran; water / 20 °C 2: palladium dichloride; copper(l) chloride; oxygen / dimethyl sulfoxide / 10 h / 120 °C / 760.05 Torr View Scheme |
(naphtalen-1-yl)methyl iodide
1-naphthaldehyde
Conditions | Yield |
---|---|
With 1‑dodecyl‑3‑methylimidazolium iron chloride; periodic acid at 50℃; for 4h; Reagent/catalyst; Green chemistry; | 92% |
1-naphthaldehyde
Conditions | Yield |
---|---|
Stage #1: N-(1-naphthoyl)-4-methylbenzenesulfonohydrazide With 1H-imidazole; 1-(Trimethylsilyl)imidazole In toluene at 55℃; for 4.5h; Inert atmosphere; Stage #2: With citric acid In toluene at 23℃; for 2.5h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In dichloromethane at 0 - 20℃; for 0.333333h; Inert atmosphere; Green chemistry; | 91% |
With dihydrogen peroxide; vanadia In water at 50℃; for 12h; | 70% |
With water; indole-2,3-dione | |
With oxalic acid; dimethyl sulfoxide; O-phenyl phosphorodichloridate; triethylamine 1.) -10 deg C, 15 min, CH2Cl2, 2.) -10 deg C to 20 deg C, 45 min, 3.) 20 deg C, 30 min; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With C13H26B(1-)*K(1+) In tetrahydrofuran for 24h; Ambient temperature; | 91% |
With sodium hydride; zinc(II) chloride In tetrahydrofuran; mineral oil at 40℃; for 8h; Inert atmosphere; Sealed tube; | 82% |
With calcium bis(hypophosphite); calcium acetate; nickel(II) acetate tetrahydrate In ethanol; water at 100℃; for 21h; Sealed tube; | 80% |
2-(2-naphthalen-1-yl)-1,3-dithiolane
1-naphthaldehyde
Conditions | Yield |
---|---|
With iodosylbenzene In dichloromethane at 20℃; for 0.5h; | 90% |
With silica gel; ferric nitrate In hexane at 50℃; for 0.166667h; Yield given; | |
With indium (III) iodide; dihydrogen peroxide In water; toluene at 20℃; for 15h; Inert atmosphere; Sealed tube; | 108 mg |
Conditions | Yield |
---|---|
With hydrogenchloride; water at 20℃; for 1h; | 90% |
Conditions | Yield |
---|---|
With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.5h; | 90% |
With titanium(IV) isopropylate; 1,1,3,3-Tetramethyldisiloxane In methyl cyclohexane at 20℃; for 24h; Inert atmosphere; | 75% |
dicobalt octacarbonyl
1-Iodonaphthalene
1-naphthaldehyde
Conditions | Yield |
---|---|
With triethylsilane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium acetate In acetonitrile at 25℃; for 16h; Schlenk technique; Inert atmosphere; | 90% |
N-cyclohexyl-N-(1-naphthylmethyl)-4-nitrobenzenesulfinamide
1-naphthaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In o-xylene for 6h; Heating; | 89% |
Conditions | Yield |
---|---|
In chloroform Ambient temperature; | 100% |
In benzene Heating; | 74% |
In water at 20℃; for 2h; | 69% |
Conditions | Yield |
---|---|
With aluminum oxide Inert atmosphere; Neat (no solvent); | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane In water at 20℃; for 0.05h; Knoevenagel Condensation; Green chemistry; | 100% |
With polystyrene-supported DABCO In methanol at 25℃; for 0.8h; Knoevenagel Condensation; Green chemistry; | 99% |
1-naphthaldehyde
1-naphtylaldehyde oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium carbonate In ethanol at 20℃; | 100% |
With hydroxylamine hydrochloride; sodium carbonate In ethanol; water at 20℃; for 2h; | 99% |
With pyridine; hydroxylamine In ethanol | 99% |
Conditions | Yield |
---|---|
With methyltriphenylphosphonium tetrahydroborate In dichloromethane Reduction; | 100% |
With Zn(BH4)2(Ph3P)2 In tetrahydrofuran at 20℃; Reduction; | 100% |
With Zn(BH4)2(bpy) In acetonitrile at 20℃; for 0.133333h; | 99% |
diethylzinc
1-naphthaldehyde
(R)-1-(1-naphthyl)propanol
Conditions | Yield |
---|---|
(1R,2S)-(-)-1-phenyl-2-piperidinopropane-1-thiol In toluene at 0℃; for 12h; | 100% |
Stage #1: diethylzinc; 1-naphthaldehyde With diphenyl-((R)-1-((S)-1-phenylethyl)aziridin-2-yl)-methanol In hexane; toluene at 0 - 25℃; for 48.5h; Inert atmosphere; Stage #2: With ammonium chloride In hexane; water; toluene Saturated solution; optical yield given as %ee; enantioselective reaction; | 99% |
Stage #1: diethylzinc With (1R,3S)-1-benzyl-6,7-dimethoxy-3-[(5R)-4-methoxy-6-methyl-5,6,7,8-tetrahydro[1,3]dioxolo[4,5-g]isoquinolin-5-yl]-1,3-dihydro-2-benzofuran-1-ol In hexane; toluene at 0℃; for 0.0833333h; Stage #2: 1-naphthaldehyde In hexane; toluene at 0℃; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; enantioselective reaction; | 99% |
1-naphthaldehyde
4-methoxy-aniline
(E)-4-methoxy-N-(naphthalene-1-ylmethylene)phenylamine
Conditions | Yield |
---|---|
In ethanol at 20℃; Inert atmosphere; | 100% |
In ethanol for 1h; Heating; | 96% |
In benzene Heating; | |
In benzene Heating; | |
In ethanol at 25℃; for 12h; |
1-naphthaldehyde
toluene-4-sulfonic acid hydrazide
(Z)-4-methyl-N'-(naphthalen-1-ylmethylene) benzenesulfonohydrazide
Conditions | Yield |
---|---|
In diethyl ether for 1h; Ambient temperature; | 100% |
In methanol | 85% |
In methanol at 60℃; |
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; hydroxylamine hydrochloride at 100℃; for 0.25h; Condensation; microwave irradiation; | 100% |
With oxygen; copper; ammonium chloride In pyridine at 60℃; for 24h; | 99% |
With hydroxylamine hydrochloride In 1-methyl-pyrrolidin-2-one for 0.0833333h; Heating; | 98% |
Conditions | Yield |
---|---|
Stage #1: Methyltriphenylphosphonium bromide With potassium tert-butylate In toluene at 0 - 20℃; for 4.5h; Stage #2: 1-naphthaldehyde In toluene at 0 - 20℃; | 100% |
Stage #1: Methyltriphenylphosphonium bromide With potassium tert-butylate In toluene at 0 - 20℃; for 4.5h; Stage #2: 1-naphthaldehyde In toluene at 0 - 20℃; | 100% |
Stage #1: Methyltriphenylphosphonium bromide With potassium tert-butylate In toluene at 0 - 20℃; for 4.5h; Stage #2: 1-naphthaldehyde In toluene at 0 - 20℃; | 100% |
1-naphthaldehyde
methylamine
(±)-(2S,3R)-ethyl 1,3-dimethyl-2-(naphthalen-1-yl)-4-oxoazetidine-3-carboxylate
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
In water for 1h; Ambient temperature; | |
In tetrahydrofuran; methanol |
1-naphthaldehyde
phosphonic acid diethyl ester
diethyl hydroxy(naphth-1-yl)methylphosphonate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine at 20℃; for 17h; | 100% |
With N-ethyl-N,N-diisopropylamine at 20℃; for 18h; | 100% |
With (2,6-iPr2PhNH)5SmLi2(THF)2 In hexane at 20℃; for 0.0833333h; Schlenk technique; Inert atmosphere; | 99% |
diethyl 1-cyanomethylphosphonate
1-naphthaldehyde
3-(1-naphthyl)acrylonitrile
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; Wadsworth-Emmons reaction; | 100% |
With potassium carbonate for 0.25h; Ambient temperature; |
Conditions | Yield |
---|---|
With hydrogenchloride; antimony In water for 16h; | 100% |
With tin(ll) chloride; zinc In water for 2h; | 99% |
With potassium fluoride; antimony In water for 16h; allylation; | 96% |
ethyl acetoacetate
1-naphthaldehyde
urea
6-methyl-4-naphthalen-1-yl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In ethanol at 100℃; for 1h; Biginelli reaction; Microwave irradiation; Inert atmosphere; | 100% |
With copper doped mesoporous silica MCM-41 supported dual acidic ionic liquid-HSO4 In ethanol at 80℃; for 1h; Biginelli Pyrimidone Synthesis; | 97% |
Stage #1: 1-naphthaldehyde; urea With hydrogenchloride In tetrahydrofuran; water at 67℃; for 1h; Biginelli Pyrimidone Synthesis; Green chemistry; Stage #2: ethyl acetoacetate With N,N′-(cyclohexane-1,2-diyl)bis(3,6-dichloropicolinamide) In tetrahydrofuran; water at 67℃; for 5h; Biginelli Pyrimidone Synthesis; Green chemistry; | 95% |
1-naphthaldehyde
trimethylsilylacetylene
1-(naphthalen-1-yl)-3-(trimethylsilyl)prop-2-yn-1-ol
Conditions | Yield |
---|---|
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: 1-naphthaldehyde In tetrahydrofuran; hexane at -78 - 20℃; for 3h; Inert atmosphere; | 100% |
Stage #1: trimethylsilylacetylene With n-butyllithium In diethyl ether; hexane at -78℃; for 0.5h; Stage #2: 1-naphthaldehyde In diethyl ether; hexane at -78 - -10℃; Further stages.; | 64% |
Stage #1: trimethylsilylacetylene With n-butyllithium In diethyl ether at -78℃; Stage #2: 1-naphthaldehyde In diethyl ether at -78 - -10℃; | 63% |
Conditions | Yield |
---|---|
With titanium(IV) isopropylate; (R,R)-1,1'-bis[N(1-ferrocenylethyl)-4-Me-benzenesulfonamide] In hexane; toluene at 20℃; for 48h; | 100% |
Conditions | Yield |
---|---|
With PPA; silica gel In 1,2-dichloro-ethane at 20℃; for 0.5h; | 100% |
Fe(CF3SO3)3 In acetonitrile at 20℃; for 0.25h; | 93% |
With eosin y In 1,4-dioxane at 20℃; for 12h; Irradiation; Inert atmosphere; Schlenk technique; | 91% |
With tantalum pentachloride In dichloromethane at 20℃; for 1.5h; | 87% |
With ammonium cerium(IV) nitrate In acetonitrile at 30℃; for 10h; | 85% |
1-naphthaldehyde
phenylacetylene
1-(1-naphthyl)-3-phenylprop-2-yn-1-ol
Conditions | Yield |
---|---|
Stage #1: phenylacetylene With n-butyllithium In hexanes; diethyl ether at 0℃; for 1h; Stage #2: 1-naphthaldehyde In hexanes; diethyl ether at 0 - 20℃; for 0.5h; | 100% |
Stage #1: phenylacetylene With titanium(IV) isopropylate; C16H15NO; dimethyl zinc(II) In tetrahydrofuran; toluene at 20℃; for 1.5h; Inert atmosphere; Stage #2: 1-naphthaldehyde In tetrahydrofuran; toluene at 0 - 20℃; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 96% |
With dimethyl zinc(II); (1R,2S)-cis-1-amino-2-indenol-derived oxazolidine In n-heptane; toluene at -4℃; for 48h; | 91% |
Conditions | Yield |
---|---|
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: 1-naphthaldehyde In dichloromethane at 20℃; for 1h; Inert atmosphere; | 100% |
With triphenylphosphine In dichloromethane at 0℃; for 2h; Inert atmosphere; | 88% |
With triphenylphosphine In dichloromethane at 0℃; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
Stage #1: 1H-indene-1,3(2H)-dione; 1-naphthaldehyde With L-proline In methanol at 20℃; for 0.5h; organocatalytic Knoevenagel condensation; Stage #2: (E)-benzalacetone In methanol at 25℃; for 96h; Diels-Alder/epimerization reaction; | 100% |
1-naphthaldehyde
(trifluoromethyl)trimethylsilane
Conditions | Yield |
---|---|
With potassium fluoride; (4R,4'R,5R,5'R)-α,α,α',α',α",α",α‴,α‴-octaphenyl-2,2'-(benzene-1,4-diyl)bis(1,3-dioxolane-4,5-dimethanol) In acetonitrile at 20℃; Inert atmosphere; | 100% |
With potassium fluoride; tetrabutylammomium bromide In toluene at 0℃; for 1h; | 99% |
With tri-tert-butyl phosphine In N,N-dimethyl-formamide at 20℃; | 95% |
1-naphthaldehyde
1-amino-2-propene
(E)-N-allyl-1-(naphthalen-1-yl)methanimine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 20h; | 100% |
With magnesium sulfate In dichloromethane for 24h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: hex-1-yne With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 1.33333h; Inert atmosphere; Stage #2: 1-naphthaldehyde In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; Stage #3: With water; ammonium chloride In tetrahydrofuran; hexane | 100% |
Stage #1: hex-1-yne With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: 1-naphthaldehyde In tetrahydrofuran; hexane at 0 - 20℃; for 0.583333h; Inert atmosphere; | 80% |
Stage #1: hex-1-yne With n-butyllithium In tetrahydrofuran at -78℃; for 0.333333h; Stage #2: 1-naphthaldehyde In tetrahydrofuran at -78 - 20℃; Further stages.; |
(4-nitro-1H-benzimidazol-2-yl)-piperidin-4-ylmethyl-amine
1-naphthaldehyde
(1-naphthalen-1-ylmethyl-piperidin-4-ylmethyl)-(4-nitro-1H-benzimidazol-2-yl)-amine
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In DMF (N,N-dimethyl-formamide); acetic acid at 20℃; | 100% |
Conditions | Yield |
---|---|
ytterbium(III) triflate In ethanol at 20℃; for 5h; | 100% |
With piperidine; acetic acid In benzene for 2.5h; Knoevenagel Condensation; Dean-Stark; Reflux; | 93% |
piperidine In methanol at 50 - 60℃; for 0.5 - 10h; Product distribution / selectivity; | 92.5% |
In methanol at 20℃; for 24h; Product distribution / selectivity; | |
With C112H128N32Pd4(12+) at 50℃; for 9h; |
Conditions | Yield |
---|---|
With ammonium acetate for 6h; Henry reaction; Reflux; | 100% |
With N-butylamine In ethanol | 97% |
With cyclohexylamine at 120℃; Microwave irradiation; | 55% |
With ammonium acetate In acetic acid | 8.5 g (33%) |
With ammonium acetate for 2h; Henry Nitro Aldol Condensation; Inert atmosphere; Reflux; |
2-thioxo-4-thiazolidinone
1-naphthaldehyde
(Z)-5-(naphthalen-1'-ylmethylene)-2-thioxothiazolidin-4-one
Conditions | Yield |
---|---|
With acetic acid; triethylamine In ethyl acetate at 85℃; for 3h; | 100% |
With sodium acetate; acetic acid for 16h; Reflux; | 82% |
With sodium acetate In acetic acid Reflux; | 76% |
With piperidine In ethanol at 70℃; for 16h; Knoevenagel Condensation; | 59% |
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
(R)-1-phenyl-ethyl-amine
1-naphthaldehyde
(R)-N-(naphthalen-1-ylmethylene)-1-phenylethanamine
Conditions | Yield |
---|---|
In toluene at 100℃; for 2h; Inert atmosphere; | 100% |
With magnesium sulfate In dichloromethane at 20℃; for 12h; |
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