Why choose us: The above product is Cuikang's strong item with best price, good quality and fast supply.Cuikang has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to provid
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:86-55-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:86-55-5
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:86-55-5
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:86-55-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:86-55-5
Min.Order:1 Kilogram
FOB Price: $15.0 / 50.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:86-55-5
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:86-55-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: 1-Naphthoic acid CAS: 86-55-5 MF: C11H8O2 MW: 172.18 EINECS: 201-681-9 Mol File: 86-55-5.mol 1-Naphthoic acid Structure 1-Naphthoic acid Chemical Properties Melting point 157-160 °C (lit.) Boiling point
1-Naphthoic acid CAS:86-55-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
Cas:86-55-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting 1-Naphthoic acid 98% CAS:86-55-5, Please contact us by email freely. We are leading exporter in China. If you really need this cargo
Cas:86-55-5
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
Cas:86-55-5
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:86-55-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:needle crystal Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used in organic
Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:86-55-5
Min.Order:0
Negotiable
Type:Trading Company
inquiryProduct name: 1-Naphthoic Acid CAS No.:86-55-5 Molecule Formula:C11H7O2 Molecule Weight:171.17 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING
Cas:86-55-5
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:86-55-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Conditions | Yield |
---|---|
Stage #1: 1,8-Naphthalic anhydride With sodium hydroxide In water at 100℃; for 0.0166667h; microwave irradiation; Stage #2: With mercury(II) diacetate In water at 200℃; for 0.25h; Pesci reaction; microwave irradiation; Stage #3: With hydrogenchloride In water at 120℃; for 0.25h; microwave irradiation; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide; cobalt(II) acetate In ethanol at 65℃; under 1520 Torr; for 4h; Irradiation; | 99.3% |
With sodium hydroxide; tetrabutylammomium bromide; dicobalt octacarbonyl In water; benzene at 65℃; under 760 Torr; for 5h; Irradiation; | 96% |
With tetrabutylammomium bromide; dicobalt octacarbonyl In sodium hydroxide; benzene at 65℃; for 4.5h; Irradiation; | 95% |
With tributyl-amine; water; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride at 110 - 130℃; under 3 Torr; for 24h; | 48% |
With water; sodium acetate; triethylamine; Pd-bis(1-methylbenzothiazole-2-carbene) In N,N-dimethyl acetamide at 130℃; for 7h; | 55 % Chromat. |
Conditions | Yield |
---|---|
With copper acetylacetonate; oxygen; sodium hydroxide; 1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene In water at 50℃; under 760.051 Torr; for 12h; Sealed tube; | 99% |
With C4H11FeMo6NO24(3-)*3C16H36N(1+); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 8h; Green chemistry; | 99% |
With 2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In acetonitrile at 20℃; | 98% |
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
Stage #1: (1-nosyl-5-nitroindol-3-yl)methyl 1-naphthoate With 2-(N,N-dimethylamino)ethylthiol hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 0.25h; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether; water; acetonitrile Inert atmosphere; | 99% |
benzyl 1-naphthoate
toluene
A
1-naphthalenecarboxylic acid
B
1-methyl-3-(phenylmethyl)-benzene
C
1-methyl-4-(phenylmethyl)benzene
D
2-benzyltoluene
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; water at 80℃; for 2h; regioselective reaction; | A 99% B n/a C n/a D n/a |
Conditions | Yield |
---|---|
Stage #1: 1-Bromonaphthalene With iodine; magnesium In tetrahydrofuran at 60℃; for 17.25h; Inert atmosphere; Stage #2: sodium methyl carbonate In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: 1-Fluoronaphthalene With C78H70Al2Cl4N6P4Rh2; magnesium; ethylene dibromide In tetrahydrofuran at 20℃; for 22h; Inert atmosphere; Glovebox; Stage #2: carbon dioxide In tetrahydrofuran at 20℃; under 760.051 Torr; for 0.5h; Reagent/catalyst; Temperature; | 99% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; oxygen In acetonitrile at 20℃; for 10h; Irradiation; | 97% |
With periodic acid; pyridinium chlorochromate In acetonitrile | 96% |
With tert.-butylhydroperoxide; manganese(II) acetate; trifluoroacetic acid In acetonitrile at 80℃; under 15001.5 Torr; for 13h; Mechanism; chemoselective reaction; | 95% |
dicobalt octacarbonyl
1-naphthyl triflate
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane; water at 20℃; for 16h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 97% |
Conditions | Yield |
---|---|
With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In N,N-dimethyl-formamide at 100℃; for 20h; Inert atmosphere; Sealed tube; | 97% |
With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In N,N-dimethyl-formamide at 80℃; for 10h; Inert atmosphere; Sealed tube; | 75% |
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 3h; | 97% |
Conditions | Yield |
---|---|
With potassium; potassium iodide; magnesium chloride In tetrahydrofuran 1.) reflux, 1 h, 2.) -3 deg C, 4.5 h; | 96% |
With C26H30B10Cl2P2Pd In toluene at 50℃; under 760.051 Torr; for 10h; | 91% |
With diethylzinc; palladium diacetate; tert-butyl XPhos In hexanes; N,N-dimethyl acetamide at 40℃; under 7600.51 Torr; Automated synthesizer; | 69% |
With manganese; 2.9-dimethyl-1,10-phenanthroline; lithium acetate; cobalt(II) bromide In N,N-dimethyl acetamide at 20℃; under 760.051 Torr; for 12h; Inert atmosphere; Schlenk technique; | 68% |
With 6,6'-dimethyl-2,2'-bipyridine; lithium chloride; cobalt(II) iodide; zinc In N,N-dimethyl-formamide; acetonitrile at 40℃; under 760.051 Torr; for 14h; Sealed tube; | 46% |
dicobalt octacarbonyl
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane; water at 20℃; for 16h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 96% |
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 0.5h; | 95% |
Conditions | Yield |
---|---|
With dicobalt octacarbonyl; potassium carbonate; methyloxirane In methanol at 60℃; under 760 Torr; for 2.5h; | 92% |
With potassium hydroxide; (bis(tricyclohexyl)phosphine)palladium(II) dichloride In water for 72h; Heating; | 10300 % Turnov. |
With dicobalt octacarbonyl; potassium carbonate; benzyl chloride at 60℃; under 760 Torr; for 0.5h; carbonylation of aryl bromides, relative reactivity, effect of cocatalysts; |
Conditions | Yield |
---|---|
With dihydrogen peroxide In water; acetonitrile at 25℃; for 10h; UV-irradiation; | 92% |
With iodine; dimethyl sulfoxide at 120℃; for 26h; Sealed tube; Green chemistry; | 88% |
1-(4-methoxyphenyl)-2-(naphthalen-1-yl)ethan-1-one
A
1-naphthalenecarboxylic acid
B
4-methoxybenzoic acid
Conditions | Yield |
---|---|
With oxygen; potassium hydroxide at 20℃; Schlenk technique; chemoselective reaction; | A 92% B 92% |
Conditions | Yield |
---|---|
With potassium acetate; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate In dimethyl sulfoxide at 60℃; for 3h; | 90% |
Conditions | Yield |
---|---|
With 4,4’‐bis(trimethylammoniummethyl)‐2,2’‐bipyridine; bis-triphenylphosphine-palladium(II) chloride; water; sodium carbonate In water at 100℃; under 7600.51 Torr; for 24h; Catalytic behavior; Autoclave; | 90% |
With water; palladium diacetate; potassium carbonate at 20℃; under 760.051 Torr; for 5h; | 87% |
With water; potassium carbonate In acetonitrile at 100℃; under 3750.38 Torr; for 0.0161111h; | 87% |
With water; palladium diacetate; triethylamine; triphenylphosphine In 1,4-dioxane at 110℃; under 11251.1 Torr; for 2h; Flow reactor; | 43% |
carbon monoxide
1-Bromonaphthalene
A
1-naphthalenecarboxylic acid
B
1-naphthylglycolic acid
C
1-naphthylglyoxylic acid
Conditions | Yield |
---|---|
With methyl iodide; sodium sulfide In water; isopropyl alcohol at 20℃; for 20h; | A 6% B 3% C 89% |
With methyl iodide; sodium sulfide In water; isopropyl alcohol at 60℃; for 20h; | A 60% B 17% C 20% |
With sodium sulfide; CoCl2 In 1,4-dioxane; water at 20℃; for 20h; Product distribution; other reag.; other solvent; | A 4 % Chromat. B 9 % Chromat. C 86 % Chromat. |
Conditions | Yield |
---|---|
With acetic anhydride; N-ethyl-N,N-diisopropylamine; lithium chloride; palladium on activated charcoal In N,N-dimethyl-formamide at 100℃; for 10h; | 89% |
Stage #1: lithium formate With acetic anhydride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; Stage #2: 1-Iodonaphthalene With tris(dibenzylideneacetone)dipalladium (0); lithium chloride In N,N-dimethyl-formamide at 80℃; for 6h; | 82% |
(±)-1,2-di(naphthalen-1-yl)ethane-1,2-diol
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With sodium hypochlorite In acetonitrile at 20℃; for 18h; | 89% |
Conditions | Yield |
---|---|
In Petroleum ether -100 deg C to 0 deg C; | 88% |
1H-cyclobutanaphthalen-1-one
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In N,N,N,N,N,N-hexamethylphosphoric triamide for 3.5h; further reagents; | 88% |
Conditions | Yield |
---|---|
With potassium hydroxide In methanol at 35℃; for 1h; | 87% |
With tetramethyl ammoniumhydroxide In water; dimethyl sulfoxide at 83.3℃; Rate constant; substituents polar effects; |
Conditions | Yield |
---|---|
With 3,4-benzo-1,1,2,2-tetraethyl-1,2-disilacyclobut-3-ene; cesium fluoride In N,N-dimethyl-formamide at 0 - 20℃; under 760.051 Torr; for 2h; | 87% |
With copper(l) iodide; diethylzinc; N,N`-dimethylethylenediamine In dimethyl sulfoxide at 70℃; under 760.051 Torr; | 68% |
thiophenol
A
3-<(phenylthio)methyl>-1H-indole
B
1-naphthalenecarboxylic acid
C
2-nitrophenyl phenyl sulfide
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile Inert atmosphere; | A 84% B 82% C 86% |
Conditions | Yield |
---|---|
With potassium hydroxide In 1,2-dimethoxyethane | A 70% B 85% |
Conditions | Yield |
---|---|
With sodium hypochlorite In acetonitrile at 20℃; for 1.5h; | 85% |
With 2-(3-thiazolium)-1-phenylethanone bromide; triethylamine In dimethyl sulfoxide; acetonitrile at 37℃; Acidic conditions; |
1-(1-naphthyl)ethanol
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With sodium nitrate; water; oxygen In dimethyl sulfoxide at 130℃; for 36h; | 85% |
Conditions | Yield |
---|---|
With thionyl chloride In toluene for 2h; Reflux; | 100% |
With thionyl chloride for 2h; Heating / reflux; | 98% |
With thionyl chloride for 2h; Heating; | 98% |
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile for 1.5h; Heating; | 100% |
With caesium carbonate In acetonitrile at 20℃; for 1.5h; Reflux; Inert atmosphere; | 79% |
With caesium carbonate In acetonitrile at 20℃; for 90h; Reflux; Inert atmosphere; | 79% |
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran for 21h; Inert atmosphere; Reflux; |
1-naphthalenecarboxylic acid
[(1R,3S)-5-Iodo-6,8-dimethoxy-1-methyl-2-(toluene-4-sulfonyl)-1,2,3,4-tetrahydro-isoquinolin-3-yl]-methanol
((1R,3S)-5-iodo-6,8-dimethoxy-1-methyl-2-tosyl-1,2,3,4-tetrahydroisoquinolin-3-yl)methyl 1-naphthoate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; Inert atmosphere; | 100% |
1-naphthalenecarboxylic acid
cis-cis-decahydro-1-naphthoic acid
Conditions | Yield |
---|---|
With platinum(IV) oxide; hydrogen In acetic acid under 3000.3 Torr; | 100% |
1-naphthalenecarboxylic acid
1-[(1,1-dimethylethoxy)carbonyl]-2(S)-(2-methoxyethyl)piperazine
1-[(1,1-dimethylethoxy)carbonyl]-2(S)-(2-methoxyethyl)-4-(1-naphthalenylcarbonyl)piperazine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; Acylation; | 99% |
piperidine
1-naphthalenecarboxylic acid
(naphthalen-1-yl)(piperidin-1-yl)methanone
Conditions | Yield |
---|---|
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 99% |
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 21h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In water at 80℃; for 3h; | 99% |
Conditions | Yield |
---|---|
Stage #1: 1-naphthalenecarboxylic acid; N,0-dimethylhydroxylamine In toluene at 0℃; for 0.166667h; Stage #2: With phosphorus trichloride In toluene at 20 - 60℃; for 0.5h; | 99% |
1-naphthalenecarboxylic acid
carbonic acid dimethyl ester
methyl 1-naphthoate
Conditions | Yield |
---|---|
With 25 wt percent zeolite NaY-Bf at 200℃; for 5h; Autoclave; Green chemistry; | 99% |
With dimanganese decacarbonyl at 180℃; for 1h; Sealed tube; | 97% |
Conditions | Yield |
---|---|
With thionyl chloride at 0 - 40℃; for 1h; | 98.5% |
With oxone at 65℃; for 30h; | 92% |
With sulfuric acid at 65℃; for 2h; | 91% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 20h; | 98.1% |
Conditions | Yield |
---|---|
With 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 80℃; for 1.66667h; | 98% |
In various solvent(s) at 80℃; for 1.66667h; | 98% |
In toluene at 110℃; for 24h; | 89% |
Conditions | Yield |
---|---|
With pyridine; ammonium bicarbonate; di-tert-butyl dicarbonate In 1,4-dioxane at 20℃; | 98% |
Stage #1: 1-naphthalenecarboxylic acid With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In tetrahydrofuran for 0.0166667h; Milling; Stage #2: With ammonium thiocyanate In tetrahydrofuran for 0.0833333h; Milling; | 90% |
With ammonium carbonate; ortho-tungstic acid; silver(l) oxide In 5,5-dimethyl-1,3-cyclohexadiene at 160℃; for 8h; | 82.4% |
1-naphthalenecarboxylic acid
2-phenyl-1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; oxygen; palladium diacetate; p-benzoquinone In tert-butyl alcohol at 100℃; under 22801.5 Torr; for 24h; | 98% |
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 21h; Inert atmosphere; | 98% |
1-naphthalenecarboxylic acid
isopropyl bromide
1-isopropyl-1,4-dihydronaphthalene-1-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: 1-naphthalenecarboxylic acid With ammonia; lithium In water at -60℃; for 0.5h; Birch reduction; Stage #2: isopropyl bromide With tert-butyl alcohol In water regioselective reaction; | 98% |
Stage #1: 1-naphthalenecarboxylic acid With ammonia; lithium at -78℃; for 1h; Stage #2: isopropyl bromide at -78℃; for 0.25h; | |
With ammonia; lithium at -78℃; for 1.25h; Birch Reduction; |
1-naphthalenecarboxylic acid
N-methoxylamine hydrochloride
N-methoxynaphthalene-1-carboxamide
Conditions | Yield |
---|---|
Stage #1: 1-naphthalenecarboxylic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; for 4h; Under an atmosphere of argon; Stage #2: N-methoxylamine hydrochloride With potassium carbonate In water; ethyl acetate at 0 - 20℃; for 4h; | 98% |
With 1,1'-carbonyldiimidazole In tetrahydrofuran at 20℃; | 75% |
Stage #1: 1-naphthalenecarboxylic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; for 3.5h; Stage #2: N-methoxylamine hydrochloride With potassium carbonate In water; ethyl acetate at 20℃; for 20h; |
1-naphthalenecarboxylic acid
cyclohexene
cyclohex-2-en-1-yl 1-naphthoate
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; C11H23N2(1+)*Br4Fe(1-) In ethyl acetate at 110℃; for 24h; | 98% |
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In benzene at 80℃; for 8h; | 77% |
1-naphthalenecarboxylic acid
4-((tert-butyldimethylsilyloxy)methyl)phenol
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In acetonitrile at 20℃; for 1h; Inert atmosphere; Schlenk technique; | 98% |
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With copper diacetate; sodium carbonate; (3aR,3a'R,8aS,8a'S)-2,2'-(propane-2,2-diyl)bis(8,8a-dihydro-3aH-indeno[1,2-d]oxazole) In dichloromethane; water at 30℃; for 12h; enantioselective reaction; | 98% |
1-naphthalenecarboxylic acid
2-phenylethynylphenol
Conditions | Yield |
---|---|
Stage #1: 1-naphthalenecarboxylic acid; 2-phenylethynylphenol With bis(1,5-cyclooctadiene)diiridium(I) dichloride In dichloromethane at 20℃; for 1h; Stage #2: With silica gel regioselective reaction; | 98% |
1-naphthalenecarboxylic acid
tert-butyl 2-aminobenzylcarbamate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 24h; | 98% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View