Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:86-87-3
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHot sell stable quality 1-Naphthylacetic acid 86-87-3 with factory price Hangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special che
Cas:86-87-3
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Type:Manufacturers
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:86-87-3
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryProduct description: Product name 1-Naphthalene acetic acid CAS number 86-87-3 Assay ≥99% Appearance White crystalline powder Capacity 200mt/year Application Plant growth re
Cas:86-87-3
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryUnique advantages for 1-Naphthalene acetic acid(NAA) CAS 86-87-3 ISO&BV Factory with the largest capacity Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Product Name: 1-Naphthaleneac
Cas:86-87-3
Min.Order:25 Kilogram
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Type:Trading Company
inquiryService we can provide: 1. Mixed container: We can mix different items in one container. 2. Quality control: Before shipment, we can provide free sample for test. Inspection before shipping. 3. Packing: We can pack according to your requ
Cas:86-87-3
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
17-year experience in Phytochemicals Each product has passed very strict tests (NMR\MS\HPLC) Agents in 13 countries Certified by ISO 9001:2008 quality management system Leader Supplier of Botanical Reference Materials in China
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:86-87-3
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryADVANTAGE: 1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day 2. The products are provided with COA, HPLC, NMR, quality assurance,
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Cas:86-87-3
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:86-87-3
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryLinchuan's expertise and flexibility have made the company become one of the leading manufacturer of Naphthalene series, Biphenyl series , Anthracene series and 1-(CHLOROMETHYL)-4-ETHENYLBENZENE series, which are wildly used in the field of ele
Cas:86-87-3
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Cas:86-87-3
Min.Order:20 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryName:1-Naphthaleneacetic acid CAS no:86-87-3 Grade:plant growth regulator Molecular formula: C12H10O2 Molecular weight: 186.21 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data
Cas:86-87-3
Min.Order:25 Kilogram
FOB Price: $1.0 / 2.0
Type:Other
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:86-87-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be
Cas:86-87-3
Min.Order:1 Kilogram
FOB Price: $48.0 / 58.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:86-87-3
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:86-87-3
Min.Order:10 Kilogram
FOB Price: $100.0 / 120.0
Type:Trading Company
inquiry86-87-3 98%MIN low price supplier Density 1.2±0.1 g/cm3 Boiling Point 373.2±11.0 °C at 760 mmHg Melting Point 141-143 °C(lit.) Molecular Formula C12H10O2 Molecular Wei
Cas:86-87-3
Min.Order:1 Gram
FOB Price: $15.0
Type:Lab/Research institutions
inquiryName 1-Naphthylacetic acid (NAA) Other name 2-(1-Naphthyl)acetic acid ; 2-(α-Naphthyl)ethanoic acid; 2-naphthalen-1-ylacetic acid
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:86-87-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:86-87-3
Min.Order:10 Gram
FOB Price: $0.6
Type:Trading Company
inquiryProduct Name: 1-Naphthaleneacetic acid CAS: 86-87-3 MF: C12H10O2 MW: 186.21 EINECS: 201-705-8 Mol File: 86-87-3.mol 1-Naphthaleneacetic acid Structure 1-Naphthaleneacetic acid Chemical Properties Melting point 141-143 °C(l
Cas:86-87-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:86-87-3
Min.Order:1 Kilogram
FOB Price: $26.0 / 30.0
Type:Trading Company
inquiry1-Naphthaleneacetic acid CAS:86-87-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
Cas:86-87-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:86-87-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several
Cas:86-87-3
Min.Order:25 Gram
FOB Price: $90.0 / 100.0
Type:Trading Company
inquiryConditions | Yield |
---|---|
Stage #1: 1-naphthylmethyl halide With lithium chloride; zinc Stage #2: carbon dioxide With lithium chloride In N,N-dimethyl-formamide at 50℃; under 760.051 Torr; for 24h; Stage #3: With hydrogenchloride; water In N,N-dimethyl-formamide | 100% |
Conditions | Yield |
---|---|
With periodic acid; tripropylammonium fluorochromate (VI) In acetonitrile at 0℃; | 99% |
With periodic acid; pyridinium chlorochromate In acetonitrile | 97% |
Conditions | Yield |
---|---|
at 200℃; Molecular sieve; Large scale; | 96.7% |
at 165℃; dann auf 180-185grad; | |
With iron; potassium bromide at 220℃; |
α-(N-Methylanilino)-β-(1-naphthyl)acrylonitrile
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran for 3h; Heating; | 96% |
(Z)-α-(N-Methylanilino)-β-(1-naphthyl)acrylonitrile
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran for 3h; Heating; | 96% |
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; for 0.0833333h; Reagent/catalyst; | 94% |
Conditions | Yield |
---|---|
With high-silica Hβ-75 zeolite In water at 130℃; for 24h; | 93% |
With potassium carbonate; thiophenol In 1-methyl-pyrrolidin-2-one at 190℃; for 0.166667h; Substitution; | 90% |
With potassium fluoride; thiophenol In various solvent(s) at 190℃; for 0.166667h; | 80% |
Naphthalen-1-yl-acetic acid 2-oxo-2-phenyl-ethyl ester
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With sodium hydrogen telluride In N,N-dimethyl-formamide for 0.333333h; Ambient temperature; | 93% |
Conditions | Yield |
---|---|
With water; sodium hydroxide In 1,4-dioxane at 60℃; for 2h; pH=10 - 14; | 92% |
With sodium hydroxide |
Conditions | Yield |
---|---|
With potassium phosphate buffer at 30℃; for 96h; Rhodococcus sp. AJ270 cells; | 91.3% |
Stage #1: naphthalen-1-ylacetonitrile With sodium hydroxide In water for 3h; Reflux; Stage #2: With hydrogenchloride In water pH=2; Time; | 74.8% |
With sulfuric acid; acetic acid |
1-naphthylacetaldehyde
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen In acetonitrile at 60℃; for 3h; Schlenk technique; | 87% |
With N-hydroxyphthalimide; oxygen In acetonitrile at 30℃; under 760.051 Torr; for 3h; Schlenk technique; | 87% |
With AgOH |
Conditions | Yield |
---|---|
Stage #1: carbon monoxide With C28H22CoN4O6 In butan-1-ol at 60℃; under 760.051 Torr; for 2h; Glovebox; High pressure; Green chemistry; Stage #2: 1-Chloromethylnaphthalene With tetra-(n-butyl)ammonium iodide; sodium hydroxide In butan-1-ol at 60℃; under 760.051 Torr; for 22h; Glovebox; High pressure; Green chemistry; regioselective reaction; | 85% |
With sodium hydroxide; cerium(III) chloride; cetyltrimethylammonim bromide; nickel cyanide In toluene at 85 - 95℃; under 1 Torr; for 7h; | 60% |
With water; palladium diacetate at 110℃; under 37503.8 Torr; for 4h; Ionic liquid; | 92 %Chromat. |
N-((E)-1-Cyano-2-naphthalen-1-yl-vinyl)-4,N-dimethyl-benzamide
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran for 6h; Heating; | 83% |
ethyl 2-(1-naphthyl)-2-oxoacetate
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(1-naphthyl)-2-oxoacetate With hydrazine In 1,2-dimethoxyethane at 130℃; for 2h; Stage #2: With potassium hydroxide In 1,2-dimethoxyethane at 80℃; for 8h; Temperature; Solvent; Reflux; | 83% |
Conditions | Yield |
---|---|
With niobium(V) oxide; water In neat (no solvent) for 30h; Reflux; Inert atmosphere; | 83% |
carbon dioxide
naphthalen-1-ylmethylene-hydrazone
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; caesium carbonate; cesium fluoride In N,N-dimethyl-formamide at 80℃; under 760.051 Torr; for 24h; chemoselective reaction; | 81% |
methanol
Naphthalen-1-yl-acetic acid pyren-1-ylmethyl ester
A
naphth-1-yl acetic acid
B
methyl 1-pyrenylmethyl ether
Conditions | Yield |
---|---|
for 2h; Quantum yield; Irradiation; | A 80% B n/a |
methyl α-oxo-1-naphthaleneacetate
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
Stage #1: methyl α-oxo-1-naphthaleneacetate With hydrazine In propylene glycol at 130℃; for 2h; Stage #2: With sodium hydroxide In propylene glycol at 80℃; for 8h; Solvent; Temperature; Reflux; | 78% |
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; α,α′-bis(2-pyridyl(tert-butyl)phosphino)-o-xylene; palladium diacetate In N,N-dimethyl-formamide at 115℃; for 12h; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With manganese; dichlorobis(trimethylphosphine)nickel In N,N-dimethyl-formamide at 20℃; under 760.051 Torr; for 48h; Schlenk technique; | 64% |
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; water In 1,4-dioxane at 175℃; for 0.5h; Microwave irradiation; Green chemistry; | 39% |
Conditions | Yield |
---|---|
With sodium acetate; palladium on activated charcoal In ethanol under 2327.2 Torr; for 1.5h; Ambient temperature; | 24% |
diethyl ether
methylammonium carbonate
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With diethyl ether; magnesium anschliessendes Behandeln mit Chloressigsaeure; |
1-allylnaphthalene
A
naphth-1-yl acetic acid
B
3-[1]naphthyl-propane-1,2-diol
Conditions | Yield |
---|---|
With potassium permanganate; ethanol; water weiteres Reagens: Natriumacetat; |
4-(naphthalen-1-yl-thioacetyl)-morpholine
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid | |
With potassium hydroxide |
4-naphthalen-1-ylmethylene-2-phenyl-4H-oxazol-5-one
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
nachfolgend Oxydation mit Wasserstoffperoxyd; |
1-naphthylglyoxylic acid
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With phosphorus; hydrogen iodide at 160℃; | |
With potassium hydroxide; hydrazine hydrate |
Conditions | Yield |
---|---|
With thionyl chloride | 100% |
With thionyl chloride for 2h; Reflux; | 100% |
With thionyl chloride; N,N-dimethyl-formamide for 4h; | 100% |
Conditions | Yield |
---|---|
With thionyl chloride for 3.5h; Heating; | 100% |
With iron(III) sulfate; sulfuric acid for 3.5h; Heating; | 86% |
With sulfuric acid |
Conditions | Yield |
---|---|
With hydrogenchloride for 1h; Heating; | 100% |
With thionyl chloride at 20℃; | 99% |
With iron(III) sulfate; sulfuric acid for 1.5h; Heating; | 98% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; copper diacetate In acetic acid for 2h; Heating; | 100% |
naphth-1-yl acetic acid
ethyl iodide
2-(naphthalen-1-yl)butanoic acid
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at 20℃; for 0.5h; Stage #2: ethyl iodide In tetrahydrofuran; n-heptane; ethylbenzene at 20℃; for 0.0833333h; Further stages.; | 100% |
Stage #1: naphth-1-yl acetic acid With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 1h; Stage #2: ethyl iodide at 0 - 20℃; | |
Stage #1: naphth-1-yl acetic acid With n-butyllithium In tetrahydrofuran; hexanes at 0℃; for 0.166667h; Inert atmosphere; Stage #2: ethyl iodide In tetrahydrofuran; hexanes Inert atmosphere; | |
Stage #1: naphth-1-yl acetic acid With n-butyllithium In tetrahydrofuran; hexane at -78 - 0℃; for 2.16667h; Inert atmosphere; Stage #2: ethyl iodide In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; |
naphth-1-yl acetic acid
endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide | 99% |
cycl-isopropylidene malonate
naphth-1-yl acetic acid
5-[1-hydroxy-2-(nalphthalen-1-yl)ethylidene]-2,2-dimethyl[1,3]dioxane-4,6-dione
Conditions | Yield |
---|---|
Stage #1: cycl-isopropylidene malonate; naphth-1-yl acetic acid With dmap In dichloromethane at -10℃; for 0.75h; Stage #2: With dicyclohexyl-carbodiimide In dichloromethane at -10 - 20℃; | 99% |
Stage #1: naphth-1-yl acetic acid With 1,1'-carbonyldiimidazole In dichloromethane for 0.5h; Stage #2: cycl-isopropylidene malonate In dichloromethane for 12h; | |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; Inert atmosphere; | |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; |
Conditions | Yield |
---|---|
With trifluoroacetic acid In acetonitrile at 60℃; for 4h; | 99% |
naphth-1-yl acetic acid
benzylamine
N-benzyl-2-(naphthalen-1-yl)acetamide
Conditions | Yield |
---|---|
With borane-ammonia complex In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Reflux; | 99% |
Stage #1: naphth-1-yl acetic acid With 1,3,5-trichloro-2,4,6-triazine; caesium carbonate In dichloromethane at 20℃; for 0.333333h; Inert atmosphere; Sonication; Stage #2: benzylamine In dichloromethane Sonication; Inert atmosphere; | 89% |
Stage #1: naphth-1-yl acetic acid With titanium(IV) isopropylate In tetrahydrofuran at 40 - 70℃; Molecular sieve; Inert atmosphere; Stage #2: benzylamine In tetrahydrofuran at 70℃; Molecular sieve; Inert atmosphere; | 79% |
Stage #1: naphth-1-yl acetic acid With 4-(dimethylamino)pyridine N-oxide; phenylboronic acid In benzene at 20℃; for 0.0833333h; Molecular sieve; Reflux; Stage #2: benzylamine In fluorobenzene for 3h; Reflux; Molecular sieve; | 20% |
Stage #1: naphth-1-yl acetic acid With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran; N,N-dimethyl-formamide at -15℃; Inert atmosphere; Stage #2: benzylamine In tetrahydrofuran; N,N-dimethyl-formamide at -15 - 20℃; for 1.5h; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In tetrahydrofuran for 0.0166667h; Milling; Stage #2: With ammonium thiocyanate In tetrahydrofuran for 0.0833333h; Milling; | 98% |
Stage #1: naphth-1-yl acetic acid With thionyl chloride In dichloromethane at 0℃; for 2h; Stage #2: With ammonium hydroxide In tetrahydrofuran at 0 - 20℃; | 88% |
With phosphorus pentachloride Behandeln mit Ammoniumcarbonat; |
Conditions | Yield |
---|---|
In toluene for 12h; Reflux; | 98% |
In toluene at 110℃; for 24h; | 92% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In acetonitrile at 60℃; for 4h; | 98% |
naphth-1-yl acetic acid
1-tosyl-4-vinyl-1,4-dihydro-2H-benzo[d] [1,3]oxazin-2-one
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid With pivaloyl chloride; caesium carbonate In 1,3,5-trimethyl-benzene at 0℃; for 0.5h; Inert atmosphere; Stage #2: 1-tosyl-4-vinyl-1,4-dihydro-2H-benzo[d] [1,3]oxazin-2-one With tris-(dibenzylideneacetone)dipalladium(0); (R)-BIDIME In 1,3,5-trimethyl-benzene at 0℃; Inert atmosphere; Molecular sieve; stereoselective reaction; | 98% |
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid; (2S,4S)-4-hydroxy-4-((3aR,7S,8aS)-7-methyl-3-methylene-2-oxo-3,3a,4,7,8,8a-hexahydro-2H-cyclohepta[b]furan-6-yl)butan-2-yl acetate With dmap In dichloromethane at 0℃; Stage #2: With dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 3.08333h; | 97% |
naphth-1-yl acetic acid
methyl iodide
2-(naphthalen-1-yl)propanoic acid
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid With lithium diisopropyl amide In tetrahydrofuran at -78 - 0℃; Stage #2: methyl iodide In tetrahydrofuran at 20℃; Further stages.; | 96% |
Stage #1: naphth-1-yl acetic acid With lithium diisopropyl amide In tetrahydrofuran at -78 - 0℃; for 1.41667h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at 20℃; Time; | 96% |
Stage #1: naphth-1-yl acetic acid With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at 20℃; for 0.5h; Stage #2: methyl iodide In tetrahydrofuran; n-heptane; ethylbenzene at 20℃; for 0.0833333h; Further stages.; | 86% |
naphth-1-yl acetic acid
trimethylsilyl cyanide
3-(naphthalen-1-yl)propanenitrile
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid With indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane; iodine In chloroform at 60℃; Inert atmosphere; Stage #2: trimethylsilyl cyanide With tetrabutyl ammonium fluoride In tetrahydrofuran; chloroform at 60℃; for 5h; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 96% |
Conditions | Yield |
---|---|
With oxygen; copper(II) trifluoroacetate; urea In dimethyl sulfoxide at 120℃; for 22h; Green chemistry; | 96% |
With 1,10-Phenanthroline; oxygen; copper(II) oxide; potassium ferrocyanide In dimethyl sulfoxide at 120℃; under 11251.1 Torr; for 40h; Autoclave; | 70% |
With iron(III) trifluoromethanesulfonate; sodium nitrite In dimethyl sulfoxide at 50℃; for 10h; Inert atmosphere; Sealed tube; | 69% |
naphth-1-yl acetic acid
(4-((tert-butyldimethylsilyl)oxy)phenyl)methanol
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 2.5h; | 96% |
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In 1,4-dioxane at 20℃; for 2h; Inert atmosphere; | 95% |
3-descladinosyl-9-deokso-9a-aza-9a-(3-aminopropyl)-9a-homoeritromicin A
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid With PS-carbodiimide In dichloromethane at 20℃; for 1h; Stage #2: 3-descladinosyl-9-deokso-9a-aza-9a-(3-aminopropyl)-9a-homoeritromicin A In dichloromethane at 20℃; for 2h; | 95% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; | 95% |
naphth-1-yl acetic acid
methyl salicylate
A
methyl 1-naphthylacetate
B
salicylic acid
Conditions | Yield |
---|---|
Stage #1: naphth-1-yl acetic acid With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.5h; Stage #2: methyl salicylate at 110℃; for 24h; | A 95% B n/a |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 95% |
Conditions | Yield |
---|---|
With tricarbonyl(η(4)-cycloocta-1,5-diene)iron; phenylsilane In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; UV-irradiation; chemoselective reaction; | 94% |
With borane In tetrahydrofuran for 1h; Ambient temperature; | 90% |
With tin(II) trifluoromethanesulfonate; tris(2,4-pentanedionato)ruthenium(III); hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In water; toluene at 160℃; under 45004.5 Torr; for 48h; Autoclave; | 87% |
naphth-1-yl acetic acid
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 10h; | 94% |
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