Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:86-52-2
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inquiryLinchuan's expertise and flexibility have made the company become one of the leading manufacturer of Naphthalene series, Biphenyl series , Phenanthrene series, Anthracene series, which are wildly used in the field of electronic chemical and
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiry1-Chloromethyl naphthalene CAS 86-52-2 English name: 1-(Chloromethyl)naphthalene Synonyms:1-Naphthylmethyl chloride; 1-(CHLOROMETHYL)-NAPHTHALENE; 1-CMN; a-Naphthylmethyl Chloride; 1-Chloromethyl naphthalene; 1-Chloromethyl-naphthalene
Cas:86-52-2
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inquiryProduct description: Product name 1-Chloromethyl naphthalene CAS number 86-52-2 Assay ≥99% Appearance Colorless liquid or Solid Capacity 200mt/year Application Organic inter
Cas:86-52-2
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:86-52-2
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:86-52-2
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inquiryProduct Name: 1-Chloromethyl naphthalene Synonyms: 1-(Chlormethyl)naftalen;1-(chloromethyl)-naphthalen;1-(Chloromethyl)naphthene;1-chloromethyl-naphthalen;1-Menaphthyl chloride;1-menaphthylchloride;alpha-(C
Cas:86-52-2
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:86-52-2
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:86-52-2
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:86-52-2
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inquiryProduct name 1-Chloromethyl naphthalene Product category Naphthalene series CAS NO. 86-52-2 Structural formula Content ≥99% Appearance:White powder Storage:Store in cool and dry pl
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Cas:86-52-2
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:86-52-2
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inquiryProduct Name: 1-Chloromethyl naphthalene CHLOROMETHYLNAPHTHYL CAS: 86-52-2 MF: C11H9Cl MW: 176.64 EINECS: 201-678-2 Mol File: 86-52-2.mol 1-Chloromethyl naphthalene Structure 1-Chloromethyl naphthalene Chemical Properties Melting p
Cas:86-52-2
Min.Order:1 Gram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:86-52-2
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inquiryBeluga chemical professional supply High quality 1-Chloromethyl naphthaleneCAS 86-52-2 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made
Cas:86-52-2
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:86-52-2
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:86-52-2
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inquiryHubei Lidu New Materials Technology Co. , Ltd. is located in No. 12,3C Industrial Park, Zhongxiang Economic Development Zone, Hubei Province. The company is committed to fine chemical raw materials, pharmaceutical intermediates and other production,
Cas:86-52-2
Min.Order:1 Gram
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:86-52-2
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:86-52-2
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:86-52-2
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:86-52-2
Min.Order:4 Kilogram
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Conditions | Yield |
---|---|
With thionyl chloride In toluene for 12h; | 98% |
With thionyl chloride In chloroform at 5 - 30℃; | 98.4% |
With pyridine; thionyl chloride In diethyl ether at -5 - 25℃; for 12h; | 98% |
1-(dimethoxymethyl)naphthalene
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With triethylsilane; acetyl chloride; tin(ll) chloride In dichloromethane at 0℃; for 2h; | 92% |
Conditions | Yield |
---|---|
With bis(tri-ortho-tolylphosphine)palladium(0); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine In toluene at 130℃; for 20h; Inert atmosphere; Glovebox; | 92% |
1-naphthalene methanol
Benzotrichlorid
A
benzylidene dichloride
B
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With TOP; phenylsilane In neat (no solvent) at 100℃; for 24h; Appel Halogenation; Inert atmosphere; | A n/a B 81% |
1-tributylstannyl-methylnaphthalene
A
1-naphthalenecarboxylic acid
B
1-naphthalene methanol
C
1-naphthaldehyde
D
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With C2H2Cl2F3O2V; oxygen In tert-butyl alcohol at 50℃; for 24h; | A 38% B n/a C 58% D n/a |
With C2H2Cl2F3O2V; oxygen In tert-butyl alcohol at 50℃; for 24h; | A 28% B 5% C 58% D 4% |
Conditions | Yield |
---|---|
With hydrogenchloride; phosphoric acid; acetic acid In water for 6h; Reflux; | 56% |
With hydrogenchloride; zinc(II) chloride; Petroleum ether | |
With hydrogenchloride at 60 - 65℃; |
1-Methylnaphthalene
A
4-chloro-1-methyl-naphthalene
B
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With N-chloro-succinimide; barium(II) chloride at 102℃; under 2625.26 Torr; for 0.0666667h; Microwave irradiation; Darkness; chemoselective reaction; | A 45% B 18% |
With aluminum oxide; iron(III) chloride Irradiation; Title compound not separated from byproducts; | |
With aluminum oxide; iron(III) chloride Irradiation; Title compound not separated from byproducts; |
dichloromethane
(naphthalene-1,8-diyl)dilithium
A
naphthalene
B
1,1'-cis-ethene-1,2-diyl-bis-naphthalene
C
(E)-1,2-bis(1-naphthyl)ethene
D
1H-Cyclobutanaphthalene
E
1-Chloromethylnaphthalene
F
acenaphthylene
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine In diethyl ether at -100 - -60℃; Product distribution; Mechanism; var. of temp., further with CD2Cl2; | A 42% B n/a C n/a D 21% E n/a F n/a |
tetrachloromethane
1-Methylnaphthalene
A
bis-chloromethylnaphthalene
B
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
at 250℃; under 52505.3 Torr; for 7h; Inert atmosphere; | A 37% B 36% |
1-Methylnaphthalene
A
bis-chloromethylnaphthalene
B
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With tetrachloromethane at 250℃; for 7h; Inert atmosphere; Autoclave; | A 37% B 36% |
Conditions | Yield |
---|---|
With N-chloro-succinimide; N-hydroxyphthalimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 80℃; for 3h; Time; Sealed tube; Inert atmosphere; | 16% |
With N-hydroxyphthalimide; carbon tetrabromide; trichloroisocyanuric acid; copper(II) acetate monohydrate In dichloromethane at 25℃; for 21h; | 15% |
With chlorine at 260℃; | |
With chlorine | |
With sodium hypochlorite; tetrabutyl-ammonium chloride In dichloromethane at 20℃; for 12h; Catalytic behavior; Inert atmosphere; Sealed tube; | 20 %Chromat. |
Conditions | Yield |
---|---|
With chlorobenzene unter Einwirkung von UV-Licht; |
Conditions | Yield |
---|---|
With hydrogenchloride; formaldehyd; arsenic trichloride | |
With hydrogenchloride; formaldehyd; arsenic(III) trioxide |
Conditions | Yield |
---|---|
With acetic acid at 65℃; |
Conditions | Yield |
---|---|
With hydrogenchloride; formaldehyd; acetic acid |
Conditions | Yield |
---|---|
With diethyl ether; tin(IV) chloride |
naphthalene
chloromethyl isocyanate
A
2-naphthylmethylisocyanate
B
1-isocyanatomethyl-naphthalene
C
1-Chloromethylnaphthalene
D
1-chloromethylnaphthalene
Conditions | Yield |
---|---|
With iron(III) chloride at 140 - 150℃; for 2h; | A 10 % Spectr. B 85 % Spectr. C n/a D n/a |
With iron(III) chloride at 40 - 150℃; for 2h; | A 10 % Spectr. B 85 % Spectr. C n/a D n/a |
1-(diazomethyl)naphthalene
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With 1,1,2-Trichloro-1,2,2-trifluoroethane Irradiation; |
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With phosphorus pentachloride |
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With phosphorus pentachloride Destillieren des Reaktionsgemisches im Vakuum; |
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With phosphorus pentachloride Destillieren des Reaktionsgemisches im Vakuum; |
formaldehyd
naphthalene
(E)-3-Ureido-but-2-enoic acid ethyl ester
1-Chloromethylnaphthalene
naphthalene
diethyl ether
ethyl chloromethyl ether
1-Chloromethylnaphthalene
hydrogenchloride
formaldehyd
naphthalene
water
A
1,4-bis(chloromethyl)naphthalene
B
1,5-bis(chloromethyl)naphthalene
C
1-Chloromethylnaphthalene
phosphorus pentachloride
bis(α-naphthylmethyl) ether
1-Chloromethylnaphthalene
1-naphthalene methanol
A
bis(α-naphthylmethyl) ether
B
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With hydrogenchloride In water at 120℃; under 5171.62 Torr; for 0.25h; Flow reactor; | A n/a B 90 %Spectr. |
A
(naphtalen-1-yl)methyl iodide
C
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With Iodine monochloride In dichloromethane at 20℃; Inert atmosphere; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride; N,N-dimethyl-formamide / 4 h 2: bis(tri-ortho-tolylphosphine)palladium(0); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine / toluene / 20 h / 130 °C / Inert atmosphere; Glovebox View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / ethanol / 0.5 h / 0 °C 2: pyridine; thionyl chloride / diethyl ether / 12 h / -5 - 25 °C View Scheme |
1-Chloromethylnaphthalene
triethyl phosphite
diethyl 1-naphthylmethylphosphonate
Conditions | Yield |
---|---|
at 160℃; for 7h; Reflux; | 100% |
at 150℃; |
(N-benzoyl-anilino)-phenyl-acetonitrile
1-Chloromethylnaphthalene
N-(1-Cyano-2-naphthalen-1-yl-1-phenyl-ethyl)-N-phenyl-benzamide
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide for 96h; | 100% |
2-<(tetrahydrofur-2-yl)methyl>propanedionate de dimethyle
1-Chloromethylnaphthalene
2-<(naphth-1-yl)methyl>-2-<(tetrahydrofur-2-yl)methyl>propanedioate de dimethyle
Conditions | Yield |
---|---|
With sodium methylate; carbonic acid dimethyl ester for 42h; Heating; | 100% |
2-<(tetrahydrofur-2-yl)methyl>propanedionate de dimethyle
1-Chloromethylnaphthalene
2-<(naphth-1-yl)methyl>-2-<(tetrahydrofur-2-yl)methyl>propanedioate de dimethyle
Conditions | Yield |
---|---|
With sodium methylate; carbonic acid dimethyl ester for 42h; Heating; | 100% |
O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate)
propylene sulphide
1-Chloromethylnaphthalene
polymer, three-armed star-shaped, Mn 11900 Da, Mw/Mn 1.14; monomer(s): 1,3,5-tri[2-(benzylaminothiocarbonyloxy)-3-mercaptopropyl]-1,3,5-triazine-2,4,6(1H,3H,5H)-trione; propylene sulfide; 1-(chloromethyl)naphthalene
Conditions | Yield |
---|---|
Stage #1: O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate) With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at -78℃; for 0.5h; Stage #2: propylene sulphide In N,N-dimethyl-formamide at 0℃; for 2h; Stage #3: 1-Chloromethylnaphthalene With triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate)
propylene sulphide
1-Chloromethylnaphthalene
polymer, three-armed star-shaped, Mn 15500 Da, Mw/Mn 1.17; monomer(s): 1,3,5-tri[2-(benzylaminothiocarbonyloxy)-3-mercaptopropyl]-1,3,5-triazine-2,4,6(1H,3H,5H)-trione; propylene sulfide; 1-(chloromethyl)naphthalene
Conditions | Yield |
---|---|
Stage #1: O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate) With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at -78℃; for 0.5h; Stage #2: propylene sulphide In N,N-dimethyl-formamide at 0℃; for 2h; Stage #3: 1-Chloromethylnaphthalene With triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
for 2.5h; Heating; | 100% |
1-Chloromethylnaphthalene
C22H24N2O
Conditions | Yield |
---|---|
Stage #1: N-tert-butyl-3-methylpyridine-2-carboxamide With n-butyllithium; sodium bromide In tetrahydrofuran; hexane at -40℃; for 0.5h; Stage #2: 1-Chloromethylnaphthalene In tetrahydrofuran; hexane at -40℃; for 1.5h; | 100% |
4-nitro-aniline
1-Chloromethylnaphthalene
bis(naphthalen-1-ylmethyl)(4-nitrophenyl)amine
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 100℃; for 24h; Inert atmosphere; | 100% |
4-nitro-phenol
1-Chloromethylnaphthalene
1-(4-nitrophenoxymethyl)naphthalene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 4h; | 99.1% |
1-Chloromethylnaphthalene
1,2-di(1-naphthyl)ethane
Conditions | Yield |
---|---|
With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; zinc In tetrahydrofuran at 23 - 25℃; for 5h; Irradiation; Inert atmosphere; | 99% |
With magnesium In tetrahydrofuran at 20℃; for 2.5h; Reflux; | 96% |
With copper(I) bromide In water at 20℃; for 0.416667h; under air; | 88% |
1-Chloromethylnaphthalene
1-(azidomethyl)naphthalene
Conditions | Yield |
---|---|
With sodium azide In acetonitrile for 16h; Reflux; | 99% |
With sodium azide In dimethyl sulfoxide | 91% |
With sodium azide In dimethyl sulfoxide | 91% |
1-Chloromethylnaphthalene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 4h; Ambient temperature; | 99% |
1H-imidazole
1-Chloromethylnaphthalene
1-(naphthalen-1-ylmethyl)-1H-imidazole
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran Heating; | 99% |
With potassium carbonate In acetonitrile Reflux; | 90% |
Stage #1: 1H-imidazole With sodium hydride In 1,2-dimethoxyethane at 0℃; for 0.75h; Stage #2: 1-Chloromethylnaphthalene In 1,2-dimethoxyethane at 20℃; for 4h; Further stages.; | |
In dichloromethane | |
Stage #1: 1H-imidazole With sodium hydride In 1,4-dioxane at 90℃; for 1h; Stage #2: 1-Chloromethylnaphthalene In 1,4-dioxane at 90℃; for 22h; |
O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate)
propylene sulphide
1-Chloromethylnaphthalene
polymer, three-armed star-shaped, Mn 8500 Da, Mw/Mn 1.06; monomer(s): 1,3,5-tri[2-(benzylaminothiocarbonyloxy)-3-mercaptopropyl]-1,3,5-triazine-2,4,6(1H,3H,5H)-trione; propylene sulfide; 1-(chloromethyl)naphthalene
Conditions | Yield |
---|---|
Stage #1: O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate) With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at -78℃; for 0.5h; Stage #2: propylene sulphide In N,N-dimethyl-formamide at 0℃; for 2h; Stage #3: 1-Chloromethylnaphthalene With triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; | 99% |
potassium phtalimide
1-Chloromethylnaphthalene
2-[(1-naphthyl)methyl]-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
In DMF (N,N-dimethyl-formamide) at 100℃; | 99% |
In N,N-dimethyl-formamide | 99% |
In N,N-dimethyl-formamide at 20℃; for 10h; Inert atmosphere; |
1-Chloromethylnaphthalene
(2E)-3-phenyl-2-propen-1-ol
(E)-3-phenyl-2-propenyl 1-naphthylmethyl ether
Conditions | Yield |
---|---|
Stage #1: (2E)-3-phenyl-2-propen-1-ol With tetra-(n-butyl)ammonium iodide; sodium hydride In tetrahydrofuran at 0 - 20℃; for 0.5h; Stage #2: 1-Chloromethylnaphthalene In tetrahydrofuran at 20℃; for 24h; | 99% |
(S)-4-benzyl-1-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazole
1-Chloromethylnaphthalene
(S)-4-benzyl-1-(2,6-diisopropylphenyl)-3-(naphthalen-1-ylmethyl)-4,5-dihydro-1H-imidazol-3-ium chloride
Conditions | Yield |
---|---|
In acetonitrile at 110℃; for 5h; | 99% |
N-formyldiethylamine
1-Chloromethylnaphthalene
1-<(N,N-diethylamino)methyl>naphthalene
Conditions | Yield |
---|---|
With NHC-Pd(II)-Im; sodium hydroxide In water at 50℃; for 3h; Inert atmosphere; Schlenk technique; | 99% |
With potassium hydroxide In water at 50℃; for 3h; Green chemistry; | 85% |
t-butyl malonate
1-Chloromethylnaphthalene
di-t-butyl (1-naphthylmethyl)malonate
Conditions | Yield |
---|---|
In tetrahydrofuran; ethyl acetate | 98.4% |
triphenylphosphine
1-Chloromethylnaphthalene
1-naphthylmethyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
In toluene Reflux; | 98% |
In acetonitrile for 8h; Heating; | 94% |
In N,N-dimethyl-formamide for 5h; Heating; | 91% |
1-Chloromethylnaphthalene
trimethylamine
N,N,N-trimethyl-1-(naphthalene-1-yl)methanaminium chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 60℃; for 12h; | 98% |
In ethanol | 80% |
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; ammonium hydroxide In PEG1000-DIL; methyl cyclohexane at 60℃; for 3h; | 98% |
With ammonia fluess. Ammoniak; | |
With hydrogenchloride; hexamethylenetetramine 1) CH2Cl2, 12 h, 2) ethanol; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere 2: hydrazine hydrate / ethanol / 4 h / Inert atmosphere; Reflux View Scheme |
Conditions | Yield |
---|---|
With potassium formate; PdCl22 In benzene at 60℃; for 4h; | 98% |
With potassium formate; PdCl22 In benzene at 60℃; for 4h; Product distribution; further catalyst, reagent; solid or aqueous solution of reagent; | 98% |
With sodium tetrahydroborate; water In methanol at 20℃; for 0.333333h; | 94% |
O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate)
propylene sulphide
1-Chloromethylnaphthalene
polymer, three-armed star-shaped, Mn 5700 Da, Mw/Mn 1.10; monomer(s): 1,3,5-tri[2-(benzylaminothiocarbonyloxy)-3-mercaptopropyl]-1,3,5-triazine-2,4,6(1H,3H,5H)-trione; propylene sulfide; 1-(chloromethyl)naphthalene
Conditions | Yield |
---|---|
Stage #1: O,O',O''-((2,4,6-trioxo-1,3,5-triazinane-1,3,5-triyl)tris(1-mercaptopropane-3,2-diyl))tris(benzylcarbamothioate) With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at -78℃; for 0.5h; Stage #2: propylene sulphide In N,N-dimethyl-formamide at 0℃; for 2h; Stage #3: 1-Chloromethylnaphthalene With triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; | 98% |
1-Chloromethylnaphthalene
2-Amino-5-nitrophenol
2-(α-naphthylmethoxy)-4-nitroaniline
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 98% |
(S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol
1-Chloromethylnaphthalene
(R)-1-O-(1-naphthylmethyl)glycerol
Conditions | Yield |
---|---|
Stage #1: (S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol; 1-Chloromethylnaphthalene With potassium hydroxide In 1,4-dioxane; toluene for 2h; Heating; Stage #2: With acetic acid at 20℃; for 6h; Further stages.; | 98% |
Stage #1: (S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol; 1-Chloromethylnaphthalene With potassium hydroxide In 1,4-dioxane; toluene at 120℃; for 2h; Stage #2: With water; acetic acid at 20℃; for 6h; | 98% |
carbon disulfide
1-amino-2-propene
1-Chloromethylnaphthalene
2-(naphthalen-1-yl)methyl N-allylcarbamodithioate
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; for 3h; | 98% |
4-morpholinecarboxaldehyde
1-Chloromethylnaphthalene
4-(naphthalene-1-ylmethyl)morpholine
Conditions | Yield |
---|---|
With NHC-Pd(II)-Im; sodium hydroxide In water at 50℃; for 3h; Inert atmosphere; Schlenk technique; | 98% |
With potassium hydroxide In water at 80℃; for 3h; Temperature; Green chemistry; | 87% |
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