DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1-NAPHTHALENEMETHYLAMINE Basic information Product Name: 1-NAPHTHALENEMETHYLAMINE Synonyms: 1-naphthalenemethanamine;1-Naphthylmethanamine;alpha-Naphthylmethylamine;A-MENAPHTHYLAMINE
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAppearance:Clear light yellow to yellow liquid Storage:Keep in dark place,Inert atmosphere,2-8°C Package:25kg/Barrel Application:APIs Transportation:Express/Sea/Air Port:Any port in China
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:118-31-0
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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Product Name: 1-NAPHTHALENEMETHYLAMINE CAS: 118-31-0 MF: C11H11N MW: 157.21 EINECS: 204-244-0 Mol File: 118-31-0.mol 1-NAPHTHALENEMETHYLAMINE Structure 1-NAPHTHALENEMETHYLAMINE Chemical Properties Melting point 262-269 °C
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
1-(azidomethyl)naphthalene
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
Stage #1: 1-(azidomethyl)naphthalene With 9-phenyl-9-phosphafluorene; phenylsilane In 1,4-dioxane at 101℃; for 16h; Staudinger reduction reaction; Inert atmosphere; Stage #2: With water In 1,4-dioxane at 20℃; Staudinger reduction reaction; Inert atmosphere; | 99% |
With ammonium chloride; zinc In ethanol; water |
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; ammonium hydroxide In PEG1000-DIL; methyl cyclohexane at 60℃; for 3h; | 98% |
With ammonia fluess. Ammoniak; | |
With hydrogenchloride; hexamethylenetetramine 1) CH2Cl2, 12 h, 2) ethanol; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere 2: hydrazine hydrate / ethanol / 4 h / Inert atmosphere; Reflux View Scheme |
Conditions | Yield |
---|---|
With C19H34Cl2CoN2P; hydrogen; sodium ethanolate; sodium triethylborohydride In benzene at 135℃; under 22502.3 Torr; for 36h; Autoclave; | 98% |
With [Ru(H)(BH4)(CO)(PPh3)(3-(di-tert-butylphosphino)-N-((1-methyl-1H-imidazol-2 yl)methyl)propylamine)]; hydrogen In isopropyl alcohol at 50℃; for 3h; Inert atmosphere; Autoclave; | 98% |
With samarium diiodide; water In tetrahydrofuran for 0.0166667h; Ambient temperature; | 95% |
1-naphtylaldehyde oxime
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With (pyridine)(tetrahydroborato)zinc In tetrahydrofuran for 0.4h; Heating; | 98% |
With sodium hydrogensulfate monohydrate; molybdenum(V) chloride; sodium cyanoborohydride In ethanol for 2h; Reflux; | 97% |
With sodium tetrahydroborate at 20℃; for 0.0333333h; neat (no solvent, solid phase); | 96% |
4-methyl-N-(naphthalen-1-ylmethyl)benzenesulfonamide
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
Stage #1: 4-methyl-N-(naphthalen-1-ylmethyl)benzenesulfonamide With n-butyllithium In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With naphthalene; lithium In tetrahydrofuran at -78 - 25℃; Stage #3: With water In tetrahydrofuran | 94% |
Conditions | Yield |
---|---|
With N,N'-bis(salicylidene)-1,2-phenylene-diaminocobalt(II); ammonia; hydrogen In tetrahydrofuran; water at 120℃; for 24h; Autoclave; | 86% |
With lithium borohydride; Rink amine resin; water; trifluoroacetic acid; trimethyl orthoformate solid phase synthesis; 1) RT, 2) THF, 70 deg C, 5 h, 3) CH2Cl2, RT, 5 h; Yield given. Multistep reaction; | |
Multi-step reaction with 3 steps 1: NaBH4 / ethanol; H2O / 20 °C 2: 2.7 g / PPh3; DEAD / tetrahydrofuran / 22 h / 0 - 20 °C 3: NaBH4; AcOH / propan-1-ol; H2O / 5 h / 80 - 90 °C View Scheme |
1-Cyanonaphthalene
A
(naphth-1-yl)methylamine
B
1-(naphthalen-1-yl)-N-(naphthalen-1-ylmethyl)methanamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel dichloride In ethanol at 20℃; for 0.0833333h; | A 82% B 7% |
With tetralin; nickel at 190℃; under 15200 Torr; Hydrogenation; | |
With nickel; decalin at 190℃; under 15200 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
Stage #1: 1-naphthalene methanol With resin-bound CH2OCONHCOOtBu; diethylazodicarboxylate In tetrahydrofuran for 12h; Solid phase reaction; Mitsunobu reaction; Stage #2: With trifluoroacetic acid In 1,2-dichloro-ethane for 4h; Decarboxylation; | 80% |
Multi-step reaction with 2 steps 1: 2.7 g / PPh3; DEAD / tetrahydrofuran / 22 h / 0 - 20 °C 2: NaBH4; AcOH / propan-1-ol; H2O / 5 h / 80 - 90 °C View Scheme | |
Multi-step reaction with 2 steps 1: acetic acid; hydrogen bromide / 0.5 h / 0 °C 2: ammonia / ethanol; water / 4 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen bromide / acetic acid / 0.5 h / 0 °C 2: ammonium hydroxide / ethanol / 4 h / 20 °C View Scheme |
methanol
1-(azidomethyl)naphthalene
A
(naphth-1-yl)methylamine
B
N,N-dimethyl(naphthalen-1-yl)methanamine
C
N-methyl-1-naphthalenemethylamine
Conditions | Yield |
---|---|
With trans-RuCl(phenpyra-Me)(PPh3)2PF6; sodium hydroxide at 125℃; for 2.5h; Sealed tube; Inert atmosphere; Glovebox; | A 8 %Chromat. B 9 %Chromat. C 68% |
1-(azidomethyl)naphthalene
B
(naphth-1-yl)methylamine
C
1-naphthaldimine
D
1-Cyanonaphthalene
Conditions | Yield |
---|---|
With tert-butylethylene; [IrClH(1,3-bis((di-tert-butylphosphino)methyl)benzene)]; sodium t-butanolate In para-xylene at 200℃; for 7h; Sealed tube; | A n/a B n/a C n/a D 64% |
1-naphtylaldehyde oxime
A
(naphth-1-yl)methylamine
B
1-Methylnaphthalene
Conditions | Yield |
---|---|
With ammonium formate; palladium on activated charcoal In methanol at 50℃; for 0.416667h; | A 56% B 40% |
Conditions | Yield |
---|---|
With sodium hydroxide; benzyltrimethylazanium tribroman-2-uide In water for 5h; Ambient temperature; | 51% |
1-naphtylaldehyde oxime
A
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With methanesulfonic acid; zinc In acetonitrile at 25℃; reduction; | A 44% B n/a C n/a |
With titanium tetrachloride; zinc In tetrahydrofuran at 25℃; reduction; | A 5% B n/a C n/a |
Conditions | Yield |
---|---|
With sulfuric acid at 48℃; bei der elektrolytischen Reduktion an einer Bleikathode und hoher Stromdichte; |
Conditions | Yield |
---|---|
With chloroform Erhitzen des Reaktionsproduts mit Aethanol und wss. Salzsaeure; |
1-naphthalenecarbothioamide
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol; zinc |
1-Cyanonaphthalene
A
(naphth-1-yl)methylamine
B
1-naphthalenecarbothioamide
Conditions | Yield |
---|---|
With NaBH2S3 In tetrahydrofuran |
hydrogenchloride
ethanol
1-naphthalenecarbothioamide
A
(naphth-1-yl)methylamine
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With sodium hydroxide Ansaeuern mit Salzsaeure, Verdampfung den Alkohol und erhitzt man bis zur vollstaendig Loesung; |
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With hydrazine | |
With hydrogenchloride | |
With sodium hydroxide |
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With chloroamine; diethyl ether anschliessesndes Behandeln mit wss. Salzsaeure; |
A
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol; zinc |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; acetic acid In propan-1-ol; water at 80 - 90℃; for 5h; | |
With hydrazine hydrate In methanol for 1h; Heating; | |
With hydrazine In ethanol at 60℃; for 3h; | |
With hydrazine hydrate In ethanol for 4h; Inert atmosphere; Reflux; | 609 mg |
(α-naphthylmethyl)ammonium chloride
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With potassium carbonate In water; ethyl acetate |
(1-naphthyl)methylcarbamic acid
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
In toluene Heating; |
C23H18N2O2
A
(naphth-1-yl)methylamine
B
1-naphthaldehyde
C
1-Cyanonaphthalene
Conditions | Yield |
---|---|
In acetonitrile at 25 - 30℃; Irradiation; |
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Et3N / CH2Cl2 / 20 °C 2: acetonitrile / 25 - 30 °C / Irradiation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 99 percent / NH2OH*HCl; Na2CO3 / ethanol; H2O / 2 h / 20 °C 2: glacial AcOH; H2 / Pd/C / ethanol / 2 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide for 1h; | 100% |
6-bromohexanoyl chloride
(naphth-1-yl)methylamine
6-bromo-hexanoic acid (naphthalen-1-ylmethyl)-amide
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide for 1h; | 100% |
(naphth-1-yl)methylamine
2,4-dichloro-6-(3-methyl-butyl)-pyrimidine
2,4-dinaphthalen-1-ylmethylamino-6-isopentylpyrimidine
Conditions | Yield |
---|---|
at 95℃; for 16h; Inert atmosphere; Autoclave; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; Sonication; | 100% |
Conditions | Yield |
---|---|
With copper(I) chloride; 4 A molecular sieve; oxygen In pyridine at 60℃; for 24h; | 99% |
With dmap; copper(l) iodide; 9-azabicyclo[3.3.1]nonane N-oxyl; oxygen; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; under 760.051 Torr; for 15h; Reagent/catalyst; | 98% |
With potassium hydroxide; nickel copper formate; (Bu4N)2S2O8 In 1,2-dichloro-ethane at 20℃; for 12h; Oxidation; | 90% |
ethyl 2-(pyridinyl-2)acetate
(naphth-1-yl)methylamine
ethyl 3-(naphthalen-1-yl)imidazo[1,5-α]pyridine-1-carboxylate
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; N-iodo-succinimide In N,N-dimethyl acetamide; water at 20℃; for 12h; | 99% |
With sulfur In dimethyl sulfoxide at 110℃; for 2h; Sealed tube; | 84% |
(naphth-1-yl)methylamine
Boc-Phe(p-F)
Conditions | Yield |
---|---|
Stage #1: (naphth-1-yl)methylamine; Boc-Phe(p-F) With 1-hydroxy-7-aza-benzotriazole; HATU In N,N-dimethyl-formamide at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0℃; for 1h; | 99% |
Stage #1: (naphth-1-yl)methylamine; Boc-Phe(p-F) With 1-hydroxy-7-aza-benzotriazole; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0℃; for 1h; | 99% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; | |
With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0℃; for 1.5h; |
Conditions | Yield |
---|---|
With iodine; sodium acetate In 1,2-dichloro-ethane for 6h; Reflux; | 99% |
With copper(II) acetate monohydrate In N,N-dimethyl-formamide at 110℃; for 8h; | 90% |
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
at 145℃; for 2h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With magnesium sulfate In ethanol for 20h; Reflux; | 99% |
In chloroform at 40℃; for 9h; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0℃; for 3h; | 99% |
(naphth-1-yl)methylamine
methyl 5-(N,N-dimethylamino)-2,4-pentadienoate
Conditions | Yield |
---|---|
In tetrahydrofuran for 120h; Heating; | 98% |
(naphth-1-yl)methylamine
dimethyl acetylenedicarboxylate
malonoyl dichloride
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 98% |
oxalyl dichloride
(naphth-1-yl)methylamine
dimethyl acetylenedicarboxylate
C19H17NO7
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 98% |
(naphth-1-yl)methylamine
chloroacetyl chloride
2-chloro-N-naphthalen-1-yl-methyl-acetamide
Conditions | Yield |
---|---|
With potassium carbonate In water; ethyl acetate at 20℃; for 2h; | 98% |
(2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoic acid
(naphth-1-yl)methylamine
benzyl (5S)-6-[(1-naphthylmethyl)amino]-6-oxo-5-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexylcarbamate
Conditions | Yield |
---|---|
Stage #1: (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoic acid With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In dichloromethane at 20℃; for 0.166667h; Stage #2: (naphth-1-yl)methylamine In dichloromethane for 1h; pH=8; | 98% |
(naphth-1-yl)methylamine
2-(2'-phenylethynyl)benzoic acid
3-benzyl-3-hydroxy-2-(naphthalen-1-ylmethyl)isoindolin-1-one
Conditions | Yield |
---|---|
Stage #1: 2-(2'-phenylethynyl)benzoic acid With tetrabutylammonium acetate In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Stage #2: (naphth-1-yl)methylamine In water at 100℃; for 0.333333h; Microwave irradiation; Inert atmosphere; regioselective reaction; | 98% |
(naphth-1-yl)methylamine
2-((4-methoxyphenyl)ethynyl)benzoic acid
3-hydroxy-3-(4-methoxybenzyl)-2-(naphthalen-1-ylmethyl)isoindolin-1-one
Conditions | Yield |
---|---|
Stage #1: 2-((4-methoxyphenyl)ethynyl)benzoic acid With tetrabutylammonium acetate In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Stage #2: (naphth-1-yl)methylamine In water at 100℃; for 0.333333h; Microwave irradiation; Inert atmosphere; regioselective reaction; | 98% |
Conditions | Yield |
---|---|
With N,O-bis-(trimethylsilyl)-acetamide; bis(η3-allyl-μ-chloropalladium(II)); N-[(S)-1-(2-(diphenylphosphino)phenyl)ethyl]-1,7,7-trimethylbicyclo[2,2,1]heptan-2-imine In toluene at 20℃; enantioselective reaction; | 98% |
1-(2-nitrophenyl)-1H-pyrrole
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With water; pyrographite at 140℃; for 20h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
In tetrahydrofuran for 48h; | 98% |
(naphth-1-yl)methylamine
2'-azido-6-chloro-2'-deoxyadenosine
2'-azido-2'-deoxy-N6-(1-naphthylmethyl)adenosine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In propan-1-ol at 50℃; for 16h; Substitution; aminolysis; | 97% |
In propan-1-ol at 50℃; for 16h; |
Conditions | Yield |
---|---|
With dmap In methanol; CH3Cl; dichloromethane | 97% |
(naphth-1-yl)methylamine
methyl chloroformate
methyl N-(1-naphthalenylmethyl)carbamate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 2h; | 97% |
With triethylamine at 20℃; for 2h; |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 97% |
N-tertiarybutoxycarbonyl-β-alanine N-hydroxysuccinimide ester
(naphth-1-yl)methylamine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2h; | 97% |
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