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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

o-Toluoyl chloride

Cas:933-88-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance Colorless to light yellow liquid Colorless to light yellow liquid PH

Top purity o-Toluoyl chloride with high quality and best price cas:933-88-0

Cas:933-88-0

Min.Order:1 Gram

FOB Price: $2.0 / 5.0

Type:Manufacturers

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality O-Toluoyl Chloride supplier in China

Cas:933-88-0

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages for o-Toluoyl chloride Cas 933-88-0 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Colorless or pale yellow liquid Storage:N/A Package:200kg/drum Applicat

High quality o-Toluoyl chloride Cas 933-88-0 with best price

Cas:933-88-0

Min.Order:1 Metric Ton

FOB Price: $6500.0 / 7000.0

Type:Trading Company

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EAST CHEMSOURCES LIMITED

o-methyl benzoyl chloride EINEC RN: 213-273-8 Molecular formula: C8H7OCl Molecular weight: 154.5 Boiling point: 8-90 °C12 mm Hg(lit.) Appearan

o-methyl benzoyl chloride

Cas:933-88-0

Min.Order:1 Kilogram

FOB Price: $2.0 / 3.0

Type:Manufacturers

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

O-methylbenzoyl chloride

Cas:933-88-0

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

o-Toluoyl chloride

Cas:933-88-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

o-Toluoyl chloride-

Cas:933-88-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 933-88-0 with best quality

Cas:933-88-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

o-Toluoyl chloride CAS933-88-0/37808-28-9

Cas:933-88-0

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd

o-Toluoyl chloride CAS933-88-0

Cas:933-88-0

Min.Order:1 Metric Ton

FOB Price: $34.0 / 45.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name:o-Toluoyl chloride CAS:933-88-0 MF:C8H7ClO MW:154.59 Boiling point:88-90 °C Density:1.185 g/mL Product Name:o-Toluoyl chloride CAS:933-88-0 MF:C8H7ClO MW:154.59 Boiling point:88-90 °C

o-Toluoyl chloride

Cas:933-88-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzoyl chloride,2-methyl- 933-88-0

Cas:933-88-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: o-Toluoyl chloride CAS: 933-88-0 MF: C8H7ClO MW: 154.59 EINECS: 213-273-8 Mol File: 933-88-0.mol o-Toluoyl chloride Structure o-Toluoyl chloride Chemical Properties Melting point 159.5-160.9 °C(Solv: ligroine

o-Toluoyl chloride

Cas:933-88-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benzoyl chloride,2-methyl-

Cas:933-88-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:933-88-0

Cas:933-88-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biological Technology Co., Ltd. is specialize in the production of chemical raw materials and reagents,located in Shijiazhuang, Hebei Province. In recent decades, under the efforts of all staff, in Shandong, Henan, Guangdong and many othe

o-Toluoyl chloride CAS 933-88-0

Cas:933-88-0

Min.Order:1 Kilogram

FOB Price: $20.0 / 40.0

Type:Trading Company

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures

O-Toluoylchloride

Cas:933-88-0

Min.Order:1 Kilogram

FOB Price: $6.0 / 10.0

Type:Lab/Research institutions

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Lonwin Chemical Group Limited

o-Toluoyl chloride CAS: 933-88-0 Specification Items Specification Result Assay ≥98.5% 99.37% Appearance

Factory supply o-Toluoyl chloride

Cas:933-88-0

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

O-Toluoyl Chloride

Cas:933-88-0

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Lorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h

o-Toluoyl chloride 933-88-0

Cas:933-88-0

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

o-Toluoyl chloride

Cas:933-88-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

o-Toluoyl chloride

Cas:933-88-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

o-Toluoyl chloride

Cas:933-88-0

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply o-Toluoyl chloride

Cas:933-88-0

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

o-Toluoyl chloride

Cas:933-88-0

Min.Order:1 Gram

Negotiable

Type:Other

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

o-Toluoyl chloride/High quality/Best price

Cas:933-88-0

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Hangzhou Lingrui Chemical Co.,Ltd.

o-Toluoyl chlorideAppearance:Colorless transparent liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(

o-Toluoyl chloride

Cas:933-88-0

Min.Order:1 Gram

Negotiable

Type:Other

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

o-Toluoyl chloride

Cas:933-88-0

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colorless or light yellow liquid Storage:store at RT Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermediates Transportation: as per your req

o-Toluoyl chloride

Cas:933-88-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Synthetic route

ortho-methylbenzoic acid
118-90-1

ortho-methylbenzoic acid

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
With oxalyl dichloride In benzene at 20℃; for 14h;100%
With thionyl chloride Reflux;100%
With thionyl chloride; N,N-dimethyl-formamide at 90℃; for 3h; Concentration; Reagent/catalyst; Temperature;99.7%
ortho-methylphenyl iodide
615-37-2

ortho-methylphenyl iodide

carbon monoxide
201230-82-2

carbon monoxide

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
With bis(tri-t-butylphosphine)palladium(0); benzyltriphenylphosphonium chloride In toluene at 110℃; under 38002.6 Torr; for 24h; Glovebox; Autoclave; Inert atmosphere;93%
2-methyl-benzyl alcohol
89-95-2

2-methyl-benzyl alcohol

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
With o-chlorobenzoyl chloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 12h;70%
ortho-methylphenyl iodide
615-37-2

ortho-methylphenyl iodide

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere;A n/a
B 68%
o-xylene
95-47-6

o-xylene

A

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

B

Phthaloyl dichloride
88-95-9

Phthaloyl dichloride

Conditions
ConditionsYield
Stage #1: o-xylene With ruthenium(II) chloride; C88H48Cl8Fe2N8O; oxygen at 185℃; under 10501.1 Torr;
Stage #2: With thionyl chloride Reagent/catalyst; Temperature; Pressure;
A 63.1%
B 10.1%
Stage #1: o-xylene With ruthenium(II) chloride; C88H48Cl8Fe2N8O; oxygen at 185℃; under 10501.1 Torr;
Stage #2: With thionyl chloride Reagent/catalyst; Temperature; Pressure;
A 24.1%
B 38.7%
2-methylbenzoic anhydride
607-86-3

2-methylbenzoic anhydride

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
With phosphorus pentachloride; trichlorophosphate
ortho-tolylmagnesium bromide
932-31-0

ortho-tolylmagnesium bromide

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diethyl ether / Einleiten von Kohlendioxid
2: thionyl chloride
View Scheme
o-tolylmagnesium iodide

o-tolylmagnesium iodide

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diethyl ether / Einleiten von Kohlendioxid
2: thionyl chloride
View Scheme
ortho-methylbenzoic acid
118-90-1

ortho-methylbenzoic acid

oxalyl dichloride
79-37-8

oxalyl dichloride

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
In dichloromethane
ortho-methylbenzoic acid
118-90-1

ortho-methylbenzoic acid

2-(4,5-Dihydro-1,3-oxazol-2-yl)aniline
3416-93-1

2-(4,5-Dihydro-1,3-oxazol-2-yl)aniline

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide
2-methylphenyl aldehyde
529-20-4

2-methylphenyl aldehyde

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
With tert.-butylhydroperoxide; N-chloro-succinimide; tris(2,2'-bipyridyl)ruthenium dichloride In acetonitrile at 20℃; for 24h; Sealed tube; Irradiation;
2-Methyl-benzoic acid methyl ester
89-71-4

2-Methyl-benzoic acid methyl ester

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydroxide / methanol / 60 °C / pH 3 / Schlenk technique; Inert atmosphere
2: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 17 h / 0 - 20 °C / Schlenk technique; Inert atmosphere
View Scheme
ortho-methylphenyl iodide
615-37-2

ortho-methylphenyl iodide

terephthaloyl chloride
100-20-9

terephthaloyl chloride

A

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

B

4-iodobenzoic acid chloride
1711-02-0

4-iodobenzoic acid chloride

Conditions
ConditionsYield
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 110℃; for 20h; Sealed tube; Inert atmosphere;A 53 %Spectr.
B n/a
1,3-Benzothiazole
95-16-9

1,3-Benzothiazole

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

2-Cyano-3-o-toluoyl-2,3-dihydrobenzothiazole

2-Cyano-3-o-toluoyl-2,3-dihydrobenzothiazole

Conditions
ConditionsYield
With aluminium trichloride In dichloromethane100%
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

N-(1-hydroxy-2-methylpropan-2-yl)-2-methylbenzamide
95217-40-6

N-(1-hydroxy-2-methylpropan-2-yl)-2-methylbenzamide

Conditions
ConditionsYield
In dichloromethane at 0℃; for 0.5h;100%
With triethylamine In dichloromethane at 0℃;
With triethylamine In dichloromethane at 0℃; for 3h; Inert atmosphere;
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

dimethyl amine
124-40-3

dimethyl amine

N,N,2-trimethylbenzamide
6639-19-6

N,N,2-trimethylbenzamide

Conditions
ConditionsYield
100%
In water; toluene
In diethyl ether at 20℃; for 16h;
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

aniline
62-53-3

aniline

2-methyl-N-phenylbenzamide
7055-03-0

2-methyl-N-phenylbenzamide

Conditions
ConditionsYield
In diethyl ether Ambient temperature;100%
With pyridine; dmap at 0 - 20℃;99%
With triethylamine In dichloromethane at 0 - 20℃;96%
1-bromo-5,6,7,8-tetrahydronaphthalen-2-ol
32337-86-3

1-bromo-5,6,7,8-tetrahydronaphthalen-2-ol

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

2-benzyloxy-1-bromo-5,6,7,8-tetrahydronaphthalene
142626-67-3

2-benzyloxy-1-bromo-5,6,7,8-tetrahydronaphthalene

Conditions
ConditionsYield
With triethylamine In dichloromethane for 1h;100%
With triethylamine In dichloromethane
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

L-proline
147-85-3

L-proline

N-(2-methylbenzoyl)-L-proline

N-(2-methylbenzoyl)-L-proline

Conditions
ConditionsYield
With sodium hydroxide for 0.5h;100%
With sodium hydroxide In tetrahydrofuran; water at 0 - 20℃;0.77 g
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

1-(4-aminobenzoyl)-9-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137983-89-2

1-(4-aminobenzoyl)-9-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

9-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137978-31-5

9-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

1-(4-aminobenzoyl)-8-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137984-96-4

1-(4-aminobenzoyl)-8-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

8-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137977-41-4

8-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

1-(4-aminobenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137984-95-3

1-(4-aminobenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

7-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137977-35-6

7-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

1-(4-amino-2-methoxybenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137976-75-1

1-(4-amino-2-methoxybenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

7-chloro-1-[2-methoxy-4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137974-15-3

7-chloro-1-[2-methoxy-4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation;100%
2,6-bis-([4R,5R]-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-pyridine
863491-46-7

2,6-bis-([4R,5R]-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-pyridine

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

2,6-bis-(1-(2-methyl-benzoyl)-[4R,5R]-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-pyridine

2,6-bis-(1-(2-methyl-benzoyl)-[4R,5R]-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-pyridine

Conditions
ConditionsYield
With dmap In dichloromethane at 0 - 20℃;100%
With dmap In dichloromethane at 20℃; for 12h;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

1-(2-methylbenzoyl)-2-methylaziridine
21384-42-9

1-(2-methylbenzoyl)-2-methylaziridine

Conditions
ConditionsYield
With sodium hydroxide In diethyl ether at 0℃;100%
With sodium hydroxide In diethyl ether; water at 0℃; Schotten-Baumann reaction;
3-methylbenzyl alcohol
587-03-1

3-methylbenzyl alcohol

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

3-methylbenzyl 2'-methylbenzoate
1070881-26-3

3-methylbenzyl 2'-methylbenzoate

Conditions
ConditionsYield
With pyridine at 0℃; for 1.5h;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

N-butylamine
109-73-9

N-butylamine

N-(n-butyl)-2-methylbenzamide

N-(n-butyl)-2-methylbenzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 2.5h; Inert atmosphere;100%
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere;86%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

(2S)-N-phenylpyrrolidine-2-carboxamide
25746-83-2, 64030-43-9, 104261-87-2

(2S)-N-phenylpyrrolidine-2-carboxamide

(S)-N-(2-methylbenzoyl)proline anilide
1415831-64-9

(S)-N-(2-methylbenzoyl)proline anilide

Conditions
ConditionsYield
With triethylamine In Dichlorofluoromethane at 20℃; Inert atmosphere;100%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Cyclopentamine
1003-03-8

Cyclopentamine

N-cyclopentyl-2-methylbenzamide
123862-57-7

N-cyclopentyl-2-methylbenzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere;100%
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere;94%
4-trifluoromethylphenylamine
455-14-1

4-trifluoromethylphenylamine

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

2-methyl-N-(4-(trifluoromethyl)phenyl)benzamide

2-methyl-N-(4-(trifluoromethyl)phenyl)benzamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0 - 20℃; for 3h;100%
N-aminopyridin-1-ium iodide
6295-87-0

N-aminopyridin-1-ium iodide

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

1-(2-methyl-benzoylamino)-pyridinium betaine
36048-80-3

1-(2-methyl-benzoylamino)-pyridinium betaine

Conditions
ConditionsYield
With sodium hydroxide at 25℃; for 24h;99.9%
4-methoxy-aniline
104-94-9

4-methoxy-aniline

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

α-(p-anisidino)-o-tolualdehyde
55814-36-3

α-(p-anisidino)-o-tolualdehyde

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃; for 1h;99%
With sodium hydroxide for 0.25h;55%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 6h;
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

1-(4-amino-2-chlorobenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137978-00-8

1-(4-amino-2-chlorobenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

7-chloro-1-[2-chloro-4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
137973-86-5

7-chloro-1-[2-chloro-4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation;99%
2-Chloroethanesulfonyl chloride
1622-32-8

2-Chloroethanesulfonyl chloride

4-fluoro-2-phenethylamine
1583-88-6

4-fluoro-2-phenethylamine

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

4-(4-((p-methylbenzylamino)methyl)-3-methoxyphenoxy)butyryl AM resin

4-(4-((p-methylbenzylamino)methyl)-3-methoxyphenoxy)butyryl AM resin

N-[2-(4-fluoro-phenyl)-ethyl]-2-methyl-N-[2-(4-methyl-benzylsulfamoyl)-ethyl]-benzamide

N-[2-(4-fluoro-phenyl)-ethyl]-2-methyl-N-[2-(4-methyl-benzylsulfamoyl)-ethyl]-benzamide

Conditions
ConditionsYield
Multistep reaction;99%
(1R,2S)-norephedrine
492-41-1

(1R,2S)-norephedrine

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

(1R,2S)-2-o-toluamide-1-phenylpropanol
696659-64-0

(1R,2S)-2-o-toluamide-1-phenylpropanol

Conditions
ConditionsYield
With potassium hydroxide In dichloromethane; water at 0 - 20℃; for 2.5h;99%
L-Phenylalaninol
3182-95-4

L-Phenylalaninol

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

(2S)-2-o-toluamide-3-phenylpropanol
497954-01-5

(2S)-2-o-toluamide-3-phenylpropanol

Conditions
ConditionsYield
With potassium hydroxide In dichloromethane at 0 - 20℃;99%
With triethylamine In tetrahydrofuran for 1h;
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

phenylacetylene
536-74-3

phenylacetylene

l

l

(5-phenyl-2H-1,2,3-triazol-4-yl)(o-tolyl)methanone
1171248-95-5

(5-phenyl-2H-1,2,3-triazol-4-yl)(o-tolyl)methanone

Conditions
ConditionsYield
Stage #1: ortho-toluoyl chloride; phenylacetylene; l With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 1h; Sonogashira coupling; Inert atmosphere; Ultrasonic;
Stage #2: With sodium azide In dimethyl sulfoxide at 20℃; for 1h;
99%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

3,5-Dichloroaniline
626-43-7

3,5-Dichloroaniline

1-(3,5-dichlorophenyl)-3-(o-tolyl)urea
97146-53-7

1-(3,5-dichlorophenyl)-3-(o-tolyl)urea

Conditions
ConditionsYield
Stage #1: ortho-toluoyl chloride With pyridine; trimethylsilylazide In N,N-dimethyl-formamide at 20℃; Curtius rearrangement; Microflow reaction; Inert atmosphere;
Stage #2: 3,5-Dichloroaniline With acetic acid In N,N-dimethyl-formamide at 110℃; Microflow reaction; Inert atmosphere;
99%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

benzyl alcohol
100-51-6

benzyl alcohol

N-benzyloxycarbonyl-2-methylaniline
108714-89-2

N-benzyloxycarbonyl-2-methylaniline

Conditions
ConditionsYield
Stage #1: ortho-toluoyl chloride With pyridine; trimethylsilylazide In N,N-dimethyl-formamide at 20℃; Curtius rearrangement; Microflow reaction; Inert atmosphere;
Stage #2: benzyl alcohol With acetic acid In N,N-dimethyl-formamide at 110℃; Microflow reaction; Inert atmosphere;
99%
1-(hydroxyethyl)-2-(methylamino)-1,2,3,6,7,12b-hexahydroindolo[2,3-a]quinolizin-4(12H)-one

1-(hydroxyethyl)-2-(methylamino)-1,2,3,6,7,12b-hexahydroindolo[2,3-a]quinolizin-4(12H)-one

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

N-(3-(1-hydroxyethyl)-4-oxo-1,2,3,4,6,7,12,12b-octahydroindolo[2,3-a]quinolizin-2-yl)-N-2-dimethylbenzamide

N-(3-(1-hydroxyethyl)-4-oxo-1,2,3,4,6,7,12,12b-octahydroindolo[2,3-a]quinolizin-2-yl)-N-2-dimethylbenzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane for 0.75h; Inert atmosphere;99%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

Propargylamine
2450-71-7

Propargylamine

2-methyl-N-(prop-2-yn-1-yl)benzamide
1090993-70-6

2-methyl-N-(prop-2-yn-1-yl)benzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 4h;99%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 3.25h; Inert atmosphere;82%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 5.25h; Inert atmosphere;
With dmap; triethylamine In dichloromethane at 0 - 20℃;
With dmap; triethylamine In dichloromethane at 0 - 20℃;
m-Anisidine
536-90-3

m-Anisidine

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

2-methyl-N-(3-methoxyphenyl)-benzamide
55814-35-2

2-methyl-N-(3-methoxyphenyl)-benzamide

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 18h; Inert atmosphere;99%
With triethylamine In dichloromethane at 0 - 20℃;90%
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