DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:933-88-0
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inquiryItems Standard Result Appearance Colorless to light yellow liquid Colorless to light yellow liquid PH
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inquiryUnique advantages for o-Toluoyl chloride Cas 933-88-0 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Colorless or pale yellow liquid Storage:N/A Package:200kg/drum Applicat
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inquiryo-methyl benzoyl chloride EINEC RN: 213-273-8 Molecular formula: C8H7OCl Molecular weight: 154.5 Boiling point: 8-90 °C12 mm Hg(lit.) Appearan
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryProduct Name:o-Toluoyl chloride CAS:933-88-0 MF:C8H7ClO MW:154.59 Boiling point:88-90 °C Density:1.185 g/mL Product Name:o-Toluoyl chloride CAS:933-88-0 MF:C8H7ClO MW:154.59 Boiling point:88-90 °C
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inquiryProduct Name: o-Toluoyl chloride CAS: 933-88-0 MF: C8H7ClO MW: 154.59 EINECS: 213-273-8 Mol File: 933-88-0.mol o-Toluoyl chloride Structure o-Toluoyl chloride Chemical Properties Melting point 159.5-160.9 °C(Solv: ligroine
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryo-Toluoyl chloride CAS: 933-88-0 Specification Items Specification Result Assay ≥98.5% 99.37% Appearance
Cas:933-88-0
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Lorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryo-Toluoyl chlorideAppearance:Colorless transparent liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(
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inquirySuperior quality, moderate price & quick delivery. Appearance:colorless or light yellow liquid Storage:store at RT Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermediates Transportation: as per your req
Conditions | Yield |
---|---|
With oxalyl dichloride In benzene at 20℃; for 14h; | 100% |
With thionyl chloride Reflux; | 100% |
With thionyl chloride; N,N-dimethyl-formamide at 90℃; for 3h; Concentration; Reagent/catalyst; Temperature; | 99.7% |
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); benzyltriphenylphosphonium chloride In toluene at 110℃; under 38002.6 Torr; for 24h; Glovebox; Autoclave; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With o-chlorobenzoyl chloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 12h; | 70% |
ortho-methylphenyl iodide
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
ortho-toluoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 68% |
Conditions | Yield |
---|---|
Stage #1: o-xylene With ruthenium(II) chloride; C88H48Cl8Fe2N8O; oxygen at 185℃; under 10501.1 Torr; Stage #2: With thionyl chloride Reagent/catalyst; Temperature; Pressure; | A 63.1% B 10.1% |
Stage #1: o-xylene With ruthenium(II) chloride; C88H48Cl8Fe2N8O; oxygen at 185℃; under 10501.1 Torr; Stage #2: With thionyl chloride Reagent/catalyst; Temperature; Pressure; | A 24.1% B 38.7% |
Conditions | Yield |
---|---|
With phosphorus pentachloride; trichlorophosphate |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether / Einleiten von Kohlendioxid 2: thionyl chloride View Scheme |
ortho-toluoyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether / Einleiten von Kohlendioxid 2: thionyl chloride View Scheme |
ortho-methylbenzoic acid
oxalyl dichloride
N,N-dimethyl-formamide
ortho-toluoyl chloride
Conditions | Yield |
---|---|
In dichloromethane |
ortho-methylbenzoic acid
2-(4,5-Dihydro-1,3-oxazol-2-yl)aniline
ortho-toluoyl chloride
Conditions | Yield |
---|---|
With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; N-chloro-succinimide; tris(2,2'-bipyridyl)ruthenium dichloride In acetonitrile at 20℃; for 24h; Sealed tube; Irradiation; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydroxide / methanol / 60 °C / pH 3 / Schlenk technique; Inert atmosphere 2: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 17 h / 0 - 20 °C / Schlenk technique; Inert atmosphere View Scheme |
ortho-methylphenyl iodide
terephthaloyl chloride
A
ortho-toluoyl chloride
B
4-iodobenzoic acid chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 110℃; for 20h; Sealed tube; Inert atmosphere; | A 53 %Spectr. B n/a |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane | 100% |
2-Amino-2-methyl-1-propanol
ortho-toluoyl chloride
N-(1-hydroxy-2-methylpropan-2-yl)-2-methylbenzamide
Conditions | Yield |
---|---|
In dichloromethane at 0℃; for 0.5h; | 100% |
With triethylamine In dichloromethane at 0℃; | |
With triethylamine In dichloromethane at 0℃; for 3h; Inert atmosphere; |
Conditions | Yield |
---|---|
100% | |
In water; toluene | |
In diethyl ether at 20℃; for 16h; |
Conditions | Yield |
---|---|
In diethyl ether Ambient temperature; | 100% |
With pyridine; dmap at 0 - 20℃; | 99% |
With triethylamine In dichloromethane at 0 - 20℃; | 96% |
1-bromo-5,6,7,8-tetrahydronaphthalen-2-ol
ortho-toluoyl chloride
2-benzyloxy-1-bromo-5,6,7,8-tetrahydronaphthalene
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 1h; | 100% |
With triethylamine In dichloromethane |
Conditions | Yield |
---|---|
With sodium hydroxide for 0.5h; | 100% |
With sodium hydroxide In tetrahydrofuran; water at 0 - 20℃; | 0.77 g |
ortho-toluoyl chloride
1-(4-aminobenzoyl)-9-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
9-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation; | 100% |
ortho-toluoyl chloride
1-(4-aminobenzoyl)-8-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
8-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation; | 100% |
ortho-toluoyl chloride
1-(4-aminobenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
7-chloro-1-[4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation; | 100% |
ortho-toluoyl chloride
1-(4-amino-2-methoxybenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
7-chloro-1-[2-methoxy-4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation; | 100% |
2,6-bis-([4R,5R]-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-pyridine
ortho-toluoyl chloride
Conditions | Yield |
---|---|
With dmap In dichloromethane at 0 - 20℃; | 100% |
With dmap In dichloromethane at 20℃; for 12h; | 100% |
ortho-toluoyl chloride
2-Methylaziridine
1-(2-methylbenzoyl)-2-methylaziridine
Conditions | Yield |
---|---|
With sodium hydroxide In diethyl ether at 0℃; | 100% |
With sodium hydroxide In diethyl ether; water at 0℃; Schotten-Baumann reaction; |
3-methylbenzyl alcohol
ortho-toluoyl chloride
3-methylbenzyl 2'-methylbenzoate
Conditions | Yield |
---|---|
With pyridine at 0℃; for 1.5h; | 100% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2.5h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere; | 86% |
ortho-toluoyl chloride
(2S)-N-phenylpyrrolidine-2-carboxamide
(S)-N-(2-methylbenzoyl)proline anilide
Conditions | Yield |
---|---|
With triethylamine In Dichlorofluoromethane at 20℃; Inert atmosphere; | 100% |
ortho-toluoyl chloride
Cyclopentamine
N-cyclopentyl-2-methylbenzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0 - 20℃; for 3h; | 100% |
N-aminopyridin-1-ium iodide
ortho-toluoyl chloride
1-(2-methyl-benzoylamino)-pyridinium betaine
Conditions | Yield |
---|---|
With sodium hydroxide at 25℃; for 24h; | 99.9% |
4-methoxy-aniline
ortho-toluoyl chloride
α-(p-anisidino)-o-tolualdehyde
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; for 1h; | 99% |
With sodium hydroxide for 0.25h; | 55% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 6h; |
ortho-toluoyl chloride
1-(4-amino-2-chlorobenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
7-chloro-1-[2-chloro-4-[(2-methylbenzoyl)amino]benzoyl]-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1.5h; Acylation; | 99% |
2-Chloroethanesulfonyl chloride
4-fluoro-2-phenethylamine
ortho-toluoyl chloride
Conditions | Yield |
---|---|
Multistep reaction; | 99% |
(1R,2S)-norephedrine
ortho-toluoyl chloride
(1R,2S)-2-o-toluamide-1-phenylpropanol
Conditions | Yield |
---|---|
With potassium hydroxide In dichloromethane; water at 0 - 20℃; for 2.5h; | 99% |
L-Phenylalaninol
ortho-toluoyl chloride
(2S)-2-o-toluamide-3-phenylpropanol
Conditions | Yield |
---|---|
With potassium hydroxide In dichloromethane at 0 - 20℃; | 99% |
With triethylamine In tetrahydrofuran for 1h; |
ortho-toluoyl chloride
phenylacetylene
(5-phenyl-2H-1,2,3-triazol-4-yl)(o-tolyl)methanone
Conditions | Yield |
---|---|
Stage #1: ortho-toluoyl chloride; phenylacetylene; l With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 1h; Sonogashira coupling; Inert atmosphere; Ultrasonic; Stage #2: With sodium azide In dimethyl sulfoxide at 20℃; for 1h; | 99% |
ortho-toluoyl chloride
3,5-Dichloroaniline
1-(3,5-dichlorophenyl)-3-(o-tolyl)urea
Conditions | Yield |
---|---|
Stage #1: ortho-toluoyl chloride With pyridine; trimethylsilylazide In N,N-dimethyl-formamide at 20℃; Curtius rearrangement; Microflow reaction; Inert atmosphere; Stage #2: 3,5-Dichloroaniline With acetic acid In N,N-dimethyl-formamide at 110℃; Microflow reaction; Inert atmosphere; | 99% |
ortho-toluoyl chloride
benzyl alcohol
N-benzyloxycarbonyl-2-methylaniline
Conditions | Yield |
---|---|
Stage #1: ortho-toluoyl chloride With pyridine; trimethylsilylazide In N,N-dimethyl-formamide at 20℃; Curtius rearrangement; Microflow reaction; Inert atmosphere; Stage #2: benzyl alcohol With acetic acid In N,N-dimethyl-formamide at 110℃; Microflow reaction; Inert atmosphere; | 99% |
ortho-toluoyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 0.75h; Inert atmosphere; | 99% |
ortho-toluoyl chloride
Propargylamine
2-methyl-N-(prop-2-yn-1-yl)benzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 4h; | 99% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 3.25h; Inert atmosphere; | 82% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 5.25h; Inert atmosphere; | |
With dmap; triethylamine In dichloromethane at 0 - 20℃; | |
With dmap; triethylamine In dichloromethane at 0 - 20℃; |
m-Anisidine
ortho-toluoyl chloride
2-methyl-N-(3-methoxyphenyl)-benzamide
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 18h; Inert atmosphere; | 99% |
With triethylamine In dichloromethane at 0 - 20℃; | 90% |
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