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inquirysuperior quality Appearance:clear yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportatio
Phthaloyl dichloride Chemical Properties Melting point 6-12 °C(lit.) Boiling point 269-271 °C(lit.) density 1.409 g/mL at 25 °C(lit.) vapor pressure 30 mm Hg ( 47 °C) refractiv
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
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88-95-9 Phthaloyl dichloride Application:88-95-9 Phthaloyl dichloride
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
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inquiryPreview CBNumber: CB7273160 Chemical Name: Phthaloyl dichloride Molecular Formula: C8
Watson International Ltd' has a very strong R&D and technical capacity supported by FCAD's platform. The subsidiaries under FCAD Group have accumulated much know-how of different fine chemical branches. For example, Apnoke Scientific L
Phthaloyl dichloride Storage: Keep container closed when not in use. Store in a cool, dry, well-ventilated area away from incompatible substances. C… Appearance:Colorless to light yellow liquid Storage:Avoid light ventilated dry place Packag
Conditions | Yield |
---|---|
With phosgene; N,N-dibutylformamide In toluene at 70℃; for 7.5h; Product distribution / selectivity; | 97.8% |
With phosgene; N-methyl-N-stearylformamide In toluene at 75℃; for 7.5h; Product distribution / selectivity; | 95% |
With phosgene; N,N-dibutylformamide In toluene at 70℃; for 8h; Product distribution / selectivity; | 91% |
phthalic anhydride
4-chlorotrichloromethylbenzene
A
4-chloro-benzoyl chloride
B
Phthaloyl dichloride
Conditions | Yield |
---|---|
zirconium(IV) chloride at 160℃; for 6h; | A 93% B 70% |
phthalic anhydride
A
N,N-dibutylcarbamoyl chloride
B
Phthaloyl dichloride
Conditions | Yield |
---|---|
With phosgene; N,N-dibutylformamide In toluene at 70℃; for 7.5h; Product distribution / selectivity; | A 0.9 %Chromat. B 89.3% |
Conditions | Yield |
---|---|
Stage #1: o-xylene With ruthenium(II) chloride; C88H48Cl8Fe2N8O; oxygen at 185℃; under 10501.1 Torr; Stage #2: With thionyl chloride Reagent/catalyst; Temperature; Pressure; | A 63.1% B 10.1% |
Stage #1: o-xylene With ruthenium(II) chloride; C88H48Cl8Fe2N8O; oxygen at 185℃; under 10501.1 Torr; Stage #2: With thionyl chloride Reagent/catalyst; Temperature; Pressure; | A 24.1% B 38.7% |
Conditions | Yield |
---|---|
With zinc(II) chloride at 220 - 300℃; |
Conditions | Yield |
---|---|
With zinc(II) chloride at 220 - 300℃; |
Conditions | Yield |
---|---|
With zinc(II) chloride at 220 - 300℃; |
Conditions | Yield |
---|---|
With zinc(II) chloride at 110 - 200℃; |
Conditions | Yield |
---|---|
at 130℃; Kinetik der Umwandlung; | |
durch Destillation; | |
at 100℃; | |
With hydrogenchloride | |
at 130℃; |
3-thioxo-3H-isobenzofuran-1-one
Phthaloyl dichloride
Conditions | Yield |
---|---|
With chlorine at 245℃; |
Conditions | Yield |
---|---|
With phosphorus pentachloride | |
With thionyl chloride | |
With thionyl chloride at 60 - 65℃; |
2,5-dioxo-2,5-dihydrobenzotellurophene
Phthaloyl dichloride
Conditions | Yield |
---|---|
With chlorine In tetrachloromethane Yield given; |
2-phenyl-isophosphindole-1,3-dione
Phthaloyl dichloride
Conditions | Yield |
---|---|
With chlorine In diethyl ether |
phthalic anhydride
phosphorus pentachloride
Phthaloyl dichloride
Conditions | Yield |
---|---|
at 245℃; |
phthalic anhydride
phosphorus pentachloride
A
1,1,3,3-tetrachloro-1,3-dihydroisobenzofuran
B
Phthaloyl dichloride
Conditions | Yield |
---|---|
at 245℃; |
phthalic anhydride
A
1,1,3,3-tetrachloro-1,3-dihydroisobenzofuran
B
α,α,α-trichloro-o-toluic chloride
C
Phthaloyl dichloride
Conditions | Yield |
---|---|
at 245℃; |
Phthaloyl dichloride
phosphorus pentachloride
benzene-1,2-dicarboxylic acid
Phthaloyl dichloride
phosphorus pentachloride
benzene-1,2-dicarboxylic acid
A
phthalic anhydride
B
Phthaloyl dichloride
Conditions | Yield |
---|---|
In benzene |
Conditions | Yield |
---|---|
In benzene |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide |
N-<(3-chloro)-propanoxy>phtalimide
Phthaloyl dichloride
Conditions | Yield |
---|---|
Stage #1: N-<(3-chloro)-propanoxy>phtalimide With hydrogenchloride In water at 100 - 105℃; for 3h; Stage #2: With thionyl chloride In toluene for 4h; Reflux; |
Tris(trimethylsilyl)phosphane
Phthaloyl dichloride
Conditions | Yield |
---|---|
In diethyl ether at -50℃; for 2h; | 100% |
cyclopentadienyl iron(II) dicarbonyl dimer
Phthaloyl dichloride
Conditions | Yield |
---|---|
With mercury In tetrahydrofuran soln. of Na#Hg, Hg, Fp2, THF was stirred for 1h, excess amalgam was drained, filtration through celite (medium porosity frit), cooling to -78°C (dry ice/aceton), addn. of 1,2-C6H4(COCl)2, warming to room temp.(1h), drying in vac., Et2O, stirring; | 0% |
chromeno[4,3,2-gh]phenanthridin-2-amine
Phthaloyl dichloride
2-(chromeno[4,3,2-gh]phenanthridin-2-yl)isoindoline-1,3-dione
Conditions | Yield |
---|---|
With pyridine; dmap In dichloromethane at 17 - 25℃; for 0.166667h; Inert atmosphere; | 100% |
4-bromo-benzaldehyde
Phthaloyl dichloride
A
phthalic anhydride
B
p-bromo-α,α-dichlorotoluene
Conditions | Yield |
---|---|
With 1-pyrrolidinecarboxaldehyde In toluene at 60℃; for 17h; | A 100% B 89% |
4-ethylpyridin-2-amine
Phthaloyl dichloride
2-(4-ethylpyridin-2-yl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With dmap In dichloromethane at 0 - 20℃; | 99.8% |
With triethylamine In dichloromethane at 20℃; for 1h; Cooling; | 90% |
With triethylamine In dichloromethane at 20℃; for 1h; | 90% |
With triethylamine In dichloromethane at 20℃; for 1h; | 90% |
Conditions | Yield |
---|---|
With triethylsilane; iron(III)-acetylacetonate at 60℃; for 0.666667h; | 99% |
With triethylsilane; iron(III)-acetylacetonate at 60℃; for 0.666667h; other catalysts: Co(acac)2, Ni(acac)2; same reaction of iso- and terephthaloyl chloride; | 99% |
With tricyclohexylborane at 300℃; for 2h; | 11.5% |
Conditions | Yield |
---|---|
With N,N-dimethylthioformamide; hydrogen sulfide In dichloromethane at 25℃; | 99% |
With sodium sulfide; cetyltributylphosphonium bromide In dichloromethane at 0℃; for 1.33333h; | 95% |
With sodium disulfide; cetyltributylphosphonium bromide In water; benzene for 0.5h; Ambient temperature; also Na2S as reagent; | 87% |
Phthaloyl dichloride
1,4,7-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane
1,1'-phthaloylbis<4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane>
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; Ambient temperature; | 99% |
thiourea
Phthaloyl dichloride
2,2'-Thiocarbonyl-bis(2H-isoindol-1,3-dion)
Conditions | Yield |
---|---|
With sodium carbonate In dichloromethane for 4h; Heating; | 98% |
With N,N-dimethyl-aniline; acetone |
2-methyl-2-propenoic acid 2-hydroxyethyl ester
Phthaloyl dichloride
α,ω-bis(methacryloylethyleneglycol)phthalate
Conditions | Yield |
---|---|
With pyridine In benzene for 5h; Heating; | 98% |
Phthaloyl dichloride
bis(1,1-dimethylethyl) 1,5,9-triazacyclododecane-1,5-dicarboxylate
1,1'-phthaloylbis<5,9-bis(tert-butyloxycarbonyl)-1,5,9-triazacyclododecane>
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; Ambient temperature; | 98% |
(phthalocyanine-2,3:9,10:16,17:23,24-tetrakis(dicarboxanhydride))cobalt(II)
Phthaloyl dichloride
Conditions | Yield |
---|---|
With zinc(II) chloride In neat (no solvent) a mixt. of complex, phthaloyl chloride and anhydrous zinc chloride was stirred for 24 h at 210-215°C; | 98% |
2-(4-aminophenoxy)-2-methyl propionic acid
Phthaloyl dichloride
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; | 98% |
3,6-diamino-9H-carbazole
Phthaloyl dichloride
3,6-diphthalimidocarbazole
Conditions | Yield |
---|---|
With pyridine for 6h; Heating; | 97% |
With pyridine Yield given; |
(μ-dithio)bis(tricarbonyliron)
Phthaloyl dichloride
para-methylphenylmagnesium bromide
Conditions | Yield |
---|---|
In tetrahydrofuran p-TolMgBr in THF was added under N2 with stirring to a THF soln. of Fe2-complex at -78°C, o-C6H4(COCl)2 was added to the resulting anionsoln. at -78°C, mixt. was allowed to warm to room temp.; volatiles were removed, residue purified by column chromy.; elem. anal.; | 97% |
4-amino-2-hydroxybutyric acid
Phthaloyl dichloride
γ-phthalimidoimino-α-hydroxybutyric acid
Conditions | Yield |
---|---|
With dmap; sodium methylate at 60 - 100℃; for 1.36667h; Reagent/catalyst; Temperature; | 96.3% |
Conditions | Yield |
---|---|
With PEG-400; sodium hydroxide In dichloromethane for 1h; Product distribution; Heating; other reagent, solvent; | 96% |
Phthaloyl dichloride
N-allyl (L)-leucine methyl ester
(S)-2-(Allyl-{2-[allyl-((S)-1-methoxycarbonyl-3-methyl-butyl)-carbamoyl]-benzoyl}-amino)-4-methyl-pentanoic acid methyl ester
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; Acylation; | 96% |
2-amino-3-nitropyridine
Phthaloyl dichloride
3-nitro-2-phthalimidopyridine
Conditions | Yield |
---|---|
With pyridine In toluene for 42h; Heating; | 96% |
Phthaloyl dichloride
cyclic phthalic selenoanhydride
Conditions | Yield |
---|---|
Stage #1: Phthaloyl dichloride With selenium; lithium aluminium tetrahydride In tetrahydrofuran; dichloromethane at 50℃; for 1h; Stage #2: With sulfuric acid In tetrahydrofuran; dichloromethane for 0.0833333h; | 95% |
Stage #1: Phthaloyl dichloride With lithium hydrogen selenide In tetrahydrofuran; dichloromethane at 50℃; for 1h; Stage #2: With sulfuric acid In tetrahydrofuran; dichloromethane for 0.0833333h; Reagent/catalyst; Solvent; | 80% |
With triethylamine; p-methylselenobenzamide In dichloromethane at 0℃; for 2h; Acylation; cyclization; | 59.6% |
With LiAlHSeH In tetrahydrofuran at 20℃; for 2h; | 57% |
With aluminium trichloride; selen(o) hydrogen |
2,5-dimethyl-2,5-dihydroperoxyhexane
succinoyl dichloride
Phthaloyl dichloride
2-(4-{2-[4-(3-{4-[3-(4-Hydroperoxy-1,1,4-trimethyl-pentylperoxycarbonyl)-propionylperoxy]-1,1,4-trimethyl-pentylperoxycarbonyl}-propionylperoxy)-1,1,4-trimethyl-pentylperoxycarbonyl]-benzoylperoxy}-1,1,4-trimethyl-pentylperoxycarbonyl)-benzoic acid
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 1.5h; | 95% |
Conditions | Yield |
---|---|
With triethylamine In benzene at 6 - 7℃; for 0.05h; | 95% |
Conditions | Yield |
---|---|
With triethylamine In benzene at 20℃; for 0.05h; | 95% |
With triethylamine In benzene at 20℃; for 0.0833333h; | 92% |
1-amino-2,6-dicyanopiperidine
Phthaloyl dichloride
1-phthalimido-2,6-dicyanopiperidine
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane for 16h; Ambient temperature; | 95% |
Phthaloyl dichloride
3,3-(α-hydroxypentamethylene)diaziridine
2-Hydroxyspiro-diazirino<1,2-b>phthalazine>-3',8'-dione
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 5 - 10℃; for 5h; | 95% |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 0 - 20℃; for 10h; Product distribution / selectivity; | 95% |
(phthalocyanine-2,3:9,10:16,17:23,24-tetrakis(dicarboxanhydride))zinc(II)
Phthaloyl dichloride
Conditions | Yield |
---|---|
With zinc(II) chloride In neat (no solvent) a mixt. of complex, phthaloyl chloride and anhydrous zinc chloride was stirred for 24 h at 210-215°C; | 95% |
Conditions | Yield |
---|---|
With triethylamine Reflux; | 95% |
Conditions | Yield |
---|---|
With sodium methylate In methanol at 0℃; | 94% |
With triethylamine In chloroform at 25℃; for 12h; | 77% |
With sodium methylate |
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