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Cas:101-83-7
Min.Order:200 Kilogram
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Type:Manufacturers
inquiryWe are manufacturer of this product. If you are looking for the material's manufacturer or supplier in China, Ality Group is your best choice. Specifications of our Dicyclohexylamine CAS 101-83-7: Items S
Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:101-83-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryProduct Description
Cas:101-83-7
Min.Order:1 Kilogram
FOB Price: $5.0 / 30.0
Type:Lab/Research institutions
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:101-83-7
Min.Order:1 Metric Ton
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inquiryProperties Dicyklohexylamin(DCHA) CAS 101-83-7 is a colorless to pale yellow transparent liquid, melting point -2 ℃,boiling point 256 ℃,density 0.912 g/mL at 20 °C(lit.),stable. Incompatible with strong acids, strong oxidizing agents. Dicycloh
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:101-83-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:101-83-7
Min.Order:1 Metric Ton
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inquiryProduct Name Dicyclohexylamine CAS No. 101-83-7 EINECS No. 202-980-7 Molecular Formula C6H13N Molecular Weight 181.32 g·mol
Product Detail Minimum Order Qty. 10 Gram
Cas:101-83-7
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryProduct Name: Dicyclohexylamine Synonyms: 8-(Boc-amino)-3,6-dioxaoctanoic acid·;Z-beta-tert-butyl-L-alanine·;3-methoxy-2-[(2-methylpropan-2-yl)oxycarbonylamino]propanoic acid;(S)-3-(1-Boc-pyrrolidin-2-yl)propionic acid·;(2S,
Cas:101-83-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryDicyclohexylamine CAS:101-83-7 Specification Product Name Dicyclohexylamine CAS No. 101-83-7 EINECS No. 202-980-7 Molecular Formula C6H13N Molecular Weight 181.32 g·mol&
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:101-83-7
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:101-83-7
Min.Order:0
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Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:101-83-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirysupplier in China Appearance:Colorless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum;200kg/drum as per your request Application:Used in organic synthesis, also used as a pesticide, acidic ga
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:101-83-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct name: Dicyclohexylamine CAS No.:101-83-7 Molecule Formula:C12H24N Molecule Weight:182.33 Purity: 99.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEM
Cas:101-83-7
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:101-83-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Dicyclohexylamine; DCHA CAS:101-83-7, Please contact us by email freely. We are leading exporter in China. If you really need this ca
Cas:101-83-7
Min.Order:0 Metric Ton
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Type:Other
inquiryHigh purity, high success rate, short cycle and moderate priceAppearance:White powder solid Storage:Negative 20 degrees Celsius Package:5mg, 10mg 100mg, 1gram Application:Applied to various scientific research
Cas:101-83-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers311.Safe and fa
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:101-83-7
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:101-83-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryaniline
A
cyclohexane
B
cyclohexylamine
C
N-cyclohexyl-cyclohexanamine
D
cyclohexene
Conditions | Yield |
---|---|
With ammonia; hydrogen at 180 - 200℃; | A n/a B 98.4% C 0.08% D n/a |
With hydrogen at 160 - 200℃; under 150015 Torr; | A n/a B 95.9% C 0.45% D n/a |
Conditions | Yield |
---|---|
With lithium hydroxide; hydrogen; 5% ruthenium/lithium aluminate In water at 150℃; under 44718.8 Torr; for 2.08333h; Product distribution / selectivity; Neat (no solvent); | A 97.1% B 1% |
With lithium hydroxide; hydrogen; 5% activated charcoal-supported ruthenium catalyst In water at 150℃; under 44718.8 Torr; for 1.21667h; Product distribution / selectivity; Neat (no solvent); | A 91.8% B 5.73% |
With hydrogen; 5% ruthenium/lithium aluminate at 150℃; under 44718.8 Torr; for 1.28333 - 3h; Product distribution / selectivity; Neat (no solvent); | A 89.2% B 0.08% |
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
Stage #1: dicyclohexyl-(3-methylbut-2-enyl)amine With 2,2'-azobis(isobutyronitrile); para-thiocresol In benzene Heating; Stage #2: With hydrogenchloride | 97% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; water at 20℃; for 4h; chemoselective reaction; | 95% |
N,N-dicyclohexyl-p-toluenesulfonamide
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With pyrrolidine; samarium diiodide; water In tetrahydrofuran at 20℃; Inert atmosphere; | 96% |
With naphthalene; tetraethylammonium bromide In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Electrolysis; | 96% |
Stage #1: N,N-dicyclohexyl-p-toluenesulfonamide With Na/K absorbed into silica gel In tetrahydrofuran at 20℃; Inert atmosphere; Stage #2: With water In tetrahydrofuran | 83% |
With diammonium hydrogenphosphate In tetrahydrofuran at 20℃; Product distribution / selectivity; Cooling with ice; | 80% |
Conditions | Yield |
---|---|
With {[(PCy3)(CO)RuH]4(μ-O)(μ-OH)2}; 4-tert-Butylcatechol In chlorobenzene at 130℃; for 16h; Glovebox; Schlenk technique; Sealed tube; chemoselective reaction; | 95% |
With tris(triphenylphosphine)ruthenium(II) chloride In tetrahydrofuran at 185℃; for 5h; | 92% |
With NiCuFeO(x) In 5,5-dimethyl-1,3-cyclohexadiene for 24h; Inert atmosphere; Sealed tube; Reflux; | 82% |
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
Stage #1: ((E)-But-2-enyl)-dicyclohexyl-amine With 2,2'-azobis(isobutyronitrile); para-thiocresol In benzene Heating; Stage #2: With hydrogenchloride | 95% |
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With formic acid; potassium hydroxide In ethanol at 70℃; for 1h; | 93% |
With Pd(OH)2/C In methanol for 8h; Reflux; | 62% |
Conditions | Yield |
---|---|
With NiCuFeO(x) In 5,5-dimethyl-1,3-cyclohexadiene for 24h; Inert atmosphere; Sealed tube; Reflux; | 92% |
With lithium hydroxide In neat (no solvent) at 140℃; for 48h; Inert atmosphere; | 74% |
With nickel at 180 - 190℃; im Ruehrautoklaven; | |
With thorium dioxide at 290 - 320℃; |
Conditions | Yield |
---|---|
With urea In 1,3,5-trimethyl-benzene at 141℃; under 760.051 Torr; for 16h; Inert atmosphere; | 92% |
With ammonium tetrafluroborate; sodium hydrogencarbonate; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] at 140℃; for 17h; | 86% |
With [Cp*Ir(NH3)3]I2; ammonia In water at 140℃; for 24h; Autoclave; Inert atmosphere; | 85% |
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; methoxybenzene In dichloromethane at 0℃; desulfonation; | 92% |
cyclohexanone N-cyclohexylimine
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With ytterbium(III) triflate; bis(η5-cyclopentadinyl)dihydridomolybdenum In methanol at 50℃; for 24h; | 90% |
With ytterbium(III) triflate; bis(η5-cyclopentadinyl)dihydridomolybdenum In methanol at 50℃; for 24h; Product distribution; other reag.; other solvent; other temp.; other reaction time; varying amount of catalyst; | 90% |
With lithium; nickel dichloride In tetrahydrofuran for 6h; Ambient temperature; | 78% |
N-allyl-N-cyclohexylcyclohexanamine
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; water at 20℃; for 18h; chemoselective reaction; | 90% |
With Pd(OH)2/C In methanol for 1h; Reflux; | 69% |
Stage #1: N-allyl-N-cyclohexylcyclohexanamine With 2,2'-azobis(isobutyronitrile); para-thiocresol In benzene Heating; Stage #2: With hydrogenchloride | 63% |
With titanium(III) chloride; lithium In tetrahydrofuran for 20h; Heating; | 47% |
With water; [Ru(η3:η2:η3-dodeca-2,6,10-triene-1,12-diyl)Cl2] at 90℃; for 1.2h; | 99 % Chromat. |
Conditions | Yield |
---|---|
With ammonium acetate In benzene for 1.5h; Leuckart type reaction; Reflux; | 85% |
With N,N,N'N'-tetramethyl-1,3-propanediamine; carbon monoxide; water; hexarhodium hexadecacarbonyl In 2-ethoxy-ethanol at 80℃; under 6080 Torr; for 5h; Mechanism; analogous reaction of other ketones; | 80% |
With N,N,N'N'-tetramethyl-1,3-propanediamine; carbon monoxide; water; hexarhodium hexadecacarbonyl In 2-ethoxy-ethanol at 80℃; under 6080 Torr; for 5h; Mechanism; analogous reaction with other ketones, analogous reaction of an other amine; | 80% |
Conditions | Yield |
---|---|
With dichloro(μ-chloro)(μ-hydrido)bis(η-p-cymene)diruthenium(II); hydrogen In 1,4-dioxane at 90℃; under 37503.8 Torr; for 40h; | 82% |
With nickel at 150℃; under 91938.4 - 147102 Torr; Hydrogenation.ohne Loesungsmittel; | |
With nickel; methyl cyclohexane at 175℃; under 147102 - 161812 Torr; Hydrogenation; |
cyclohexylamine
toluene
A
N-phenyl-2-cyclohexylamine
B
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With Co2Rh2/C at 180℃; under 760.051 Torr; for 18h; Temperature; Autoclave; Inert atmosphere; | A 12% B 82% |
aniline
A
cyclohexanone
B
cyclohexylamine
C
N-cyclohexyl-cyclohexanamine
D
cyclohexanol
Conditions | Yield |
---|---|
With hydrogen; silica gel; rhodium In water at 49.9℃; under 15151.2 Torr; Product distribution; Other catalysts, other temperatures.; | A n/a B 81.5% C 2.8% D 15.7% |
With hydrogen; 5 percent Rh/MgO; magnesium oxide In water at 49.9℃; under 15001.2 Torr; Product distribution; Hydrogenation in the presence of cyclohexylamine; cyclohexanone; cyclohexanol; dicyclohexylamine; ammonia and mixture of them.; | A 0.8% B 73.2% C 6.6% D 18.8% |
With hydrogen; Ru(OH)Cl3 In water at 99.9℃; under 30002.4 Torr; Kinetics; Rate constant; Product distribution; energy data; variation of temperature, pressure; also in presence of oxides; activation energy; | A 1.5% B 64.7% C 1% D 32.5% |
aniline
A
N-phenyl-2-cyclohexylamine
B
cyclohexylamine
C
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
aluminum oxide; ruthenium at 170℃; for 2.5h; Product distribution; Mechanism; investigation of the hydrogenation of aniline with various hydrogenation catalysts in the presence and abscence of the fused salts; | A 0.3% B 80.4% C 7% |
With hydrogen; palladium/alumina at 240℃; for 2.5h; Product distribution; Mechanism; investigation of the hydrogenation of aniline with various hydrogenation catalysts in the presence and abscence of the fused salts; | A 1.1% B 20% C 51.9% |
With formic acid; palladium on activated charcoal In methanol for 70h; Ambient temperature; | A 49 % Chromat. B 20 % Chromat. C 31 % Chromat. |
2-Dicyclohexylamino-ethylacetat
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With bis(p-methoxyphenyl)methanone; water In acetonitrile for 3h; deprotection; Irradiation; | 80% |
cyclohexanone
aniline
A
cyclohexylamine
B
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
Stage #1: cyclohexanone; aniline With hydrogen at 120℃; under 15001.5 Torr; Stage #2: at 180℃; Pressure; Temperature; | A 20.2% B 78.3% |
Stage #1: cyclohexanone; aniline With ammonia; hydrogen at 150℃; under 37503.8 Torr; Stage #2: at 170℃; Reagent/catalyst; Temperature; Pressure; | A 65.3% B 32.8% |
1,1-dicyclohexylhydrazine
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With titanium(III) chloride; water In ethanol pH=7; Reflux; Alkaline aq. solution; Inert atmosphere; | 76% |
With titanium tetrachloride; magnesium In tetrahydrofuran at 20℃; Inert atmosphere; | 70% |
N,N-dicyclohexylmethanesulfonamide
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
Stage #1: N,N-dicyclohexylmethanesulfonamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.25h; Inert atmosphere; Stage #2: With oxygen In tetrahydrofuran; hexane at 20℃; for 1h; Stage #3: With water In tetrahydrofuran; hexane | 75% |
cyclohexylamine
cyclohexanol
A
cyclohexanone N-cyclohexylimine
B
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With Mg-Al hydrotalcite supported copper at 180℃; for 15h; | A 74% B 26% |
With C27H19ClNO3PRu; potassium tert-butylate at 110 - 150℃; for 4h; Inert atmosphere; | A 38 %Spectr. B 9 %Spectr. |
N-cyclohexylisopropylamine
A
cyclohexylamine
B
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); ammonia In tert-Amyl alcohol at 170℃; for 23.5h; Inert atmosphere; Schlenk technique; Autoclave; | A 74% B 7.5% |
Conditions | Yield |
---|---|
With Rh/Al2O3; hydrogen In tetrahydrofuran; water at 80℃; under 15001.5 Torr; for 24h; | A 73% B 27% |
With 5 wt% ruthenium/carbon; hydrogen; sodium nitrite In tetrahydrofuran at 170℃; under 62256.2 Torr; for 4h; Solvent; Autoclave; | |
With dodecane; 5 wt% ruthenium/carbon; hydrogen In tetrahydrofuran at 140℃; under 75007.5 Torr; for 3h; Reagent/catalyst; Autoclave; | |
With hydrogen; sodium chloride In isopropyl alcohol at 90℃; under 45004.5 Torr; for 0.833333h; Catalytic behavior; Reagent/catalyst; |
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
Stage #1: (E)-N,N-dicyclohexyl-3-phenyl-2-propenylamine With 2,2'-azobis(isobutyronitrile); para-thiocresol In benzene Heating; Stage #2: With hydrogenchloride | 70% |
nitrobenzene
A
cyclohexylamine
B
aniline
C
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With octylated silica; hydrogen; sodium 4-dodecylbenzenesulfonate; {[(CH3)(C8H17)3N](+)[RhCl4](-)} at 80℃; under 10343 Torr; for 24h; | A 25% B 6% C 69% |
With propane; hydrogen at 200 - 250℃; under 60006 Torr; Supercritical conditions; Flow reactor; | A 29 %Chromat. B 9 %Chromat. C 58 %Chromat. |
With dodecane; 5 % platinum on carbon; hydrogen In tetrahydrofuran at 140℃; under 75007.5 Torr; for 3h; Reagent/catalyst; Autoclave; |
Conditions | Yield |
---|---|
With copper(l) iodide; tert-butylimino-tri(pyrrolidino)phosphorane; 1,1'-bi-2-naphthol In N,N-dimethyl-formamide; acetonitrile at -10℃; for 24h; Irradiation; | 69% |
cyclohexanone N-cyclohexylimine
A
cyclohexylamine
B
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel boride In methanol Yield given; | A 68% B n/a |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel boride In methanol Yields of byproduct given; | A 68% B n/a |
With Pt/Al2O3; hydrogen In ethanol at 100℃; under 4500.45 Torr; for 3h; Autoclave; chemoselective reaction; |
piperidine
cyclohexylamine
A
1-cyclohexylpiperidine
B
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With platinum-nickel nanoclusters on activated carbon; hydrogen at 160℃; under 760.051 Torr; Flow reactor; chemoselective reaction; | A 62% B 26.3% |
Conditions | Yield |
---|---|
Stage #1: N-cyclohexyl-cyclohexanamine With n-butyllithium In tetrahydrofuran Metallation; Stage #2: With nitrogen(II) oxide In tetrahydrofuran at -78℃; for 3h; Nitrosation; | 100% |
Stage #1: N-cyclohexyl-cyclohexanamine With n-butyllithium In hexane Stage #2: With nitric oxide In tetrahydrofuran under 759811 Torr; for 3h; cooling; | 100% |
With [NO(1+)*18-crown-6*H(NO3)2(1-)] In dichloromethane at 20℃; for 0.0833333h; | 100% |
N-cyclohexyl-cyclohexanamine
epichlorohydrin
1-Chloro-3-dicyclohexylamino-propan-2-ol
Conditions | Yield |
---|---|
In ethanol for 24h; Heating; | 100% |
tert-butylsulfinyl chloride
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; sulfinylation; | 100% |
Conditions | Yield |
---|---|
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) at 100℃; | 100% |
With TiO2 supported nano-Pd(0.8) catalyst In water at 20℃; for 15h; Inert atmosphere; Irradiation; Green chemistry; | 93% |
With [Cp*Ir(2-(1H-benzo[d]imidazol-2-yl)-1H-benzo[d]imidazole)Cl][Cl]; caesium carbonate at 120℃; for 12h; Schlenk technique; | 82% |
formaldehyd
phenylacetylene
N-cyclohexyl-cyclohexanamine
N-cyclohexyl-N-(3-phenylprop-2-yn-1-yl)cyclohexanamine
Conditions | Yield |
---|---|
With copper(l) iodide In water at 25℃; for 1.5h; Mannich reaction; | 100% |
With polystyrene-supported 1-benzyl-1H-imidazole-Ag(I) catalyst at 20℃; for 24h; Inert atmosphere; | 97% |
copper(l) iodide In water; dimethyl sulfoxide at 30℃; for 20h; | 96% |
di-tert-butyl dicarbonate
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With perchloric acid at 30 - 35℃; for 0.75h; | 100% |
at 20℃; for 0.166667h; Ionic liquid; | 100% |
With 1,4-disulfopiperazine-1,4-diium chloride In neat (no solvent) at 20℃; for 1h; Green chemistry; chemoselective reaction; | 96% |
n-butyllithium
N-cyclohexyl-cyclohexanamine
2,2-dicyclohexyl-1-butylidenehydrazine
Conditions | Yield |
---|---|
Stage #1: N-cyclohexyl-cyclohexanamine With n-butyllithium In hexane Stage #2: With nitric oxide In tetrahydrofuran under 759811 Torr; for 3h; cooling; Stage #3: n-butyllithium In tetrahydrofuran; hexane | 100% |
3-(1-adamantyl)-4-vinylbenzoic acid
N-cyclohexyl-cyclohexanamine
3-(1-adamantyl)-4-vinylbenzoyl chloride
Conditions | Yield |
---|---|
With thionyl chloride In diethyl ether; dichloromethane | 100% |
benzene-1,2-diol
N-cyclohexyl-cyclohexanamine
N-(trimethoxysilylmethyl)hexahydroazepin-2-one
Conditions | Yield |
---|---|
In o-xylene at 130 - 140℃; | 100% |
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether; water at 20℃; for 0.5h; | 100% |
With hydrogenchloride In 1,4-dioxane; water at 20℃; for 12h; | 98% |
With hydrogenchloride In diethyl ether; hexane Inert atmosphere; |
N-(tert-butyloxycarbonyl)-12-aminododecanoic acid
N-cyclohexyl-cyclohexanamine
dicyclohexylammonium 12-((tert-butoxycarbonyl)amino)dodecanoate
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.166667h; | 100% |
In methanol at 20℃; for 0.166667h; |
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
With hydrogen iodide In 1,4-dioxane; water at 20℃; for 12h; | 100% |
With hydrogen iodide In diethyl ether; water at 20℃; for 0.5h; | 79% |
N-cyclohexyl-cyclohexanamine
dicyclohexylamine hydrobromide
Conditions | Yield |
---|---|
With hydrogen bromide In 1,4-dioxane; water at 20℃; for 12h; | 100% |
With hydrogen bromide In diethyl ether; water at 20℃; for 0.5h; | 74% |
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; Inert atmosphere; | 100% |
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 24h; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: N-cyclohexyl-cyclohexanamine With n-butyllithium In diethyl ether; hexane at -78 - 0℃; for 0.5h; Inert atmosphere; Stage #2: N,N-dimethylaminodichlorophosphane In diethyl ether; cyclohexane at 20℃; for 0.75h; Inert atmosphere; | 100% |
N-cyclohexyl-cyclohexanamine
Conditions | Yield |
---|---|
In water at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
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