Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:636-98-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiry1 high purity 2 able to provide COA/HNMR/HPLC 3 High quality 4 low price 5 Best service Appearance:white powder Storage:Keep Cold Package:bag/bottle/drum Application:pharmaceutical intermediate Transportation:common transportation Port:Shangh
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:636-98-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiry1-Iodo-4-nitrobenzene Basic information Product Name: 1-Iodo-4-nitrobenzene Synonyms: 4-IODONITROBENZENE;1-IODO-4-NITROBENZENE;AURORA KA-6698;IODONITROBENZENE;P-IODONITROBENZENE;P-NITROI
Cas:636-98-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryCAS No.: 636-98-6 Formula: C6H4INO2 Exact Mass: 248.92900 Molecular Weight: 249.00600 PSA: 45.82000 LogP: 2.72260
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:636-98-6
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:636-98-6
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used for APIs Transportation:as per you
1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:636-98-6
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Our company is engaged in customizing the benzene ring and pyridine derivative organic intermediates, and the quantity is flexible according to customer's needs. It mainly provides high-quality intermediates for domestic and foreign pharmaceutical an
Cas:636-98-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:636-98-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:636-98-6
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiry1-Iodo-4-nitrobenzene Application:1-Iodo-4-nitrobenzene
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
1-Iodo-4-nitrobenzeneAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place Package:foil bags, drums or bottles Application:Pharmaceutical Intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
in storeAppearance:Crystal light yellow to gray red and yellow Package:25g Application:Organic Chemicals
Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:636-98-6
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquirylowest price,highest quality,shortest delivery! 1.Rich experience We specialize in this filed for many years,our steriods and hormones exported to all over the world and established long friendly relations of c
Cas:636-98-6
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Trading Company
inquiry1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume
Cas:636-98-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With potassium iodide; 10-camphorsulfonic acid; sodium nitrite In acetic acid at 20℃; for 24h; Time; | 100% |
With Nitrogen dioxide; sodium iodide In acetonitrile at -20℃; for 10h; | 98% |
Stage #1: 4-nitro-aniline With toluene-4-sulfonic acid In water at 20℃; Stage #2: With potassium iodide In water at 20℃; for 1.5h; | 95% |
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With potassium iodide for 24h; | 100% |
Conditions | Yield |
---|---|
With iodine; dibenzyl hantzsch ester In dimethyl sulfoxide at 20℃; | 99% |
With trimethylsilyl iodide; methyl iodide In N,N-dimethyl-formamide for 1h; Ambient temperature; | 91% |
With iodine; potassium iodide In dimethyl sulfoxide at 15℃; |
1-(4-nitrophenyl)-2-(pyrrolidin-1-yl)diazene
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With iodine In various solvent(s) at 100℃; for 12h; | 98% |
With trifluoroacetic acid; potassium iodide In water Yield given; |
A
p-nitrobenzene iodide
B
para-dinitrobenzene
C
iodobenzene
D
nitrobenzene
Conditions | Yield |
---|---|
With sodium nitrite In chloroform; water at 56℃; for 1h; | A 1% B 98% C 93 % Chromat. D 1 % Chromat. |
Conditions | Yield |
---|---|
With potassium iodide In water at 20℃; for 0.0833333h; | 98% |
With potassium iodide In water for 0.333333h; paste form; |
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With potassium iodide In water at 20℃; | 98% |
iodobenzene
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
benzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 95% |
para-iodoanisole
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
4-methoxy-benzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Kinetics; Solvent; Reagent/catalyst; Temperature; Sealed tube; Inert atmosphere; | A n/a B 95% |
para-diiodobenzene
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
4-iodobenzoic acid chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 95% |
4-tolyl iodide
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
4-methyl-benzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 94% |
4-iodobenzoic acid ethyl ester
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
ethyl 4-(chlorocarbonyl)benzoate
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 94% |
1-Chloro-4-iodobenzene
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
4-chloro-benzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 93% |
1,4-bromoiodobenzene
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
4-chlorobenzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 93% |
3-Iodotoluene
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
3-Methylbenzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 93% |
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In acetonitrile at 20℃; for 0.75h; Substitution; | 92% |
4-nitro-benzoyl chloride
5-iodo-1,3-benzodioxole
A
p-nitrobenzene iodide
B
3,4-(methylenedioxy)benzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 92% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 100℃; for 12h; | 91% |
With 2,2'-azobis(isobutyronitrile); 2-mercaptopyridine-1-oxide sodium salt; methyl iodide In toluene for 0.583333h; Heating; Yield given; |
4-fluoro-1-iodobenzene
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
4-fluorobenzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 91% |
3,5-dimethylphenyl iodide
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
3,5-dimethylbenzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 91% |
1-Fluoro-3-iodobenzene
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
3-fluorobenzoyl chloride
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 91% |
Conditions | Yield |
---|---|
With 1,1,1,3',3',3'-hexafluoro-propanol; N–nitrosaccharin at 60℃; for 19h; Inert atmosphere; Schlenk technique; | 91% |
4-nitro-benzoyl chloride
2-(4-iodophenyl)-2-methyl-[1,2]-dioxolane
A
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 90% |
tert-butyl 2-(4-nitrophenyl)diazenecarboxylate
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With iodine; trifluoroacetic acid In acetonitrile at 80℃; for 0.5h; | 89% |
With iodine; trifluoroacetic acid In acetonitrile at 80℃; | 89% |
With iodine; trifluoroacetic acid In acetonitrile at 80℃; for 4h; | 80% |
Conditions | Yield |
---|---|
With hydrogen iodide In acetonitrile at 60℃; for 0.25h; | 88% |
bis(trifluoromethanesulfonyl)amide
4-nitro-aniline
p-nitrobenzene iodide
Conditions | Yield |
---|---|
Stage #1: bis(trifluoromethanesulfonyl)amide With tert.-butylnitrite; acetic acid In ethanol Cooling with ice; Stage #2: 4-nitro-aniline With tetraethylammonium iodide In water at 20℃; | 88% |
Conditions | Yield |
---|---|
With tributylphosphine; sodium iodide; nickel dibromide In 1-methyl-pyrrolidin-2-one at 180℃; for 3h; Finkelstein reaction; Inert atmosphere; Molecular sieve; Sealed tube; | 87% |
With copper(I) oxide; L-proline; potassium iodide In ethanol at 110℃; for 30h; Schlenk technique; Inert atmosphere; Sealed tube; | 85% |
With KI-CuI-alumina In various solvent(s) at 150℃; for 6h; | 78 % Chromat. |
With copper(l) iodide; 3-azapentane-1,5-diamine; sodium iodide In acetonitrile at 110℃; for 24h; Finkelstein Reaction; Inert atmosphere; | 60 %Chromat. |
4-nitrophenylboronic acid
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With perfluoroisopropyl iodide; copper; hydroquinone In N,N-dimethyl-formamide at 20℃; for 24h; | 87% |
With sodium nitrite In acetonitrile at 80℃; for 8h; Sealed tube; | 87% |
4-nitro-benzoyl chloride
5-iodo-1-(4-methylphenylsulfonyl)indole
A
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 85% |
4-iodobenzonitrile
4-nitro-benzoyl chloride
A
p-nitrobenzene iodide
B
4-cyanobenzoyl chlorIde
Conditions | Yield |
---|---|
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere; | A n/a B 82% |
Conditions | Yield |
---|---|
With hydrazine hydrate In methanol at 26℃; for 0.166667h; Reagent/catalyst; Solvent; | 100% |
With cadmium sulphide; ammonium formate In water at 20℃; for 20h; Inert atmosphere; Irradiation; Sealed tube; | 100% |
With magnesium; nickel dichloride In water at 20℃; for 12h; Sealed tube; Photolysis; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; under 9000720 Torr; for 20h; | 100% |
With copper(l) iodide; 1-(5,6,7,8-tetrahydroquinolin-8-yl)ethan-1-one; caesium carbonate In N,N-dimethyl-formamide at 25℃; for 24h; Ullmann condensation; Inert atmosphere; | 95% |
With copper(l) iodide In N,N-dimethyl acetamide at 130℃; for 24h; | 95% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; under 9000720 Torr; for 20h; | 100% |
With potassium carbonate In dimethyl sulfoxide at 50℃; | 100% |
With sodium acetate In N,N-dimethyl-formamide for 8h; | 95% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; under 9000720 Torr; for 50h; | 100% |
With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; potassium hydroxide In dimethyl sulfoxide at 120℃; for 0.166667h; | 98% |
With sodium t-butanolate In dimethyl sulfoxide at 110℃; for 12h; Buchwald-Hartwig Coupling; | 96% |
1,4-diaza-bicyclo[2.2.2]octane
p-nitrobenzene iodide
1-(4-Nitro-phenyl)-4-aza-1-azonia-bicyclo[2.2.2]octane; iodide
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; under 4500360 Torr; for 75h; | 100% |
In tetrahydrofuran at 50℃; under 4500360 Torr; for 20h; Yield given; |
Conditions | Yield |
---|---|
With copper(l) iodide; iodophenylbis(triphenylphosphine)palladium; triethylamine In chloroform at 60℃; for 1h; | 100% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tributyl-amine; potassium carbonate In water at 20℃; for 4h; | 95% |
With piperidine; 1,3-bis(5-ferrocenylisoxazoline-3-yl)benzene; tetrabutylammomium bromide; palladium diacetate In water; N,N-dimethyl-formamide at 40℃; for 3h; Sonogashira Cross-Coupling; | 94% |
Conditions | Yield |
---|---|
With potassium carbonate; bis-triphenylphosphine-palladium(II) chloride In water; N,N-dimethyl-formamide at 50℃; under 760 Torr; for 3h; | 100% |
With amphiphilic resin-supported phosphine-palladium; water; potassium carbonate at 25℃; under 760 Torr; for 12h; hydroxycarbonylation; | 100% |
With potassium carbonate; bis-triphenylphosphine-palladium(II) chloride In water; N,N-dimethyl-formamide at 50℃; for 3h; Product distribution; effect of different catalysts; | 100% |
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II) In N,N-dimethyl-formamide at 20℃; for 3h; | 100% |
With Palladium nanoparticle cored dendrimer In tetrahydrofuran for 4h; Stille coupling; Reflux; | 96% |
With (4-nitrophenyl)Pd(P(C6H5)3)2I In N,N,N,N,N,N-hexamethylphosphoric triamide at 70℃; for 3.5h; Product distribution; other solvents; also in DMF in vacuum, in the air, and in O2 at various reaction times; | 94 % Chromat. |
p-nitrobenzene iodide
carbon monoxide
triethylmethoxystannane
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With iodophenylbis(triphenylphosphine)palladium under 760 Torr; for 1h; | 100% |
Conditions | Yield |
---|---|
With bis(triethyltin) sulfide; iodophenylbis(triphenylphosphine)palladium In dimethyl sulfoxide for 4h; Heating; | 100% |
With potassium thioacyanate; cetyltrimethylammonim bromide; potassium hydroxide In water at 135℃; for 7h; Green chemistry; | 100% |
With copper(l) iodide; sodiumsulfide nonahydrate; potassium carbonate In N,N-dimethyl-formamide at 120℃; for 18h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With 1-Benzyl-1,4-dihydronicotinamide; RhCl(PPh3)3 In acetonitrile at 70℃; for 3h; Product distribution; other organic halides; var. times, var. temp., also in the presence of PNAH as reductant and Pd(OAc)2 as catalyst; | 100% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 6h; Inert atmosphere; | 100% |
With 18-crown-6 ether In diethyl ether; N,N-dimethyl-formamide for 4h; Heating; | 84% |
p-nitrobenzene iodide
2-(trimethylstannyl)thiophene
2-(4-nitrophenyl)thiophene
Conditions | Yield |
---|---|
With lithium chloropalladite In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 0.5h; other reagents; | 100% |
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; titanium(IV) oxide at 20℃; for 24h; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane; caesium carbonate; palladium diacetate In acetonitrile at 20℃; for 6h; Sonogashira cross-coupling reaction; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane; air; palladium diacetate In acetonitrile at 20℃; for 18h; Sonogashira reaction; | 100% |
p-nitrobenzene iodide
acrylic acid methyl ester
p-nitrocinnamic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine; fluorine-substituted palladium In N,N-dimethyl-formamide at 140℃; for 3h; Heck reaction; | 100% |
With [P5(η3-allyl)(4,4'-(CF3(CF2)9CH2OCH2)-2,2'-bpy)][OTf]; triethylamine In N,N-dimethyl-formamide at 145℃; for 0.25h; Catalytic behavior; Reagent/catalyst; Heck Reaction; Microwave irradiation; | 100% |
With palladium diacetate; triethylamine In toluene at 110℃; for 2.5h; Heck reaction; | 99% |
Conditions | Yield |
---|---|
With [PdCl2(2-ethyl-2-oxazoline)2]; sodium acetate In N,N-dimethyl-formamide at 140 - 150℃; for 24h; Heck reaction; | 100% |
With tetrabutyl ammonium fluoride; palladium dichloride at 40℃; for 12h; Heck reaction; Inert atmosphere; neat (no solvent); | 100% |
With tributyl-amine In N,N-dimethyl-formamide at 120℃; for 24h; Heck-Mizoroki reaction; stereoselective reaction; | 99% |
Conditions | Yield |
---|---|
With palladium diacetate; 4-Ph2P-C6H4-2-N-glucosamine; sodium carbonate In water at 60℃; for 1h; Product distribution; Further Variations:; Temperatures; Reagents; Suzuki cross-coupling reaction; | 100% |
With polyhydroxylated phosphine; sodium carbonate; palladium diacetate In ethanol; water; toluene at 60℃; for 1h; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane; potassium carbonate; palladium diacetate In acetone at 110℃; for 2h; Suzuki-Miyaura cross-coupling reaction; | 100% |
p-nitrobenzene iodide
1-(thiophen-2-yl)prop-2-yn-1-ol
(E)-3-(4-nitropheny)-1-thiophen-3-yl-propenone
Conditions | Yield |
---|---|
With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide In tetrahydrofuran Isomerization; Sonogashira coupling; Heating; | 100% |
With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide In tetrahydrofuran for 9h; Sonogashira coupling-isomerization reaction; Heating; | 95% |
With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran for 16h; Sonogashira coupling; Isomerization; Heating; |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; palladium diacetate In 1,4-dioxane at 100℃; for 8h; Stille reaction; | 100% |
With palladium diacetate; orotic acid; cesium fluoride In 1,4-dioxane at 100℃; for 18h; Concentration; Time; Stille Cross Coupling; Sealed tube; Inert atmosphere; Schlenk technique; | 100% |
With C31H33INPPd In N,N-dimethyl-formamide at 80℃; for 24h; Stille coupling; | 99% |
Conditions | Yield |
---|---|
With copper phthalocyanine; sodium hydroxide In dimethyl sulfoxide at 100℃; | 100% |
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane; dodecane at 110℃; for 24h; | 99% |
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium 10% on activated carbon; caesium carbonate In 1,3,5-trimethyl-benzene at 180℃; for 24h; Inert atmosphere; | 99% |
p-nitrobenzene iodide
acrylic acid n-butyl ester
(E)-n-butyl 4-nitrocinnamate
Conditions | Yield |
---|---|
With C29H33Cl2N5Pd; tetrabutylammomium bromide; sodium carbonate In N,N-dimethyl acetamide at 140℃; for 3h; Heck reaction; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; Heck reaction; Inert atmosphere; regioselective reaction; | 99% |
With 4,4’‐bis(trimethylammoniummethyl)‐2,2’‐bipyridine; diamminedichloropalladium(II); tributyl-amine In water at 140℃; for 12h; Mizoroki-Heck cross-coupling; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With potassium hydroxide; palladium on activated charcoal In water Heating; | 100% |
Conditions | Yield |
---|---|
With copper phthalocyanine; sodium hydroxide In dimethyl sulfoxide at 100℃; | 100% |
With Hippuric Acid; copper diacetate; caesium carbonate In N,N-dimethyl-formamide at 140℃; for 30h; Ullmann coupling reaction; | 99% |
With caesium carbonate In dimethyl sulfoxide at 110℃; for 1h; Ullmann Condensation; | 98% |
p-nitrobenzene iodide
4-methoxyphenylboronic acid
4-methoxy-4'-nitrobiphenyl
Conditions | Yield |
---|---|
With sodium carbonate In ethanol; water at 80℃; for 1h; Suzuki-Miyaura Coupling; Green chemistry; | 100% |
With palladium diacetate; 4-Ph2P-C6H4-2-N-glucosamine; sodium carbonate In tetrahydrofuran; ethanol; water at 60℃; for 18h; | 99% |
With polyhydroxylated phosphine; sodium carbonate; palladium diacetate In ethanol; water; toluene at 60℃; for 18h; | 99% |
(Z)-3-methyl-4-phenyl-4-trimethylsilanylbut-3-en-2-ol
p-nitrobenzene iodide
Conditions | Yield |
---|---|
With copper(l) iodide; lithium tert-butoxide; bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 20℃; for 0.666667h; | 100% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; caesium carbonate; palladium diacetate In acetonitrile at 20℃; for 6h; Sonogashira cross-coupling reaction; | 100% |
With caesium carbonate; 2-aminopyrimidine-4,6-diol; palladium diacetate In acetonitrile at 20℃; for 5h; Sonogashira reaction; | 95% |
With tetrabutyl ammonium fluoride; copper diacetate at 130 - 135℃; for 14h; Sonogashira cross-coupling reaction; | 95% |
With 1,4-diaza-bicyclo[2.2.2]octane; air; palladium diacetate In acetonitrile at 20℃; for 20h; Sonogashira reaction; | 90% |
With 1,4-diaza-bicyclo[2.2.2]octane; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 135 - 140℃; for 4h; Sonogashira cross-coupling; |
p-nitrobenzene iodide
tert-Butyl acrylate
(E)-tert-butyl 3-(4-nitrophenyl)prop-2-enoate
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; potassium carbonate; palladium diacetate In N,N-dimethyl-formamide at 80℃; for 4h; Heck cross-coupling reaction; | 100% |
With tetrabutyl ammonium fluoride; palladium dichloride at 40℃; for 3h; Heck reaction; Inert atmosphere; neat (no solvent); | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane; poly(ethylene glycol)-400; potassium carbonate; palladium diacetate In water at 80℃; for 4h; Heck cross-coupling; | 98% |
p-nitrobenzene iodide
tributylstannylethynylbenzene
4-(phenylethynyl)nitrobenzene
Conditions | Yield |
---|---|
With potassium fluoride; 1,4-dicyclohexyl-diazabutadiene; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane at 100℃; for 16h; Stille cross-coupling reaction; | 100% |
diphenylphosphine-based palladium(0) complex on MCM-41 In water; N,N-dimethyl-formamide at 60℃; for 6h; Stille coupling; | 87% |
Stage #1: p-nitrobenzene iodide With diphenylphosphinoethane functionalized polystyrene resin-supported Pd(0) complex In N,N-dimethyl-formamide at 20℃; for 0.25h; Stille Cross Coupling; Stage #2: tributylstannylethynylbenzene In N,N-dimethyl-formamide at 65℃; for 7h; Stille Cross Coupling; | 86% |
p-nitrobenzene iodide
2-(tributylstannyl)furan
2-(4-nitrophenyl)furan
Conditions | Yield |
---|---|
With potassium fluoride; 1,4-dicyclohexyl-diazabutadiene; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane at 100℃; for 16h; Stille cross-coupling reaction; | 100% |
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