img _fcksavedurl="/UserAppearance:clear colorless liquid with a sharp characteristic odor Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate use
Cas:141-32-2
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Cas:141-32-2
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Product Description Product website: http://www.finerchem.com Product Name Butyl acrylate CAS No. 141-32-2
Cas:141-32-2
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inquiryProduct Name: Butyl acrylate Synonyms: n-Butyl acrylate, 98+%, stab. with up to 50ppM 4-Methoxyphenol;BUTYL ACRYLATE (STABILISED WITH HYDROQUI;BUTYL-2-ACRYLATE;Acrylsure-n-butylester;N-BUTYL ACRYLATE , STABILIZED WITH 50PPM 4-METHOXYPH
Cas:141-32-2
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inquiryProduct Name:Butyl acrylate CAS No.:141-32-2 EINECS: 216-768-7 Molecular Formula: C7H12O2 Molecular Weight: 128.17 Appearance:colorless liquid Appearance: Colorless Transparent Liquid Storage: Preserve in well-closed, light-resistant and airt
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Cas:141-32-2
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inquiryn-Butyl acrylate CAS:141-32-2 Specification Analysis item Grade Result Standard Appearance colorless clear liquid Purity% 99.5min 99.
Appearance:White or off-white Solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Organic synthesis Transportation:Common products:Sea/Air/Courier Dangerous Che
Cas:141-32-2
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Cas:141-32-2
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Cas:141-32-2
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inquirySuperior quality, moderate price & quick delivery. Appearance:colorless transparent liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used in organic syn
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inquiryProduct Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:141-32-2
Min.Order:1 Kilogram
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Cas:141-32-2
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inquiryFree sample Butyl acrylate CAS:141-32-2 with good priceAppearance:Clear colorless to yellow liquid Storage:Store at RT. Package:25 kg/200 kg drum or as customer required. Application:Synthetic resin and synthetic fiber,etc Transportation:By express (
Cas:141-32-2
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inquiryConditions | Yield |
---|---|
sulfuric acid at 89℃; under 127 Torr; Continuous process; | 99.8% |
In neat (no solvent) at 80℃; for 3h; | 90% |
With sulfuric acid |
Conditions | Yield |
---|---|
Stage #1: acrylic acid With hydroquinone; sodium hydroxide In water at 0 - 20℃; for 0.5h; Large scale; Stage #2: 1-bromo-butane With Aliquat 336; potassium iodide at 70 - 80℃; for 3h; Reagent/catalyst; Temperature; Large scale; | 89.6% |
zirconocene dichloride
hex-3-yne
butyl 2-bromoacrylate
A
acrylic acid n-butyl ester
B
butyl 2,3,4,5-tetraethylbenzoate
Conditions | Yield |
---|---|
Stage #1: zirconocene dichloride With n-butyllithium In tetrahydrofuran at -78℃; Inert atmosphere; Stage #2: hex-3-yne In tetrahydrofuran at 20℃; Inert atmosphere; Stage #3: butyl 2-bromoacrylate Further stages; | A n/a B 67% |
carbon monoxide
acetylene
butan-1-ol
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II); sodium acetylacetonate In tetrahydrofuran at 230℃; under 1500.15 - 35253.5 Torr; for 0.75h; Reagent/catalyst; Temperature; Pressure; Solvent; Autoclave; | 65.4% |
With copper(ll) bromide; nickel dibromide In acetylacetone at 200℃; under 60006 Torr; | |
With 2-Picolinic acid In tetrahydrofuran at 200℃; under 1500.15 - 37503.8 Torr; for 1h; Autoclave; Inert atmosphere; | |
With nickel(II) sulfamate; 7-propyl-8-hydroxyquinoline; diethylaluminium chloride; triphenylphosphine In n-heptane at 80℃; under 29252.9 - 30753.1 Torr; for 0.666667h; Reagent/catalyst; Solvent; Temperature; Pressure; Autoclave; Inert atmosphere; |
Conditions | Yield |
---|---|
Continuous process; | A n/a B 60% |
Conditions | Yield |
---|---|
With triethylamine In diethyl ether for 16h; Heating; | 53% |
With triethylamine In chloroform at 10℃; for 12h; |
butan-1-ol
A
acrylic acid n-butyl ester
B
2-carboxyethyl acrylate
C
acrylic acid
Conditions | Yield |
---|---|
at 280℃; under 48754.9 Torr; for 0.0933333h; Product distribution / selectivity; | A 31% B 30% C 52% |
Conditions | Yield |
---|---|
With <(2,2'-bipyridine)(2,2':6',2''-terpyridine)RuO>2+; phosphate buffer pH 8.1 for 24h; Ambient temperature; electrocatalytic oxidation with Ru(IV)-complex; | 42% |
Conditions | Yield |
---|---|
With boron fluoride ether at 250℃; Behandeln des Reaktionsprodukts mit Butan-1-ol und Erhitzen des mit Schwefelsaeure versetzten Reaktionsgemisches; |
Conditions | Yield |
---|---|
With lead acetate; silica gel at 400℃; |
Conditions | Yield |
---|---|
With quartz at 510 - 530℃; |
Conditions | Yield |
---|---|
With catalyst from lithium dihydrogenphosphate and graphite at 510℃; |
Conditions | Yield |
---|---|
With sulfuric acid zuletzt bei 160grad; |
Conditions | Yield |
---|---|
With phosphoric acid; pumice stone; hydroquinone; butan-1-ol at 180℃; |
Conditions | Yield |
---|---|
With sulfuric acid Erhitzen des Reaktionsprodukts mit Butan-1-ol oder wenig Wasser auf 170grad; |
acrylic acid methyl ester
butan-1-ol
A
methanol
B
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
at 58 - 85℃; Equilibrium constant; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; hydroquinone Abdestillieren des entstandenen Methanols als azeotropes Gemisch mit Methylacrylat; |
3-chloro-propionic acid butyl ester
N,N-diethylaniline
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
at 200℃; |
butyl 3-bromopropanate
N,N-diethylaniline
A
1-bromo-butane
B
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
at 200℃; |
5-Oxo-5-pyridin-4-yl-pentanoic acid butyl ester; hydrochloride
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
In acetonitrile Quantum yield; Irradiation; |
p-(γ-carbobutoxybutyryl)pyridine
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
In acetonitrile Quantum yield; Irradiation; |
Conditions | Yield |
---|---|
With porcine pancreatic lipase In tetrahydrofuran for 48h; Ambient temperature; Yield given; | |
With zirconium(IV) acetylacetonate; 4-methoxy-phenol at 70℃; for 2.91667h; Kinetics; Reagent/catalyst; Inert atmosphere; | |
With 10H-phenothiazine; 2,6-di-tert-butyl-4-methyl-phenol; 4-methoxy-phenol; di(n-butyl)tin oxide at 110℃; under 60.006 - 97.5098 Torr; for 4.5h; |
carbon monoxide
acetylene
butan-1-ol
A
propionic acid butyl ester
B
acrylic acid n-butyl ester
C
dibutyl succinate
Conditions | Yield |
---|---|
With hydrogenchloride; dicarbonyl(η5-cyclopentadienyl)nitrosylchromium at 70℃; under 750.06 Torr; Rate constant; other catalysts; |
carbon monoxide
acetylene
butan-1-ol
A
Dibutyl maleate
B
acrylic acid n-butyl ester
C
dibutyl succinate
D
dibutyl fumarate
Conditions | Yield |
---|---|
(PdPPh3Cl2)CO at 25℃; Product distribution; effect of the catalyst to the production and the selectivity; |
Conditions | Yield |
---|---|
In 2,2,4-trimethylpentane at 37℃; immobilized lipase from Candida cylindracea; |
2,3-butanedione mono-oxime acrylate
butan-1-ol
A
acrylic acid n-butyl ester
B
butane-2,3-dione mono-oxime
Conditions | Yield |
---|---|
With porcine pancreatic lipase In tetrahydrofuran for 48h; Ambient temperature; Yield given; |
cyclohexanone oxime acrylate
butan-1-ol
A
Cyclohexanone oxime
B
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
With porcine pancreatic lipase In tetrahydrofuran for 48h; Ambient temperature; Yield given; |
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
With N,N-diethylaniline at 200℃; |
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
at 240℃; |
Conditions | Yield |
---|---|
With hydrogen; Pd(II) complex containing tridentate hydrazonic ligands In methanol at 40℃; for 5h; Hydrogenation; | 100% |
With C44H40IrNP2; hydrogen In benzene-d6 at 25℃; under 760.051 Torr; Catalytic behavior; Reagent/catalyst; Schlenk technique; | 100% |
With hydrogen; Pd-polymethylhydrosiloxane nanocomposite In benzene at 20℃; for 4h; | 94% |
acrylic acid n-butyl ester
Butyl 2,3-dibromopropanoate
Conditions | Yield |
---|---|
With bromine In dichloromethane at 0 - 20℃; for 15h; Inert atmosphere; | 100% |
With bromine In tetrachloromethane | 96% |
With bromine at 20℃; | 96% |
With bromine In tetrachloromethane; dichloromethane | 77% |
With bromine In acetic acid at 30℃; Mechanism; Rate constant; |
bromobenzene
acrylic acid n-butyl ester
(E)-3-(phenyl)acrylic acid butyl ester
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; sodium carbonate; [PdClMe(MeSC6H4CH2PPh2)] at 130℃; for 72h; Heck arylation; | 100% |
With tetrabutylammonium acetate; resin-PPh2-Pd(OAc)2 In carbon dioxide at 120℃; under 155149 Torr; for 16h; Heck reaction; | 100% |
With tetrabutylammonium acetate; polyurea-encapsulated Pd(OAc)2 In various solvent(s) at 100℃; Heck reaction; | 99% |
1-bromo-4-methoxy-benzene
acrylic acid n-butyl ester
(E)-3-(4-methoxyphenyl)acrylic acid butyl ester
Conditions | Yield |
---|---|
With 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) In N,N-dimethyl-formamide at 130℃; for 20h; Heck cross-coupling; | 100% |
With phenyl carbamate; tetrabutylammomium bromide; potassium carbonate; palladium diacetate In N,N-dimethyl-formamide at 130℃; for 2h; Heck-type reaction; | 99% |
With potassium carbonate; di-μ-acetato-bis[2-[bis(1,1-dimethylethyl)phosphino]-2-methylpropyl-C,P]dipalladium In ISOPROPYLAMIDE | 99.2% |
acrylic acid n-butyl ester
4-bromo-benzaldehyde
butyl (E)-4-formylcinnamate
Conditions | Yield |
---|---|
With 2-n-butyl-1,1,1,3,3-tetramethylguanidine acetate; palladium dichloride at 140℃; for 0.25h; | 100% |
With sodium acetate In ISOPROPYLAMIDE | 100% |
With sodium acetate In ISOPROPYLAMIDE | 100% |
acrylic acid n-butyl ester
para-bromoacetophenone
(E)-3-(4-acetylphenyl)acrylic acid butyl ester
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate In N,N-dimethyl acetamide at 100℃; for 3h; Product distribution; Further Variations:; Reagents; Heck reaction; | 100% |
With tributyl-amine In N,N-dimethyl-formamide at 150℃; for 1h; Heck reaction; | 100% |
With C29H33Cl2N5Pd; tetrabutylammomium bromide; sodium carbonate In N,N-dimethyl acetamide at 140℃; for 4h; Heck reaction; Inert atmosphere; | 100% |
iodobenzene
acrylic acid n-butyl ester
(E)-3-(phenyl)acrylic acid butyl ester
Conditions | Yield |
---|---|
With triethylamine; polymer(fiber)-supported palladium In 1,4-dioxane at 100℃; for 2h; Heck reaction; | 100% |
With caesium carbonate; 1,3-bis(mesityl)imidazolium chloride; bis(acetylacetonate)nickel(II) In N,N-dimethyl-formamide at 150℃; for 3h; Heck reaction; | 100% |
With tetramethylquanidine; sodium acetate; palladium dichloride In N,N-dimethyl acetamide at 140℃; for 2h; Heck reaction; | 100% |
acrylic acid n-butyl ester
para-nitrophenyl bromide
(E)-n-butyl 4-nitrocinnamate
Conditions | Yield |
---|---|
With tetramethylquanidine; sodium acetate; palladium dichloride In N,N-dimethyl acetamide at 140℃; for 20h; Heck reaction; | 100% |
With 2-n-butyl-1,1,1,3,3-tetramethylguanidine acetate; palladium dichloride at 140℃; for 0.25h; | 100% |
With tri-n-propylamine In 1-methyl-pyrrolidin-2-one at 125℃; for 1h; Mizoroki-Heck reaction; Inert atmosphere; | 100% |
iodobenzene
acrylic acid n-butyl ester
n-butyl cinnamate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 140℃; for 24h; Heck reaction; | 100% |
With tributyl-amine In N,N-dimethyl acetamide at 100℃; for 4h; Reagent/catalyst; Inert atmosphere; | 100% |
With tributyl-amine In N,N-dimethyl acetamide at 100℃; for 4h; Reagent/catalyst; | 100% |
Conditions | Yield |
---|---|
With diethylene glycol dibutyl ether; [PdBr2]([Ph2PCH2C(Ph)=N(2,6-iPr2C6H3)]) In N,N-dimethyl acetamide at 130℃; for 20h; Product distribution; Further Variations:; Catalysts; Heck coupling; | 100% |
With water; potassium carbonate In 1-methyl-pyrrolidin-2-one at 135℃; for 24h; Catalytic behavior; Heck Reaction; | 99% |
With tributyl-amine; Palladium bipyridyl complex anchored on nanosized MCM-41 In various solvent(s) at 170℃; for 16h; Heck reaction; | 98% |
acrylic acid n-butyl ester
9-benzyl-6-hypoxanthine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 80℃; for 20h; Addition; | 100% |
3-methoxyphenyl bromide
acrylic acid n-butyl ester
(E)-n-butyl 3-(3-methoxyphenyl)acrylate
Conditions | Yield |
---|---|
With potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride In N,N-dimethyl acetamide at 140℃; for 12h; Heck reaction; | 100% |
With di-tert-butylneopentylphosphonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0) In N,N-dimethyl-formamide at 24℃; for 24h; Heck Reaction; Glovebox; | 98% |
With bis(1,1'-ethylene-3,3'-divinylimidazole-2,2'-diylidene)nickel(II) dibromide dihydrate; potassium carbonate In N,N-dimethyl-formamide at 100℃; for 4h; Heck Reaction; Inert atmosphere; Schlenk technique; | 96% |
acrylic acid n-butyl ester
4-tolyl iodide
(E)-n-butyl 3-(p-tolyl)acrylate
Conditions | Yield |
---|---|
With 1-tert-butyl-3-(2-(diphenylarsinyl)benzyl)-1H-imidazol-3-ium chloride; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) In ISOPROPYLAMIDE at 60℃; for 20h; Heck reaction; Inert atmosphere; | 100% |
With triethylamine; bis(N-methylimidazol-2-yl)Pd(Cl)Me In various solvent(s) at 120℃; for 0.5h; Heck coupling; | 99% |
With potassium phosphate; N,N'-(1,2-ethanediylidene)bishexahydro-1H-azepin-1-amine; tetrabutylammomium bromide; dichloro bis(acetonitrile) palladium(II) In N,N-dimethyl-formamide at 130℃; for 24h; Mizoroki-Heck reaction; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride In N,N-dimethyl acetamide at 140℃; for 24h; Heck reaction; | 100% |
With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane In N,N-dimethyl-formamide at 130℃; for 20h; Heck reaction; | 92% |
p-nitrobenzene iodide
acrylic acid n-butyl ester
(E)-n-butyl 4-nitrocinnamate
Conditions | Yield |
---|---|
With C29H33Cl2N5Pd; tetrabutylammomium bromide; sodium carbonate In N,N-dimethyl acetamide at 140℃; for 3h; Heck reaction; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; Heck reaction; Inert atmosphere; regioselective reaction; | 99% |
With 4,4’‐bis(trimethylammoniummethyl)‐2,2’‐bipyridine; diamminedichloropalladium(II); tributyl-amine In water at 140℃; for 12h; Mizoroki-Heck cross-coupling; Sealed tube; | 99% |
1-Chloro-4-iodobenzene
acrylic acid n-butyl ester
butyl (E)-4-chlorocinnamate
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); 1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene monohydrochloride In N,N-dimethyl-formamide at 120℃; for 0.5h; Heck reaction; Inert atmosphere; | 100% |
With sodium carbonate In N,N-dimethyl-formamide at 80℃; for 24h; Mizoroki-Heck reaction; Inert atmosphere; | 100% |
With 1,3-bis(5-ferrocenylisoxazoline-3-yl)benzene; tetrabutylammomium bromide; sodium acetate; palladium diacetate In water at 80℃; for 4h; Heck Reaction; diastereoselective reaction; | 95% |
acrylic acid n-butyl ester
4-Iodoacetophenone
(E)-3-(4-acetylphenyl)acrylic acid butyl ester
Conditions | Yield |
---|---|
With C29H33Cl2N5Pd; tetrabutylammomium bromide; sodium carbonate In N,N-dimethyl acetamide at 140℃; for 3h; Heck reaction; Inert atmosphere; | 100% |
With tributyl-amine; chloro-[2-(9-phenyl-1,10-phenanthrolin-2-yl)phenyl]palladium In 1-methyl-pyrrolidin-2-one at 140℃; for 15h; Heck Reaction; Inert atmosphere; | 100% |
With phenyl carbamate; potassium carbonate; palladium diacetate In N,N-dimethyl-formamide at 130℃; for 2h; Heck-type reaction; | 99% |
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
With Ethyl 2-bromopropionate; bis(1,3-dicyclohexyl-2,3-dihydro-1H-imidazolyl)Cl2RuCHPh In toluene at 85℃; for 16h; | 100% |
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
With Ethyl 2-bromopropionate; bis[1,3-(i-Pr)2-2,3-dihydro-1H-imidazolyl]Cl2PCy3RuCHPh In toluene at 85℃; for 16h; | 100% |
bromobenzene
acrylic acid n-butyl ester
n-butyl cinnamate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 130℃; for 0.75h; Catalytic behavior; Reagent/catalyst; | 100% |
With Br(1-)*C27H29BrN5Pd(1+); potassium carbonate In 1-methylpiperidin-2-one at 140℃; for 8h; Heck reaction; | 99% |
With C8H19Cl2N2O2PPd; tetrabutylammomium bromide; sodium hydrogencarbonate at 140℃; for 4h; Heck reaction; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride In N,N-dimethyl acetamide at 140℃; for 45h; Heck reaction; | 100% |
With triethylamine; bis(N-methylimidazol-2-yl)Pd(Cl)Me In various solvent(s) at 120℃; for 4h; Heck coupling; | 80% |
With palladium diacetate; caesium carbonate; triphenylphosphine In N,N-dimethyl-formamide at 120℃; for 24h; Heck Reaction; Schlenk technique; | 77% |
1-bromo-3-chlorobenzene
acrylic acid n-butyl ester
3-chloro-trans-cinnamic acid n-butyl ester
Conditions | Yield |
---|---|
With potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride In N,N-dimethyl acetamide at 120℃; for 5h; Heck reaction; | 100% |
With tetrabutylammonium acetate; palladium diacetate at 100℃; for 0.5h; Heck reaction; Air atmosphere; Ionic liquid; chemoselective reaction; |
acrylic acid n-butyl ester
1-bromo-3,5-di-tert-butylbenzene
Conditions | Yield |
---|---|
With potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride In N,N-dimethyl acetamide at 140℃; for 24h; Heck reaction; | 100% |
Conditions | Yield |
---|---|
With trans-[PdCl2(1-phenyl imidazole)2]; potassium carbonate In N,N-dimethyl-formamide at 140℃; for 24h; Catalytic behavior; Reagent/catalyst; Heck Reaction; Inert atmosphere; | 100% |
With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; tetrabutylammomium bromide; triethylamine In N,N-dimethyl-formamide at 140℃; for 20h; Reagent/catalyst; Heck Reaction; Sealed tube; Inert atmosphere; Schlenk technique; | 99% |
With C24H21ClN2PdS; potassium carbonate In N,N-dimethyl acetamide for 24h; Reagent/catalyst; Heck Reaction; Inert atmosphere; Heating; | 96% |
acrylic acid n-butyl ester
poly-n-butyl acrylate, obtained by anionic polymerization, initiated with the tBuOK/iBu3Al system, Mn = 46100, Mw/Mn = 2.30; monomer(s): n-butyl acetate
Conditions | Yield |
---|---|
With potassium tert-butylate; triisobutylaluminum In toluene at 0 - 20℃; | 100% |
With potassium tert-butylate; triisobutylaluminum In toluene at 0 - 20℃; | 100% |
Conditions | Yield |
---|---|
With 1,4-benzoquinoline; toluene-4-sulfonic acid; palladium diacetate In acetic acid; toluene at 22℃; for 17h; | 100% |
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
With potassium tert-butylate; triisobutylaluminum In hexane; toluene at 0 - 20℃; for 2h; | 100% |
acrylic acid n-butyl ester
4-bromo-benzaldehyde
butyl (E)-4-formylcinnamate
Conditions | Yield |
---|---|
With sodium acetate In ISOPROPYLAMIDE | 100% |
acrylic acid n-butyl ester
2-Methylaziridine
3-(2-methylaziridin-1-yl)propionic acid butyl ester
Conditions | Yield |
---|---|
at 20℃; for 20h; Michael Condensation; | 100% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 80℃; for 24h; Mizoroki-Heck reaction; Inert atmosphere; | 100% |
With 4,4’‐bis(trimethylammoniummethyl)‐2,2’‐bipyridine; diamminedichloropalladium(II); tributyl-amine In water at 140℃; for 12h; Mizoroki-Heck cross-coupling; Sealed tube; | 99% |
With palladium diacetate; triethylamine In acetonitrile at 180℃; under 41254.1 Torr; for 0.166667h; Mizoroki-Heck coupling; | 94% |
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