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Nanjing Fred Technology Co.,Ltd.

Taizhou FredChem Co. Ltd. is a high-tech enterprise located in China Medical City specializing in R&D, manufacturing, sales of new APIS, pharmaceutical intermediates and fine chemicals. All of our company is committed to provide high quality ch

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 4'-Iodoacetophenone supplier in China

Cas:13329-40-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C

4'-Iodoacetophenone manufacturer with low price

Cas:13329-40-3

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Kilogram

FOB Price: $4.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

4'-Iodoacetophenone Basic information Product Name: 4'-Iodoacetophenone Synonyms: 1-(4-IODOPHENYL)ETHANONE;4'-IODOACETOPHENONE;4-IODOACETOPHENONE;Ethanone, 1-(4-iodophenyl)-;

13329-40-3

Cas:13329-40-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 13329-40-3 with best price

Cas:13329-40-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name: 4'-Iodoacetophenone Synonyms: 1-(4-iodophenyl)ethan-1-one CAS:13329-40-3 MF: C8H7IO Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:Agrochemical Intermediates, Dyestuf

4'-Iodoacetophenone CAS:13329-40-3

Cas:13329-40-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Ethanone,1-(4-iodophenyl)- 13329-40-3

Cas:13329-40-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Kilogram

FOB Price: $76.0 / 85.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

4'-Iodoacetophenone CAS:13329-40-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i

4'-Iodoacetophenone CAS:13329-40-3

Cas:13329-40-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Ethanone,1-(4-iodophenyl)-

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h

Factory Supply 1-(4-iodophenyl)ethan-1-one

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Other

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea

13329-40-3CAS NO.: 13329-40-3

Cas:13329-40-3

Min.Order:1 Gram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 4'-Iodoacetophenone CAS: 13329-40-3 MF: C8H7IO MW: 246.05 EINECS: 236-372-8 Mol File: 13329-40-3.mol 4'-Iodoacetophenone Structure 4'-Iodoacetophenone Chemical Properties Melting point 82-84 °C(li

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Changzhou Anchor Biological Technology Co., Ltd.

Our company is engaged in customizing the benzene ring and pyridine derivative organic intermediates, and the quantity is flexible according to customer's needs. It mainly provides high-quality intermediates for domestic and foreign pharmaceutical an

1-(4-Iodophenyl)ethanone Manufacturer/High quality/Best price/In stock CAS NO.13329-40-3

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratoryAppearance:White to light yellow crystal Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

4'-Iodoacetophenone cas no. 13329-40-3 98%

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

4-Iodoacetophenone

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

1-(4-iodophenyl)ethan-1-one

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Other

inquiry

Wuxi TAA Chemical Industry Co.,LTD.

1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

13329-40-3

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Fandachem Co.,Ltd

4'-Iodoacetophenone,cas:13329-40-3 from fandachem Appearance:Brown crystalline powder Storage:Store in dry, dark and ventilated place Application:intermediate Transportation:by air, by sea, by express

4'-Iodoacetophenone,cas:13329-40-3 from fandachem

Cas:13329-40-3

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

4'-Iodoacetophenone

Cas:13329-40-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

1-(4-iodophenyl)ethanol
68120-56-9, 104013-25-4, 53207-29-7

1-(4-iodophenyl)ethanol

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With silica-supported Jones reagent In dichloromethane for 0.00269444h;99.6%
With 1,10-Phenanthroline; iron(III)-acetylacetonate; potassium carbonate In toluene for 48h; Reflux; Green chemistry;94%
With [bis({2‐[bis(propan‐2‐yl)phosphanyl]ethyl})amine](borohydride)(carbonyl)(hydride)iron(II) In toluene at 120℃; for 12h; Glovebox; Schlenk technique; Inert atmosphere;94%
1-ethynyl-4-iodobenzene
766-99-4

1-ethynyl-4-iodobenzene

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With tetrakis(p-sulfonatophenyl)porphyrin cobalt(III) trisodium salt hexahydrate; water; bis(trifluoromethanesulfonyl)amide In methanol at 80℃; for 12h; Sealed tube;97%
4-Aminoacetophenone
99-92-3

4-Aminoacetophenone

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
Stage #1: p-aminobenzophenone With hydrogenchloride In water at 0 - 5℃; for 0.166667h;
Stage #2: With 1-methyl-3-(2-[2-(1-methyl-1H-imidazol-3-ium-3-yl)ethyloxy]ethyl)-1H-imidazol-3-ium dinitrite In water for 0.166667h;
Stage #3: With potassium iodide In water at 20℃; for 0.166667h; Ionic liquid;
95%
With toluene-4-sulfonic acid; sodium iodide In water; acetonitrile at 10 - 20℃; for 2h; Inert atmosphere;94%
With N-iodo-succinimide; sodium nitrite In N,N-dimethyl-formamide at 20℃; for 4h; Reagent/catalyst; Temperature; Solvent;92%
1-(p-acetophenyl)-3,3-diethyl-1-triazene
86452-55-3

1-(p-acetophenyl)-3,3-diethyl-1-triazene

A

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

B

benzene
71-43-2

benzene

Conditions
ConditionsYield
With sulfonic acid resin (H+ form, Bio-Rad AG 50W-12); sodium iodide In acetonitrile at 75℃; for 0.133333h;A 95%
B n/a
1-(3,4-Diiodocyclohexa-1,3-dienyl)ethanone
85972-28-7

1-(3,4-Diiodocyclohexa-1,3-dienyl)ethanone

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene95%
1,2,2-triphenyl-1-iodoethylene
22021-09-6

1,2,2-triphenyl-1-iodoethylene

4,5-dimethoxy-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

4,5-dimethoxy-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With thallium(I) acetate; cesium fluoride; bis(dibenzylideneacetone)-palladium(0) In toluene; acetonitrile at 90℃; for 8h;95%
4-acetophenyl triflate
109613-00-5

4-acetophenyl triflate

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With [Cp*Ru(CH3CN)3]OTf; sodium iodide at 120℃; for 12h; Inert atmosphere;95%
With iodine; lithium fluoride; sodium iodide In acetonitrile at 25℃; for 24h; Inert atmosphere; UV-irradiation; Schlenk technique;20%
Multi-step reaction with 2 steps
1: KOAc / PdCl2(dppf) / dimethylsulfoxide / 3 h / 80 °C
2: 30 percent / aq. NaI; chloramine-T / tetrahydrofuran / 6 h
View Scheme
1-(p-acetophenyl)-3,3-diethyl-1-triazene
86452-55-3

1-(p-acetophenyl)-3,3-diethyl-1-triazene

A

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With cation exchange resin BioRad AG 50W-X12 (H+); sodium iodide In acetonitrile at 75℃; Product distribution; further solvent: THF, DMSO;A 94%
B 6%
para-bromoacetophenone
99-90-1

para-bromoacetophenone

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With copper(I) oxide; L-proline; potassium iodide In ethanol at 110℃; for 30h; Schlenk technique; Inert atmosphere; Sealed tube;92%
With tributylphosphine; potassium iodide; nickel dibromide In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide at 50℃; for 1.5h;66%
With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; potassium iodide at 150 - 160℃; for 5h;60%
1-(p-acetophenyl)-3,3-diethyl-1-triazene
86452-55-3

1-(p-acetophenyl)-3,3-diethyl-1-triazene

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With chloro-trimethyl-silane; sodium iodide In acetonitrile at 60℃; for 0.0833333h;92%
4-acetylphenylboronic acid
149104-90-5

4-acetylphenylboronic acid

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With iodine; potassium carbonate In acetonitrile at 80℃; for 8h; Inert atmosphere; Schlenk technique; Sealed tube;91%
With sodium nitrite In acetonitrile at 80℃; for 5h; Sealed tube;86%
With 1,10-Phenanthroline; oxygen; potassium iodide; copper(ll) bromide In N,N-dimethyl-formamide at 80℃; for 20h;76%
1-(4-acetylphenyl)diazonium tetrafluoroborate
350-47-0

1-(4-acetylphenyl)diazonium tetrafluoroborate

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With N-iodo-succinimide; sodium nitrite In dimethyl sulfoxide at 20℃; for 2.5h;90%
With diiodomethane; tetrabutylammonium perchlorate In methanol; N,N-dimethyl-formamide at 20℃; for 3h; Sandmeyer Reaction; Electrochemical reaction;87%
iodobenzene
591-50-4

iodobenzene

4-(phenylethynyl)nitrobenzene
1942-30-9

4-(phenylethynyl)nitrobenzene

2-(trimethylsilyl)phenyl trifluoromethanesulfonate
88284-48-4

2-(trimethylsilyl)phenyl trifluoromethanesulfonate

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With thallium(I) acetate; cesium fluoride; bis(dibenzylideneacetone)-palladium(0) In toluene; acetonitrile at 90℃; for 8h;89%
1-iodo-4-(prop-1-en-2-yl)benzene
561023-21-0

1-iodo-4-(prop-1-en-2-yl)benzene

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With sodium tetrafluoroborate; [Cu(salicylate)2(NCMe)]2; tetrabutyl-ammonium chloride; oxygen In tetrahydrofuran at 60℃; for 12h;85%
carbon monoxide
201230-82-2

carbon monoxide

para-diiodobenzene
624-38-4

para-diiodobenzene

methylmercury(II) iodide
143-36-2

methylmercury(II) iodide

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With dichloro bis(acetonitrile) palladium(II); tetra-(n-butyl)ammonium iodide In N,N,N,N,N,N-hexamethylphosphoric triamide under 760 Torr; for 5.5h; Ambient temperature;83%
4-Aminoacetophenone
99-92-3

4-Aminoacetophenone

bis(trifluoromethanesulfonyl)amide
82113-65-3

bis(trifluoromethanesulfonyl)amide

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
Stage #1: bis(trifluoromethanesulfonyl)amide With tert.-butylnitrite; acetic acid In ethanol Cooling with ice;
Stage #2: p-aminobenzophenone With tetraethylammonium iodide In water at 20℃;
81%
carbon monoxide
201230-82-2

carbon monoxide

tetramethylstannane
594-27-4

tetramethylstannane

4-iodobenzenediazonium tetrafluoroborate
1514-50-7

4-iodobenzenediazonium tetrafluoroborate

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
palladium diacetate In acetonitrile under 6619.6 Torr; for 1.5h; Heating;79%
With palladium diacetate In acetonitrile for 0.5h; Ambient temperature;79%
4-(2-methyl-[1,3]dioxolan-2-yl)-phenylamine
19073-16-6

4-(2-methyl-[1,3]dioxolan-2-yl)-phenylamine

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With N-iodo-succinimide; sodium nitrite In N,N-dimethyl-formamide at 20℃; for 4h;75%
Multi-step reaction with 2 steps
1: sodium nitrite; N-iodo-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C
2: sodium nitrite; N-iodo-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: sodium nitrite; N-iodo-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C
2: tert.-butylnitrite / water; ethanol / 2 h / 0 - 20 °C
3: sodium nitrite; N-iodo-succinimide / dimethyl sulfoxide / 2.5 h / 20 °C
View Scheme
4-ethyl-1-iodobenzene
25309-64-2

4-ethyl-1-iodobenzene

A

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

B

1-(4-iodophenyl)ethanol
68120-56-9, 104013-25-4, 53207-29-7

1-(4-iodophenyl)ethanol

Conditions
ConditionsYield
With 1-hydroxy-1,2-benzodioxol-3-(1H)-one; tris(2,2'-bipyridyl)ruthenium dichloride; water at 30℃; for 10h; Reagent/catalyst; Irradiation; Inert atmosphere;A 8%
B 71%
2-(4-iodophenyl)propan-2-ol
60514-82-1

2-(4-iodophenyl)propan-2-ol

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With bismuth(lll) trifluoromethanesulfonate; dipotassium peroxodisulfate; silver nitrate In water at 30℃; for 24h; Inert atmosphere; Green chemistry;71%
4-ethyl-1-iodobenzene
25309-64-2

4-ethyl-1-iodobenzene

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With tert.-butylhydroperoxide; C26H23ClN8ORu In water at 20℃; for 2h; Catalytic behavior; Schlenk technique;66%
With tert.-butylhydroperoxide at 90℃; for 5h; Neat (no solvent);
With calcined praseodymium incorporated AlPO-5 molecular sieves ((Al+P)/Pr = 25); air In neat liquid at 120℃; for 6h; Green chemistry;
With oxygen; Langlois reagent In acetonitrile at 25℃; under 760.051 Torr; for 12h; Irradiation; Green chemistry;96 %Chromat.
1,1,1,3',3',3'-hexafluoro-propanol
920-66-1

1,1,1,3',3',3'-hexafluoro-propanol

1-(4-(dichloro-λ3-iodanyl)phenyl)ethan-1-one
92527-07-6

1-(4-(dichloro-λ3-iodanyl)phenyl)ethan-1-one

A

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

B

Hexafluoroacetone
684-16-2

Hexafluoroacetone

Conditions
ConditionsYield
In dichloromethane-d2 at 20℃; for 20h; Inert atmosphere;A 65%
B n/a
4-(2-methyl-[1,3]dioxolan-2-yl)-phenylamine
19073-16-6

4-(2-methyl-[1,3]dioxolan-2-yl)-phenylamine

A

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

B

4-Aminoacetophenone
99-92-3

4-Aminoacetophenone

Conditions
ConditionsYield
With N-iodo-succinimide; sodium nitrite In N,N-dimethyl-formamide at 20℃; for 4h;A 31%
B 62%
4-acetyl-benzoic acid
586-89-0

4-acetyl-benzoic acid

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 1-iodo-butane; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; chloro-N,N,N',N'-bis(tetramethylene)formamidinium hexafluorophosphate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 120℃; for 16h; Sealed tube; Inert atmosphere;62%
potassium 4-acetylphenyltrifluoroborate

potassium 4-acetylphenyltrifluoroborate

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With chloroamine-T; sodium iodide In tetrahydrofuran; water at 20℃; for 1.5h;60%
α-(benzoyloxy)-p-iodoacetophenone
135774-36-6

α-(benzoyloxy)-p-iodoacetophenone

A

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

B

phenacyl benzoate
33868-50-7

phenacyl benzoate

Conditions
ConditionsYield
With 1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole; azobisisobutyronitrile In acetonitrile at 61℃; for 19h; Rate constant;A 19.6%
B 35%
1-(4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl)ethan-1-one
460088-33-9

1-(4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl)ethan-1-one

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With chloroamine-T; sodium iodide In tetrahydrofuran for 6h;30%
iodobenzene
591-50-4

iodobenzene

acetyl chloride
75-36-5

acetyl chloride

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
With carbon disulfide; aluminium trichloride
With aluminium trichloride
With aluminum (III) chloride In dichloromethane at 40℃; for 24h; Friedel-Crafts Acylation; Sealed tube; Inert atmosphere;
methyllithium
917-54-4

methyllithium

4-iodobenzoic acid chloride
1711-02-0

4-iodobenzoic acid chloride

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

Conditions
ConditionsYield
(i) CuI, Et2O, (ii) /BRN= 774718/, MeOH; Multistep reaction;
iodobenzene
591-50-4

iodobenzene

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

2-bromo-1-(4-iodophenyl)ethanone
31827-94-8

2-bromo-1-(4-iodophenyl)ethanone

Conditions
ConditionsYield
With bromine In 1,4-dioxane at 20℃; for 1h;100%
With bromine In 1,4-dioxane at 0 - 20℃; for 1 - 1.66667h; Product distribution / selectivity;100%
With bromine In chloroform at 20℃; for 4h;94%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

(E)-1-(4-iodophenyl)-3-(4-methoxyphenyl)prop-2-en-1-one
92855-02-2

(E)-1-(4-iodophenyl)-3-(4-methoxyphenyl)prop-2-en-1-one

Conditions
ConditionsYield
With potassium hydroxide In ethanol; water at 20℃; for 4.25h; Cooling with ice;100%
With sodium hydroxide In methanol at 0 - 20℃; for 4h; Claisen-Schmidt condensation;91%
With SiO2-H3PO4 Aldol Condensation; Microwave irradiation;88%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

1-(4-iodophenyl)ethanol
68120-56-9, 104013-25-4, 53207-29-7

1-(4-iodophenyl)ethanol

Conditions
ConditionsYield
With zirconium dioxide hydrate; isopropyl alcohol at 130℃; for 0.366667h; Meerwein-Ponndorf-Verley Reduction;100%
With C9H8BrMnN2O3; potassium tert-butylate In isopropyl alcohol at 30℃; for 168h; Inert atmosphere; Schlenk technique; Glovebox;99%
With sodium tetrahydroborate In ethanol for 5h;98.7%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 36h; Inert atmosphere;100%
With triethylamine In toluene at 20℃; for 24h; Inert atmosphere; Irradiation; Sealed tube;83.4%
With tris-(trimethylsilyl)silane In acetonitrile Schlenk technique; Inert atmosphere; Irradiation;80%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

phenylacetylene
536-74-3

phenylacetylene

4-(phenylethinyl)acetophenone
1942-31-0

4-(phenylethinyl)acetophenone

Conditions
ConditionsYield
With tetrabutylammonium acetate; copper aluminum In N,N-dimethyl-formamide at 110℃; for 24h; Sonogashira coupling;100%
With copper(l) iodide; triethylamine; triphenylphosphine In water at 60℃; for 24h; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere;100%
With sodium phosphate dodecahydrate In water; isopropyl alcohol at 80℃; for 1h; Reagent/catalyst; Sonogashira Cross-Coupling; Inert atmosphere;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

acrylic acid methyl ester
292638-85-8

acrylic acid methyl ester

methyl (2E)-3-(4-acetylphenyl)acrylate
71348-24-8, 71348-27-1

methyl (2E)-3-(4-acetylphenyl)acrylate

Conditions
ConditionsYield
With PdCl2[4,4'-bis(n-C10F21CH2OCH2)-2,2'-bipyridine]; triethylamine In N,N-dimethyl-formamide at 145℃; for 0.167h; Catalytic behavior; Reagent/catalyst; Heck Reaction; Microwave irradiation;100%
With trihexyl(tetradecyl)phosphonium chloride; sodium acetate; palladium diacetate In water at 50℃; for 2h; Heck reaction;99%
With C42H50Cl2N6Pd; sodium formate; triethylamine In N,N-dimethyl-formamide at 80℃; Heck Reaction; diastereospecific reaction;99%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

tetrabutylammonium triphenyldifluorosilicate

tetrabutylammonium triphenyldifluorosilicate

biphenyl-4-acetaldehyde
92-91-1

biphenyl-4-acetaldehyde

Conditions
ConditionsYield
bis(η3-allyl-μ-chloropalladium(II)) In N,N-dimethyl-formamide at 95℃; for 21h;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

(R)-(+)-1-(4-iodophenyl)ethanol
220089-24-7

(R)-(+)-1-(4-iodophenyl)ethanol

Conditions
ConditionsYield
With magnesium chloride In isopropyl alcohol at 25℃; pH=7; Catalytic behavior;100%
With (S,S)-RuCl2(2,2'-bis(di-3,5-xylylphosphino)-1,1'-binaphthyl)(1,1-dianisyl-2-isopropyl-1,2-ethylenediamine); potassium tert-butylate; hydrogen In isopropyl alcohol at 26 - 30℃; under 6080 Torr; for 4h;99.7%
With C37H40MnN2O2P2(1+)*Br(1-); sodium t-butanolate In isopropyl alcohol at 50℃; for 3h; Inert atmosphere; Schlenk technique; enantioselective reaction;98%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

(E)-2-pyridyldimethyl-(2-thien-2-ylethenyl)silane
321155-45-7

(E)-2-pyridyldimethyl-(2-thien-2-ylethenyl)silane

(E)-1-(4-acetyl)phenyl-2-(2-thienyl)ethene
63483-65-8

(E)-1-(4-acetyl)phenyl-2-(2-thienyl)ethene

Conditions
ConditionsYield
With bis(benzonitrile)palladium(II) dichloride; tetrabutyl ammonium fluoride In tetrahydrofuran at 60℃; Hiyama coupling;100%
acrylic acid n-butyl ester
141-32-2

acrylic acid n-butyl ester

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

(E)-3-(4-acetylphenyl)acrylic acid butyl ester
173464-57-8

(E)-3-(4-acetylphenyl)acrylic acid butyl ester

Conditions
ConditionsYield
With C29H33Cl2N5Pd; tetrabutylammomium bromide; sodium carbonate In N,N-dimethyl acetamide at 140℃; for 3h; Heck reaction; Inert atmosphere;100%
With tributyl-amine; chloro-[2-(9-phenyl-1,10-phenanthrolin-2-yl)phenyl]palladium In 1-methyl-pyrrolidin-2-one at 140℃; for 15h; Heck Reaction; Inert atmosphere;100%
With phenyl carbamate; potassium carbonate; palladium diacetate In N,N-dimethyl-formamide at 130℃; for 2h; Heck-type reaction;99%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

2-Methoxyphenylboronic acid
5720-06-9

2-Methoxyphenylboronic acid

4-acetyl-2'-methoxybiphenyl
52807-17-7

4-acetyl-2'-methoxybiphenyl

Conditions
ConditionsYield
With trihexyl(tetradecyl)phosphonium chloride; potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex In toluene at 50℃; for 1h; Suzuki cross-coupling;100%
With caesium carbonate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran Suzuki cross-coupling reaction; Heating;
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

phenylboronic acid
98-80-6

phenylboronic acid

biphenyl-4-acetaldehyde
92-91-1

biphenyl-4-acetaldehyde

Conditions
ConditionsYield
With trihexyl(tetradecyl)phosphonium chloride; potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex In toluene at 50℃; for 1h; Suzuki cross-coupling;100%
Stage #1: 4-Iodoacetophenone With tetrakis(triphenylphosphine) palladium(0) In 1-butyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide at 20 - 110℃; Suzuki coupling; Inert atmosphere; Ionic liquid;
Stage #2: phenylboronic acid With triethylamine In 1-butyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide; water at 20 - 110℃; Suzuki coupling; Ionic liquid; Inert atmosphere;
100%
With potassium carbonate In ethanol; water at 20℃; for 0.5h; Suzuki-Miyaura reaction; in air;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

2-methyl-but-3-yn-2-ol
115-19-5

2-methyl-but-3-yn-2-ol

1-(4-acetylphenyl)-3-methyl-1-butyn-3-ol
95785-28-7

1-(4-acetylphenyl)-3-methyl-1-butyn-3-ol

Conditions
ConditionsYield
With copper(l) iodide; 1-isobutyl-2,2,6,6-tetramethyl-phosphorinane*HBF4; diisopropylamine; bis(benzonitrile)palladium(II) dichloride In 1,4-dioxane at 20℃; for 6h; Sonogashira reaction;100%
With piperidine; copper(l) iodide; polystyrene-N(CH2PPh2)2PdCl2 In 1,4-dioxane at 60℃; for 2h; Sonogashira coupling reaction;94%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Inert atmosphere;90%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

4-Ethynylaniline
14235-81-5

4-Ethynylaniline

4-((4-aminophenyl)ethynyl)acetophenone
123770-68-3

4-((4-aminophenyl)ethynyl)acetophenone

Conditions
ConditionsYield
With triethylamine In water at 80℃; for 0.5h; Sonogashira Cross-Coupling;100%
With triethylamine; Nd2.04Cu0.95Pd0.05O4 In N,N-dimethyl-formamide at 120℃; for 16h; Sonogashira reaction;92%
With Pd/SiO2; triethylamine In diethyl ether; water at 20℃; for 10h; Sonogashira Cross-Coupling;86%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

4-Hydroxyacetophenone
99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With sodium hydroxide; copper(l) iodide; L-proline In water at 20 - 300℃; microwave irradiation;100%
Stage #1: 4-Iodoacetophenone With copper(l) iodide; tetra(n-butyl)ammonium hydroxide In water at 60℃; for 24h; Inert atmosphere; Sealed tube;
Stage #2: With hydrogenchloride In water; ethyl acetate at 20℃; for 2h; Inert atmosphere; chemoselective reaction;
96%
With copper(l) iodide; potassium hydroxide In water at 100℃; Inert atmosphere;96%
N,N,N,N,-tetramethylethylenediamine
110-18-9

N,N,N,N,-tetramethylethylenediamine

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

bis(dibenzylideneacetone)-palladium(0)
32005-36-0

bis(dibenzylideneacetone)-palladium(0)

PdI(4-MeCOC6H4)(N,N,N',N'-tetramethylethylenediamine)
191667-17-1

PdI(4-MeCOC6H4)(N,N,N',N'-tetramethylethylenediamine)

Conditions
ConditionsYield
In not given byproducts: dibenzylideneacetone; N2-atmosphere; according to Markies, A. J. et al.: J. Organomet. Chem. 482 (1994) 191; elem. anal.;100%
tert-Butyl acrylate
1663-39-4

tert-Butyl acrylate

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

(E)-tert-butyl 3-(4-acetylphenyl)prop-2-enoate
389091-50-3

(E)-tert-butyl 3-(4-acetylphenyl)prop-2-enoate

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride; palladium dichloride at 40℃; for 3h; Heck reaction; Inert atmosphere; neat (no solvent);100%
With tributyl-amine In N,N-dimethyl-formamide at 120℃; Heck-Mizoroki reaction;99%
With di-μ-iodobis(tri-tert-butylphosphino)dipalladium(l); N-ethyl-N,N-diisopropylamine In toluene at 100℃; for 15h; Heck Reaction; Inert atmosphere; Sealed tube; Glovebox;99%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

acrylic acid methyl ester
292638-85-8

acrylic acid methyl ester

methyl 4-acetylcinnamate

methyl 4-acetylcinnamate

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 0.25h; Heck Reaction;100%
With triethylamine In water; acetonitrile at 120℃; for 3h; Heck Reaction; Green chemistry;99%
With 3C22H14N3O2(1-)*Ho(3+)*Pd(2+)*2Cl(1-); potassium carbonate In N,N-dimethyl-formamide at 100℃; for 1h; Heck Reaction;99%
(4-methylphenyl)gold(triphenylphosphine)
40667-81-0

(4-methylphenyl)gold(triphenylphosphine)

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

1-{4-[2-(4-methylphenyl)ethynyl]phenyl}ethanone
123770-66-1

1-{4-[2-(4-methylphenyl)ethynyl]phenyl}ethanone

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; diisopropylamine; 1,2-bis-(diphenylphosphino)ethane In toluene at 130℃; for 16h; Sonogashira coupling; Inert atmosphere;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

4,4-dimethyl-1-phenyl-1-(pyridin-2-yl)pent-2-yn-1-ol
1046337-99-8

4,4-dimethyl-1-phenyl-1-(pyridin-2-yl)pent-2-yn-1-ol

2-(4-acetylphenyl)-3-tert-butyl-8a-phenylindolizin-1(8aH)-one
1227746-69-1

2-(4-acetylphenyl)-3-tert-butyl-8a-phenylindolizin-1(8aH)-one

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In acetonitrile at 90℃; for 13h;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

3-phenyl-1,1-di(pyridin-2-yl)prop-2-yn-1-ol
87446-01-3

3-phenyl-1,1-di(pyridin-2-yl)prop-2-yn-1-ol

2-(4-acetylphenyl)-3-phenyl-8a-(pyridin-2-yl)indolizin-1(8aH)-one
1383711-44-1

2-(4-acetylphenyl)-3-phenyl-8a-(pyridin-2-yl)indolizin-1(8aH)-one

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In acetonitrile at 90℃; for 13h;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

1-(4-iodophenyl)ethan-1-one oxime
27760-43-6

1-(4-iodophenyl)ethan-1-one oxime

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium acetate In ethanol; water at 95℃;100%
With hydroxylamine hydrochloride; sodium hydroxide In methanol at 20℃; Green chemistry;78%
With hydroxylamine hydrochloride; sodium acetate In ethanol; water for 1h; Reflux;
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

m-tolylboronic acid
17933-03-8

m-tolylboronic acid

4-acetyl-3'-methylbiphenyl
76650-29-8

4-acetyl-3'-methylbiphenyl

Conditions
ConditionsYield
With potassium carbonate In water; N,N-dimethyl-formamide at 80℃; for 0.333333h; Suzuki-Miyaura Coupling; Green chemistry;100%
With potassium carbonate In water at 25℃; for 2h; Suzuki Coupling; Schlenk technique;98%
With potassium carbonate In water at 20℃; for 4h; Catalytic behavior; Suzuki-Miyaura Coupling;100 %Chromat.
4,7-dichloroisatin
18711-13-2

4,7-dichloroisatin

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

4,7-dichloro-3-hydroxyl-3-[2-(4-iodophenyl-2-oxoethyl)]-1,3-dihydroindol-2-one
1037184-42-1

4,7-dichloro-3-hydroxyl-3-[2-(4-iodophenyl-2-oxoethyl)]-1,3-dihydroindol-2-one

Conditions
ConditionsYield
With diethylamine In methanol at 20℃;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

2-(2-(4-bromophenyl)-4-(4-ethylphenyl)-5-(4-methoxyphenyl)furan-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

2-(2-(4-bromophenyl)-4-(4-ethylphenyl)-5-(4-methoxyphenyl)furan-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

1-(4-(2-(4-bromophenyl)-4-(4-ethylphenyl)-5-(4-methoxyphenyl)furan-3-yl)phenyl)ethan-1-one

1-(4-(2-(4-bromophenyl)-4-(4-ethylphenyl)-5-(4-methoxyphenyl)furan-3-yl)phenyl)ethan-1-one

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; Schlenk technique;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

4,4'-diacetylbiphenyl
787-69-9

4,4'-diacetylbiphenyl

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; [2-(Pd-Cl)-4,4'-dichlorobenzophenone oxime]2 In decane; N,N-dimethyl-formamide at 110℃; for 5h; Ullmann homocoupling;99%
With potassium iodide; nickel dibromide; zinc In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide at 50℃; for 3h;98%
With potassium phosphate In water at 110℃; for 48h; Ullmann Condensation;98%
n-butyllithium
109-72-8, 29786-93-4

n-butyllithium

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

2-(4-iodophenyl)-2-hexanol
84735-52-4

2-(4-iodophenyl)-2-hexanol

Conditions
ConditionsYield
With cerium(III) triiodide In tetrahydrofuran; hexane at -65℃; for 3h;99%
Stage #1: n-butyllithium With cerium(III) chloride at -78℃;
Stage #2: 4-Iodoacetophenone at -78℃;
93%
With cerium(III) triiodide in THF, 1) -65 deg C, 30 min., 2) -65 deg C, 3h; Yield given. Multistep reaction;
ethanol
64-17-5

ethanol

4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

carbon monoxide
201230-82-2

carbon monoxide

ethyl-4-acetylbenzoate
38430-55-6

ethyl-4-acetylbenzoate

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium diacetate at 20 - 125℃; under 7500.75 - 22502.3 Torr; for 0.333333h; microwave irradiation;99%
With 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium diacetate at 125℃; under 7757.43 Torr; for 0.333333h; microwave irradiation;97%
With triethylamine at 100℃; under 3750.38 Torr; for 1.5h; Inert atmosphere;96%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

acrylic acid
79-10-7

acrylic acid

4-acetylcinnamic acid
18910-24-2

4-acetylcinnamic acid

Conditions
ConditionsYield
With potassium hydroxide In water at 90℃; for 5h; Mizoroki-Heck reaction;99%
With potassium hydroxide In methanol at 80℃; for 24h; Heck reaction;65%
With sodium carbonate; palladium dichloride In water at 100℃; Yield given;
With palladium diacetate; potassium carbonate In water at 120℃; for 0.416667h; Heck reaction; Microwave irradiation;
With potassium carbonate In water at 90℃; for 12h; Heck Reaction; Inert atmosphere;

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