Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:2398-37-0
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inquiryhigh quality Appearance:liquid Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1986.html Product Name 3-Bromoanisole CAS No. 2398-37-0 A
Cas:2398-37-0
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inquiryGood quantity 3-Bromoanisole Basic information Product Name: 3-Bromoanisole Synonyms: M-BROMOANISOLE;META BROMO ANISOLE;BROMOANISOLE(3-);1-BROMO-3-METHOXYBENZENE;5-bromoanisole;3-BROMO
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:2398-37-0
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
ProName: 3-Bromoanisole CasNo: 2398-37-0 Molecular Formula: C7H7BrO Appearance: liquid Application: Pharmaceutical intermediates DeliveryTime: 10day PackAge: According to the demand of customer Port: shanghai Prod
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inquiryProduct Name 3-Bromoanisole CAS NO 2398-37-0 Formula C7H7BrO Molecuht Weight 187.03 Appearance Clear colorless to
Our Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High q
Cas:2398-37-0
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:2398-37-0
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:2398-37-0
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
3-Bromoanisole CAS:2398-37-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
Cas:2398-37-0
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Product Detail Minimum Order Qty. 10 Gram
Cas:2398-37-0
Min.Order:10 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
3-Bromoanisole CAS:2398-37-0 Specification Item Standard Test Results Identification A.H-NMR:Comply with the structure Complies B.LC-MS:C
Cas:2398-37-0
Min.Order:1 Kilogram
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Type:Other
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Name:3-Bromoanisole Cas no.:2398-37-0 Stock:Fresh Purity:99.5% Standard: In-house Application:2398-37-0
Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
Cas:2398-37-0
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inquiryProduct Name: 3-Bromoanisole Synonyms: m-Bromophenylmethylether;m-Methoxybromobenzene;m-Methoxyphenyl bromide;m-Bromoanisoles;m-bromoanisole(MBA);3-BROMOANISOLE, 98+%;3-Bromoanisole99%;3-BROMO ANISOLE FOR SYNTHESIS CAS: 2398-37-0 MF: C7H7BrO
Cas:2398-37-0
Min.Order:100 Gram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:2398-37-0
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran for 16h; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | 92% |
Conditions | Yield |
---|---|
Stage #1: 3-Bromophenol With potassium carbonate In acetone for 0.25h; Stage #2: dimethyl sulfate In acetone for 10h; Reflux; | 95% |
With sodium hydroxide | |
With sodium hydroxide |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In sulfolane at 220℃; for 0.166667h; | 95% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 220℃; for 0.166667h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
Stage #1: methanol With tetrabutyl-ammonium chloride; potassium hydroxide In cyclohexane at 55℃; for 0.0833333h; Stage #2: m-nitrobromobenzene In cyclohexane at 55 - 60℃; for 3h; Reagent/catalyst; | 83% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium hydroxide In n-heptane at 20 - 50℃; for 3h; Reagent/catalyst; | 82% |
3-methoxyphenyl bromide
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; copper In acetonitrile at 20℃; for 0.75h; Substitution; | 78% |
With tetrabutylammomium bromide In acetonitrile at 60℃; for 0.75h; Substitution; | 72% |
Conditions | Yield |
---|---|
Stage #1: methanol With sodium hydride In tert-butyl methyl ether; mineral oil at 20℃; for 0.25h; Inert atmosphere; Sealed tube; Stage #2: 3-bromophenyl(mesityl)iodonium bromide In tert-butyl methyl ether; mineral oil at 50℃; for 1h; Inert atmosphere; Sealed tube; chemoselective reaction; | 77% |
(2,4,6-trimethylphenyl)(3’-methoxyphenyl)iodonium triflate
3-methoxyphenyl bromide
Conditions | Yield |
---|---|
With copper(I) bromide In acetonitrile at 80℃; for 2h; | 64% |
Conditions | Yield |
---|---|
Stage #1: m-Anisidine With Bromotrichloromethane; sodium nitrite In dichloromethane; water at 23℃; for 0.0833333h; Stage #2: With acetic acid In dichloromethane; water at 23℃; for 24h; Temperature; | 28% |
With sulfuric acid; sodium nitrite anschliessend Erwaermen mit Kupfer(I)-bromid; | |
With hydrogen bromide; sodium nitrite anschliessend Erwaermen mit Kupfer-Pulver; |
Conditions | Yield |
---|---|
With potassium hydroxide |
A
bromobenzene
B
iodobenzene
C
3-methoxyphenyl bromide
D
3-methoxy-1-iodobenzene
Conditions | Yield |
---|---|
With BrNBu4 In chloroform at 55℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous H2SO4 / Diazotization.Kochen der Diazoniumsalz-Loesung 2: aqueous NaOH View Scheme | |
Multi-step reaction with 2 steps 1: aqueous H2SO4 / Diazotization.Kochen der Diazoniumsalz-Loesung 2: aqueous KOH View Scheme |
(3-methoxyphenyl)(triphenyl-λ5-phosphanyl)gold
3-methoxyphenyl bromide
Conditions | Yield |
---|---|
With N-Bromosuccinimide In chloroform-d1 at 20℃; chemoselective reaction; | > 95 %Spectr. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 3-chloro-benzenecarboperoxoic acid 2: copper(I) bromide / acetonitrile / 2 h / 80 °C View Scheme |
(3-bromophenyl)boronic acid
3-methoxyphenyl bromide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere 1.2: 0.5 h / 20 °C 2.1: sodium hydride / tert-butyl methyl ether; mineral oil / 0.25 h / 20 °C / Inert atmosphere; Sealed tube 2.2: 1 h / 50 °C / Inert atmosphere; Sealed tube View Scheme |
3-bromo-4-iodoanisole
3-methoxyphenyl bromide
Conditions | Yield |
---|---|
With nickel(II) iodide; 1,4-bis(dicyclohexylphosphino)butane; sodium carbonate; cesium iodide In tetrahydrofuran at 35℃; for 72h; Irradiation; |
benzophenone
3-methoxyphenyl bromide
(3-methoxyphenyl)(diphenyl)methanol
Conditions | Yield |
---|---|
Stage #1: 3-methoxyphenyl bromide With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: benzophenone In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; | 100% |
With magnesium 1.) ether, 2.) a) RT, 6 h, b) reflux, 1 h; Yield given. Multistep reaction; | |
With n-butyllithium |
Conditions | Yield |
---|---|
With tetraphenyldisilane; cesium fluoride In acetonitrile at 100℃; for 0.0833333h; | 100% |
With tetrakis(triphenylphosphine) palladium(0); formaldehyd; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; | 85% |
With N,N,N,N,-tetramethylethylenediamine; C39H46IrN4 In acetonitrile at 45℃; for 48h; Sealed tube; Glovebox; Inert atmosphere; | 80% |
3-methoxyphenyl bromide
3-methoxy-benzaldehyde
bis(3-methoxyphenyl)methanol
Conditions | Yield |
---|---|
With n-butyllithium In hexane; ethyl acetate | 100% |
With magnesium In diethyl ether for 1h; Ambient temperature; | 62% |
With magnesium 1.) ether, ultrasound; Yield given. Multistep reaction; | |
Stage #1: 3-methoxyphenyl bromide With magnesium In tetrahydrofuran at 0℃; Reflux; Inert atmosphere; Stage #2: 3-methoxy-benzaldehyde In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Stage #3: With hydrogenchloride; water In tetrahydrofuran | |
Stage #1: 3-methoxyphenyl bromide With magnesium In diethyl ether at 20℃; for 2h; Inert atmosphere; Stage #2: 3-methoxy-benzaldehyde In diethyl ether at 20℃; for 2h; Inert atmosphere; |
3-methoxyphenyl bromide
Dichlorophenylphosphine
bis(3-methoxyphenyl)(phenyl)phosphine oxide
Conditions | Yield |
---|---|
Stage #1: 3-methoxyphenyl bromide With magnesium Metallation; Stage #2: Dichlorophenylphosphine Arylation; Stage #3: With water; dihydrogen peroxide In tetrahydrofuran Oxidation; Further stages.; | 100% |
With magnesium Yield given; |
Conditions | Yield |
---|---|
With potassium phosphate; 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride; bis(η3-allyl-μ-chloropalladium(II)) In 1,4-dioxane at 80℃; for 12h; Suzuki cross-coupling; | 100% |
With potassium carbonate In 5,5-dimethyl-1,3-cyclohexadiene | 100% |
With potassium phosphate; naphthidine di(radical cation)s-stabilized Pd nanoparticles In 1,4-dioxane at 80℃; for 5h; Suzuki-Miyaura cross-coupling reaction; | 99% |
3-methoxyphenyl bromide
acrylic acid n-butyl ester
(E)-n-butyl 3-(3-methoxyphenyl)acrylate
Conditions | Yield |
---|---|
With potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride In N,N-dimethyl acetamide at 140℃; for 12h; Heck reaction; | 100% |
With di-tert-butylneopentylphosphonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0) In N,N-dimethyl-formamide at 24℃; for 24h; Heck Reaction; Glovebox; | 98% |
With bis(1,1'-ethylene-3,3'-divinylimidazole-2,2'-diylidene)nickel(II) dibromide dihydrate; potassium carbonate In N,N-dimethyl-formamide at 100℃; for 4h; Heck Reaction; Inert atmosphere; Schlenk technique; | 96% |
Conditions | Yield |
---|---|
With Me2Zn(TMP)Li In tetrahydrofuran at 20℃; for 12h; | 100% |
With bis(2,2,6,6-tetramethylpiperidin-1-yl)magnesium-bis(lithium chloride) complex In tetrahydrofuran at -78 - 20℃; for 8h; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
With caesium carbonate; diisopropyl(2-tert-butyl)phenoxyphosphine; RhCl(PPh3)3 In toluene for 18h; Heating; | 100% |
3-methoxyphenyl bromide
m-Anisidine
3-methoxy-N-(3-methoxyphenyl)benzenamine
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 110℃; for 48h; Buchwald-Hartwig amination; | 100% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium t-butanolate In toluene at 100℃; for 18h; Buchwald-Hartwig Coupling; Inert atmosphere; | 72% |
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In toluene at 120℃; | 40% |
With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene for 72h; Reflux; Inert atmosphere; |
3-methoxyphenyl bromide
1-(3-Bromophenyl)ethanone
1-(3-bromo-phenyl)-1-(3-methoxy-phenyl)-ethanol
Conditions | Yield |
---|---|
Stage #1: 3-methoxyphenyl bromide With bromine; magnesium In diethyl ether at 20℃; Stage #2: 1-(3-Bromophenyl)ethanone In diethyl ether for 3h; Reflux; | 100% |
3-methoxyphenyl bromide
4-methyl-3-(triisopropylsilyloxy)aniline
N-(3-methoxyphenyl)-4-methyl-3-(triisopropylsilyloxy)aniline
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 31h; Buchwald-Hartwig Coupling; Inert atmosphere; | 100% |
3-methoxyphenyl bromide
Methyl 4-amino-2-methoxybenzoate
methyl 2-Methoxy-4-[(3-methoxyphenyl)amino]benzoate
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 21h; Inert atmosphere; | 100% |
3-methoxyphenyl bromide
1-amino-3-methylbenzene
3-methoxy-N-(3-methylphenyl)aniline
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 15h; Buchwald-Hartwig Coupling; Inert atmosphere; | 100% |
3-methoxyphenyl bromide
4-amino-2-(benzyloxy)benzonitrile
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 31h; Buchwald-Hartwig Coupling; | 100% |
imidazo[1,2-a]pyridine
3-methoxyphenyl bromide
3-(3-methoxyphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With C27H22N4O2Pd; potassium acetate In N,N-dimethyl acetamide at 140℃; for 18h; Catalytic behavior; Schlenk technique; Inert atmosphere; | 100% |
With palladium diacetate; potassium hydroxide In water at 100℃; for 24h; Inert atmosphere; | 53% |
3-methoxyphenyl bromide
(2-cyclopropylethynyl)trimethylsilane
1-(2-cyclopropylethynyl)-3-methoxybenzene
Conditions | Yield |
---|---|
Stage #1: 3-methoxyphenyl bromide With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; cesium fluoride In water at 20℃; for 0.25h; Sealed tube; Inert atmosphere; Stage #2: (2-cyclopropylethynyl)trimethylsilane In water at 80℃; for 16h; Sealed tube; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; L-lysine at 130℃; for 5h; Microwave irradiation; | 99% |
With copper(l) iodide; N-((4-nitro-1-oxy-pyridin-2-yl)methyl)oxalamic acid; tetrabutylammomium bromide; potassium hydroxide In water at 100℃; for 36h; Schlenk technique; Inert atmosphere; Sealed tube; | 99% |
With potassium tert-butylate; copper(I) oxide In N,N-dimethyl-formamide at 130℃; for 24h; | 91% |
N-Methylformamide
3-methoxyphenyl bromide
N-methyl-N-(3-methoxyphenyl)carboxamide
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; for 16h; | 99% |
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; for 16h; Arylation; | 98% |
3-methoxyphenyl bromide
bis(pinacol)diborane
2-(3-bromo-5-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1-(4,4'-di-tert-butyl-[2,2'-bipyridin]-6-yl)-2-(dimethyl(phenyl)silyl)-2,3-dihydro-1H-benzo[d][1,3,2]diazaborole Inert atmosphere; Schlenk technique; Sealed tube; | 99% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; cyclopentyl methyl ether; 1,1'-di(pyridin-2-yl)-1,1',3,3'-tetrahydro-2,2'-bibenzo[d][1,3,2]diazaborole at 100℃; for 16h; Schlenk technique; Inert atmosphere; | 96% |
With Pinacolborane; 4,4'-di-tert-butylbipyridine In cyclohexane at 80℃; | 77% |
3-methoxyphenyl bromide
4-methylphenylboronic acid
3-methoxy-4'-methylbiphenyl
Conditions | Yield |
---|---|
With cetyltrimethylammonim bromide; sodium hydroxide In water at 25℃; for 1h; Catalytic behavior; Suzuki Coupling; Microwave irradiation; | 99% |
With caesium carbonate; [PdCl(NNCNHC-nBu)]BF4 In water; N,N-dimethyl-formamide at 80℃; for 2h; Suzuki-Miyaura reaction; | 95% |
With potassium phosphate; N-[(4-diphenylphosphinophenyl)methyl] D-gluconamide; PdCl2(GLCAphos)2 In water at 80℃; for 16h; | 93% |
Conditions | Yield |
---|---|
With [Pd(N,N'-bis(2,6-bis(di-p-tolylmethyl)-4-methylphenyl)-imidazol-2-ylidene)(acetylacetonate)Cl]; lithium hexamethyldisilazane In 1,4-dioxane at 110℃; for 3h; Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube; | 99% |
With sodium t-butanolate; palladium diacetate In toluene at 80℃; for 0.5h; Buchwald-Hartwig amination; | 98% |
With C27H34N5P; sodium hydroxide; bis(dibenzylideneacetone)-palladium(0) In tert-Amyl alcohol at 100℃; Inert atmosphere; | 97.77% |
3-methoxyphenyl bromide
1-Naphthylboronic acid
1-(3-methoxybiphenyl)naphthalene
Conditions | Yield |
---|---|
With potassium fluoride; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane at 100℃; for 18h; Suzuki coupling; | 99% |
With KF; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In 1,2-dioxacyclohexane | 99% |
With potassium phosphate In ethanol; water at 20℃; for 1h; Suzuki-Miyaura Coupling; Inert atmosphere; Green chemistry; | 98% |
With ethyl 2-hydroxypropionate; palladium diacetate; potassium carbonate In water at 80℃; for 2h; Suzuki-Miyaura Coupling; Green chemistry; | 50% |
With Br(1-)*C25H29BrN5O6(1+); potassium carbonate In water at 100℃; for 2h; Suzuki-Miyaura coupling; | > 99 %Spectr. |
3-methoxyphenyl bromide
2-Methylphenylboronic acid
3'-methoxy-2-methyl-1,1'-biphenyl
Conditions | Yield |
---|---|
With cetyltrimethylammonim bromide; sodium hydroxide In water at 30℃; for 2h; Catalytic behavior; Temperature; Time; Suzuki Coupling; Microwave irradiation; | 99% |
With C20H12N2O8PdS2(2-)*2Na(1+); sodium hydroxide In water at 100℃; for 3h; | 95% |
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water for 24h; Heating; | 90% |
Conditions | Yield |
---|---|
With sodium azide In ethylene glycol at 100℃; for 3h; Green chemistry; | 99% |
With copper(l) iodide; sodium azide; sodium L-ascorbate; (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane In ethanol for 0.666667h; Heating; | 95% |
With copper(l) iodide; sodium azide; L-proline; sodium hydroxide In ethanol at 95℃; for 24h; | 92% |
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; L-proline In dimethyl sulfoxide at 90℃; for 31h; | 99% |
With potassium phosphate; copper(l) iodide; N-((1-oxy-pyridin-2-yl)methyl)oxalamic acid In dimethyl sulfoxide at 80℃; for 48h; Schlenk technique; Inert atmosphere; Sealed tube; chemoselective reaction; | 71% |
With 8-Hydroxyquinoline-N-oxide; caesium carbonate; copper(I) bromide In dimethyl sulfoxide at 50℃; for 60h; Ullmann coupling; Inert atmosphere; Sealed tube; chemoselective reaction; |
3-methoxyphenyl bromide
phenylacetylene
1-methoxy-3-(phenylethynyl)benzene
Conditions | Yield |
---|---|
With copper(l) iodide; ethanolamine; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran; water at 60℃; for 26h; Sonogashira coupling; | 99% |
With UC Pd; potassium carbonate; XPhos In ethanol; water at 50℃; for 5h; Sonogashira coupling; Inert atmosphere; | 95% |
With potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine In 1,4-dioxane at 105℃; for 20h; Sonogashira coupling; Inert atmosphere; | 94% |
3-methoxyphenyl bromide
Pentafluorobenzene
2,3,4,5,6-pentafluoro-3'-methoxy-1,1'-biphenyl
Conditions | Yield |
---|---|
With potassium phosphate; chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); Trimethylacetic acid In N,N-dimethyl acetamide at 80℃; Glovebox; | 99% |
With potassium phosphate; chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)] palladium(II); Trimethylacetic acid In N,N-dimethyl acetamide at 80℃; for 2 - 4h; | 98% |
With [Pd(trifluoroacetato)2(1,3-diisopropylbenzimidazolin-2-ylidene)(C2N3CH2Ph3)]; potassium carbonate In N,N-dimethyl acetamide at 120℃; for 24h; | 95% |
Conditions | Yield |
---|---|
With C34H52Cl2N2Pd; potassium carbonate; Trimethylacetic acid In N,N-dimethyl acetamide at 120℃; for 16h; Reagent/catalyst; | 99% |
With pentamethylcyclopentadienyltricarbonylrhenium for 2.5h; Schlenk technique; Inert atmosphere; UV-irradiation; | 92% |
With potassium tert-butylate at 100℃; for 24h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With bis(tri-ortho-tolylphosphine)palladium(0); (R)-(-)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyl-di-tert-butylphosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 80℃; for 5h; Inert atmosphere; | 99% |
With copper(l) iodide; 2-carboxyquinoline N-oxide; potassium carbonate; ammonium hydroxide In dimethyl sulfoxide at 80℃; for 23h; Inert atmosphere; | 93% |
With ammonium hydroxide; copper(l) iodide; diethylenetriaminopentaacetic acid; potassium hydroxide In water at 100℃; for 12h; Sealed tube; | 90% |
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