ProName: 3-Bromoaniline CasNo: 591-19-5 Appearance: Colorless liquid Application: Used as Pharmaceutical DeliveryTime:3 days after got PO# PackAge: 25kg/drum Port: Shanghai ProductionCapacity: 5000 Kilogram/Month
Cas:591-19-5
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:591-19-5
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inquiryhigh quality Appearance:Colorless liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
3-Bromoaniline CAS No.:591-19-5 Name: 3-Bromoaniline Synonyms: m-Bromoaniline; 3-bromobenzenamine Molecular Structure Molecular Formula: C6H6BrN Molecular Weight: 172.02 CAS Registry Number
Cas:591-19-5
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Description Name 3-Bromoaniline CAS 591-19-5 Assay 99% Appearance C
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryIdentification Product name: 3-bromoaniline Product name: 3-bromoaniline Molecular formula: C6H6BrN Molecular weight: 172.02 Structural formula:
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:591-19-5
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:591-19-5
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
CAS:591-19-5 EINECS:209-704-4 MW:172.02 MF:C6H6BrN Melting point:16.8 °C Boiling point:251 °C(lit.) Appearance:light yellow crystal Package:25kg/drum Transportation:by sea/air/courier Port:Shanghai
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Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:591-19-5
Min.Order:1 Kilogram
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Name 3-Bromoaniline Synonyms m-Bromoaniline; 3-bromobenzenamine Molecular Structure Molecular Formula
Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Prompt reaction, good quality and best service make us reliable and outstanding in this industry.Appearance:White to beige powder Stora
Cas:591-19-5
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inquirylow price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China
Conditions | Yield |
---|---|
With hydrazine In ethanol at 80℃; for 0.333333h; Catalytic behavior; chemoselective reaction; | 99.5% |
With hydrogen In water at 120℃; under 15001.5 Torr; for 5h; Green chemistry; chemoselective reaction; | 99% |
With sodium tetrahydroborate In methanol at 25℃; for 1h; Sealed tube; | 98% |
Conditions | Yield |
---|---|
With copper(l) iodide; ascorbic acid In ammonia at 25℃; for 18h; liquid NH3; | 99% |
With copper(I) oxide; ammonium hydroxide; C17H14N2O3; potassium hydroxide In ethanol at 60℃; for 24h; Schlenk technique; Inert atmosphere; | 93% |
With iron(III) oxide; sodium hydroxide; copper(l) iodide; ammonia In ethanol; water at 90℃; for 16h; | 89% |
With acetamidine hydrochloride; caesium carbonate In N,N-dimethyl-formamide at 130℃; for 20h; Inert atmosphere; Green chemistry; | 72% |
tert-butyl (3-bromophenyl)carbamate
3-bromoaniline
Conditions | Yield |
---|---|
With molecular sieve; boron trifluoride diethyl etherate In dichloromethane Ambient temperature; | 98% |
1,2-bis(3-bromophenyl)diazene
3-bromoaniline
Conditions | Yield |
---|---|
With potassium hydroxide; nickel-incorporated hexagonal mesoporous aluminophosphate In isopropyl alcohol at 82.84℃; for 1.5h; | 90% |
With potassium hydroxide; isopropyl alcohol; molecular sieve at 82.84℃; for 3h; | 85 % Chromat. |
Conditions | Yield |
---|---|
Stage #1: 3-bromoacetanilide With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.05h; Inert atmosphere; Stage #2: With water In tetrahydrofuran Inert atmosphere; | 90% |
3-bromoaniline
Conditions | Yield |
---|---|
With hydrogenchloride; water at 190℃; for 3h; | 78% |
Conditions | Yield |
---|---|
With methanol; O-benzenesulfonyl-acetohydroxamic acid ethyl ester; toluene-4-sulfonic acid for 24h; Inert atmosphere; Reflux; | 78% |
3-bromobenzamide
3-bromoaniline
Conditions | Yield |
---|---|
With sodium hydroxide; benzyltrimethylazanium tribroman-2-uide In water for 1h; Ambient temperature; | 76% |
With potassium hypobromite at 70 - 75℃; | |
Multi-step reaction with 2 steps 1: alkaline aqueous sodium hypobromite solution 2: aqueous NaOH-solution View Scheme |
3-bromophenyl magnesium bromide
3-bromoaniline
Conditions | Yield |
---|---|
Stage #1: 3-bromophenyl magnesium bromide With zinc(II) chloride In tetrahydrofuran at -3℃; for 0.0833333h; Stage #2: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone In tetrahydrofuran at 20℃; for 3h; Stage #3: With hydrogenchloride In tetrahydrofuran at 20℃; for 4h; | 70% |
Conditions | Yield |
---|---|
With methanesulfonic acid; trimethylsilylazide In tetrachloromethane at 80℃; for 4h; | 70% |
3-bromophenylhydrazine
3-bromoaniline
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel dichloride In methanol at 20℃; for 0.5h; | 65% |
2-(3-bromophenoxy)propanamide
3-bromoaniline
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 140℃; for 4h; Green chemistry; | 65% |
Conditions | Yield |
---|---|
With bromine; hydrogen fluoride; antomony(V) at -40℃; for 0.25h; | A 29% B 62% C 3% |
With bromine; hydrogen fluoride; antomony(V) at -40℃; for 0.25h; Mechanism; Product distribution; dependence of product distribution on ammount of catalyst; |
Conditions | Yield |
---|---|
With water; sodium acetate; acetic acid In ethanol at 70℃; for 38h; | A 30% B 61% |
(3-bromophenyl)boronic acid
3-bromoaniline
Conditions | Yield |
---|---|
With O-(2,4-dinitrophenyl)hydroxylamine In toluene at 50℃; for 24h; Inert atmosphere; | 54% |
With copper(I) oxide; ammonium hydroxide In water for 0.0833333h; Microwave irradiation; |
ethanol
3-Bromonitrobenzene
A
3-bromo-bisethyl-aminobenzene
B
3-bromoaniline
Conditions | Yield |
---|---|
With Au NCs/TiO2 for 4h; Kinetics; Reagent/catalyst; Inert atmosphere; UV-irradiation; | A 21.3% B 52.1% |
bromobenzene
A
3-bromoaniline
B
4-bromo-aniline
C
2-bromoaniline
Conditions | Yield |
---|---|
With tris-(2-chloro-ethyl)-amine; trifluorormethanesulfonic acid; trifluoroacetic acid In chloroform at 60℃; for 3h; | A 10% B 25% C 30% |
With hydroxylamine-O-sulfonic acid; iron(II) sulfate In water; acetic acid at 40℃; for 2h; Yield given. Yields of byproduct given; | |
With hydroxylamine-O-sulfonic acid; iron(II) sulfate In water; acetic acid at 40℃; for 2h; Product distribution; Mechanism; k(C6H5Br)/k(C6H6); |
1-methyl-4-nitrosobenzene
3-bromo-benzoic acid bromoamide
A
m-bromobenzoic acid
B
3-bromoaniline
Conditions | Yield |
---|---|
at 30℃; Kinetics; |
Conditions | Yield |
---|---|
With PPA; hydroxylamine | |
With thionyl chloride; hydroxylamine-O-sulfonic acid 1) 1h, reflux, 2) toluene, 4h, reflux; Yield given. Multistep reaction; |
3-Bromonitrobenzene
A
3-bromoaniline
B
1,2-bis(3-bromophenyl)diazene
Conditions | Yield |
---|---|
With potassium hydroxide; palladium on activated charcoal; hydrazine |
3-bromo-benzoic acid bromoamide
3-bromoaniline
Conditions | Yield |
---|---|
With sodium hydroxide |
N,N'-bis-(3-bromo-phenyl)-formamidine
N-phenylacetoacetamide
B
3-bromoaniline
Conditions | Yield |
---|---|
at 140℃; |
dimethylsulfide
1-azido-3-bromobenzene
A
4-amino-2-bromophenyl methyl sulphide
C
2-amino-4-bromophenyl methyl sulphide
D
3-bromoaniline
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; trifluoroacetic acid at 25℃; for 4h; | A 18 % Chromat. B 18 % Chromat. C 23 % Chromat. D 25 % Chromat. |
With trifluorormethanesulfonic acid; trifluoroacetic acid at 25℃; for 4h; Title compound not separated from byproducts; | A 18 % Chromat. B 18 % Chromat. C 23 % Chromat. D 25 % Chromat. |
N-(3-bromo-phenyl)-3-oxo-butyramide
A
4-methyleneoxetan-2-one
B
3-bromoaniline
Conditions | Yield |
---|---|
In cyclohexane at 25℃; Equilibrium constant; |
Conditions | Yield |
---|---|
With hydrogenchloride; 2H(1+)*2H3N*Cl3Cu(2-) In acetic acid at 90℃; Rate constant; other solvent, other temp., other Cu(I) complex; |
3-amino-1,2-dibromobenzene
A
3-bromo-4-chloroaniline
B
3,4-dibromoaniline
C
2,3,4-tribromoaniline
E
3-bromoaniline
Conditions | Yield |
---|---|
With copper(l) chloride In hydrogenchloride; acetic acid at 90℃; Rate constant; |
Conditions | Yield |
---|---|
With hydrogenchloride; copper(l) chloride In acetic acid at 90℃; for 45h; CuCl2; |
1-(3-bromophenyl)-2,2,5,5-tetramethyl-1,2,5-azadisilolidine
3-bromoaniline
Conditions | Yield |
---|---|
With methanol; toluene-4-sulfonic acid In diethyl ether Yield given; |
N-(3-bromophenyl)-O-pivaloylhydroxylamine
A
2-bromo-1,4-benzoquinone
B
4-amino-2-bromophenol
C
3-bromo-4-chloroaniline
D
3-bromoaniline
Conditions | Yield |
---|---|
With hydrogenchloride In water; acetonitrile at 40℃; Mechanism; Rate constant; | A 15.1 % Chromat. B 0.2 % Chromat. C 3.3 % Chromat. D 33 % Chromat. |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 10 - 20℃; for 4h; | 100% |
With sulfuric acid at 0 - 20℃; for 0.0833333h; | 99% |
With sulfuric acid for 0.0833333h; | 98% |
diethyl 2-ethoxymethylenemalonate
3-bromoaniline
ethyl α-carbethoxy-β-m-bromoanilinoacrylate
Conditions | Yield |
---|---|
at 90 - 110℃; for 1h; | 100% |
In toluene at 110℃; for 24h; | 100% |
In toluene for 1h; Inert atmosphere; Reflux; | 91% |
p-toluenesulfonyl chloride
3-bromoaniline
N-(3-bromophenyl)-4-methyl-benzenesulfonamide
Conditions | Yield |
---|---|
With pyridine for 0.333333h; Tosylation; Heating; | 100% |
With pyridine at 0 - 20℃; for 10h; | 99% |
for 0.1h; microwave irradiation; | 88% |
pent-4-enoic acid
3-bromoaniline
pent-4-enoic acid (3-bromo-phenyl)-amide
Conditions | Yield |
---|---|
With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane | 100% |
With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide Acylation; |
Conditions | Yield |
---|---|
With sodium carbonate; palladium diacetate In methanol Heating / reflux; | 100% |
With palladium diacetate; sodium carbonate In methanol Suzuki Coupling; Reflux; Inert atmosphere; | 100% |
With palladium diacetate; sodium carbonate In methanol Reflux; | 100% |
bis(trichloromethyl) carbonate
3-bromoaniline
3-Bromophenyl isocyanate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
With triethylamine In toluene for 7h; Reflux; Cooling with ice; | 70.7% |
With triethylamine In benzene for 3h; Heating; |
ethyl 2,4-dichloropyrimidine-5-carboxylate
3-bromoaniline
ethyl 4-(3-bromoanilino)-2-chloropyrimidine-5-carboxylate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile for 1h; Heating; | 100% |
Conditions | Yield |
---|---|
Stage #1: formaldehyd With sulfuric acid In tetrahydrofuran; water at 0℃; for 0.166667h; Stage #2: m-Bromoaniline With sodium tetrahydroborate In tetrahydrofuran; water at 20℃; for 1h; | 100% |
Stage #1: formaldehyd With sulfuric acid In tetrahydrofuran; water at 0℃; for 0.166667h; Stage #2: m-Bromoaniline In tetrahydrofuran; water for 0.333333h; Stage #3: With sodium tetrahydroborate In tetrahydrofuran; water at 0 - 20℃; for 1.5h; | 98% |
With sodium tetrahydroborate; sulfuric acid In tetrahydrofuran; water Inert atmosphere; | 94% |
di-tert-butyl dicarbonate
3-bromoaniline
tert-butyl (3-bromophenyl)carbamate
Conditions | Yield |
---|---|
In sodium hydroxide | 100% |
In sodium hydroxide | 100% |
In dichloromethane at 20℃; for 18h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: m-Bromoaniline With hydrogenchloride In water at 0℃; Stage #2: With sodium nitrite In water at 0℃; for 0.333333h; Stage #3: With sodium azide In water at 0℃; for 3h; | 100% |
Stage #1: m-Bromoaniline With hydrogenchloride In water at 0 - 5℃; for 0.5h; Stage #2: With sodium azide; sodium nitrite In water at 0 - 5℃; for 1h; | 97% |
Stage #1: m-Bromoaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h; Stage #2: With sodium azide In water at 0℃; for 1h; | 94.5% |
Conditions | Yield |
---|---|
In toluene Heating; | 100% |
N′-(2-cyano-4-nitrophenyl)-N,N-dimethylformimidamide
3-bromoaniline
6-nitro-4-(3-bromophenylaniline)quinazoline
Conditions | Yield |
---|---|
In acetic acid at 148℃; for 1.5h; | 100% |
With acetic acid for 2h; Reflux; | 93% |
With acetic acid Reflux; | 85% |
C11H11ClN2O3
3-bromoaniline
4-[(3-bromo-phenyl)amino]-6-methylcarbonyloxy-7-methoxy-quinazoline
Conditions | Yield |
---|---|
In isopropyl alcohol at 110℃; for 3h; | 100% |
di-tert-butyl dicarbonate
3-bromoaniline
B
tert-butyl (3-bromophenyl)carbamate
Conditions | Yield |
---|---|
In sodium hydroxide | A 100% B n/a |
di-tert-butyl dicarbonate
3-bromoaniline
B
tert-butyl (3-bromophenyl)carbamate
Conditions | Yield |
---|---|
In sodium hydroxide | A 100% B n/a |
Conditions | Yield |
---|---|
With potassium carbonate; bis(tri-t-butylphosphine)palladium(0) In methanol; water; toluene at 135℃; for 0.583333h; Irradiation; | 100% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water; N,N-dimethyl-formamide at 80℃; for 16h; Sealed tube; | 100% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In 1,4-dioxane; water at 80℃; for 8h; Suzuki Coupling; Inert atmosphere; |
Conditions | Yield |
---|---|
100% |
N-[4-chloro-6-(2-phenylethyl)-7H-pyrrolo[2,3-d]pyrimidin-2-yl]-2,2-dimethylpropanamide
3-bromoaniline
N-{4-(3-bromophenylamino)-6-(2-phenylethyl)-7H-pyrrolo[2,3-d]pyrimidin-2-yl}-2,2-dimethylpropanamide
Conditions | Yield |
---|---|
With hydrogenchloride In isopropyl alcohol Heating; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water at 70℃; for 14h; | 100% |
With potassium carbonate In acetonitrile at 100℃; for 29h; | 95% |
With potassium carbonate In acetonitrile at 80℃; Inert atmosphere; | 93% |
cycl-isopropylidene malonate
3-bromoaniline
5-(((3-bromophenyl)amino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione
Conditions | Yield |
---|---|
Stage #1: cycl-isopropylidene malonate; trialkyl orthoformate for 1h; Reflux; Stage #2: m-Bromoaniline for 2h; Reflux; | 100% |
Conditions | Yield |
---|---|
With triethylamine at 0℃; for 1h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 0℃; for 1.25h; Inert atmosphere; | 99% |
at -77℃; | |
With sodium hydrogencarbonate In ethyl acetate at 0 - 20℃; |
Conditions | Yield |
---|---|
With pyridine at 50℃; | 100% |
With pyridine In dichloromethane at 0 - 20℃; for 16h; | 83% |
3-bromoaniline
bis(pinacol)diborane
3-aminophenylboronic acid pinacolate
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane for 2.75h; Inert atmosphere; Reflux; | 100% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane for 2.75h; Inert atmosphere; Reflux; | 100% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane at 110℃; for 2.75h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 160℃; for 36h; | 100% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 2h; | 99.3% |
With triethylamine In dichloromethane at 0℃; for 2h; | 99.3% |
With triethylamine In dichloromethane at 0℃; for 2h; | 99.3% |
3-bromoaniline
malononitrile
2-[(3-bromophenyl)-hydrazono]malononitrile
Conditions | Yield |
---|---|
Stage #1: m-Bromoaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h; Stage #2: malononitrile With sodium acetate In water at 0℃; for 2h; | 99% |
Stage #1: m-Bromoaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h; Stage #2: malononitrile With sodium acetate In water at 0℃; for 2h; | 97% |
Stage #1: m-Bromoaniline With hydrogenchloride; sodium nitrite at 20℃; for 0.166667h; Stage #2: malononitrile With sodium acetate In methanol at 0 - 20℃; for 3.5h; | 30% |
3,5-dimethylphenyl boronic acid
3-bromoaniline
3-amino-3',5'-dimethylbiphenyl
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; cesium fluoride In tetrahydrofuran at 20℃; for 2h; Suzuki coupling; | 99% |
With cesium fluoride; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In tetrahydrofuran at 20℃; for 2h; Suzuki Coupling; | 99% |
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; L-proline; PS[DMVBIM][Pro] In dimethyl sulfoxide at 120℃; for 60h; | 99% |
With copper(l) iodide; potassium carbonate; heptakis(6-amino-6-deoxy)-β-cyclodextrin In dimethyl sulfoxide at 110℃; for 36h; Sealed tube; | 90% |
With copper(I) oxide; 4,7-dimethoxy-1,10-phenanthroline; caesium carbonate; ethylene glycol; poly(ethylene glycol) In various solvent(s) at 110℃; for 20h; | 88% |
3-bromoaniline
isoquinoline 5-boronic acid
1-amino-3-isoquinolylbenzene
Conditions | Yield |
---|---|
Stage #1: m-Bromoaniline; isoquinoline 5-boronic acid With sodium carbonate; tetrakis-(triphenylphosphino)-palladium(0) In 1,2-dimethoxyethane for 48h; Suzuki cross-coupling reaction; Heating; Stage #2: In tetrahydrofuran for 1h; | 99% |
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