CAS No.100-01-6,4-Nitroaniline Suppliers

: 100-25-4
para-dinitrobenzene

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With formic acid In acetonitrile at 20℃; for 1h; Irradiation;	100%
In water at 25℃; for 0.333333h; Sonication;	99%
With sodium tetrahydroborate In water at 95℃; for 0.333333h; Green chemistry;	98%

: 1516-60-5
4-nitrophenyl azide

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With 1,1,1,3',3',3'-hexafluoro-propanol; tetrabutylammonium perchlorate In N,N-dimethyl-formamide electrolytic reduction at a Pt gauze electrode at a potential of -0.30 V;	100%
With Decaborane; palladium on activated charcoal In methanol at 20℃; for 0.25h;	99%
With triethylsilane; indium(III) chloride In acetonitrile at -20℃; for 0.25h;	99%

: 77853-01-1
(4-nitro-phenyl)-m-tolyl sulfone

A: 100-32-3
di(p-nitrophenyl) disulfide

B: 77853-09-9
Toluene-3-thiosulfonic acid; compound with ammonia

C: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With sulfur; ammonia at 100℃; for 2h; titanium autoclave;	A 43% B 100% C 40%

...Expand

: 22865-57-2
1-methoxy-4-((4-nitrophenyl)sulfonyl)benzene

A: 100-32-3
di(p-nitrophenyl) disulfide

B: 77853-03-3
4-Methoxy-benzenethiosulfonic acid; compound with ammonia

C: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With sulfur; ammonia at 100℃; for 2h; titanium autoclave;	A 56% B 100% C 32%
With sulfur; ammonia at 100℃; for 2h; Product distribution; titanium autoclave; various reactions temp. and amounts of S8;

...Expand

: 1984-23-2
p-nitrophenyl isocyanide

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With graphitic carbon nitride; hydrazine hydrate In water at 70℃; for 8h; Time; Darkness; Sealed tube; Green chemistry; chemoselective reaction;	100%

: 100-00-5
4-chlorobenzonitrile

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With ammonium hydroxide at 120 - 190℃; under 45004.5 - 46504.7 Torr; for 4h; Temperature; Pressure;	99.31%
With ammonium hydroxide; copper(l) iodide at 200℃; for 6.5h; Reagent/catalyst; Temperature; Time; Autoclave; Green chemistry;	97%
With copper(ll) sulfate pentahydrate; ammonium hydroxide In PEG1000-DIL; methyl cyclohexane at 60℃; for 4h;	96%

: 18437-63-3
tert-butyl N-(4-nitrophenyl)carbamate

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With EPZG clay In dichloromethane for 1.5h; deacylation; Heating;	99%
With H-β zeolite In dichloromethane for 4h; Heating;	98%
With water at 150℃; for 10h; Subcritical conditions;	97%

: 636-98-6
p-nitrobenzene iodide

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With copper(l) iodide; ascorbic acid In ammonia at 25℃; for 18h; Kinetics; liquid NH3;	99%
With ammonium hydroxide; copper(l) iodide; phosphate potassium salt In N,N-dimethyl-formamide at 20℃; for 36h; Inert atmosphere;	98%
Stage #1: p-nitrobenzene iodide With copper(l) iodide; D-glucosamine hydrochloride; potassium carbonate In water; acetone at 90℃; for 0.166667h; Stage #2: With ammonia In water; acetone at 90℃; for 28h;	98%

: 586-78-7
para-nitrophenyl bromide

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
Stage #1: para-nitrophenyl bromide With copper(l) iodide; D-glucosamine hydrochloride; potassium carbonate In water; acetone at 90℃; for 0.166667h; Stage #2: With ammonia In water; acetone at 90℃; for 28h;	98%
With ammonium hydroxide at 20℃; for 3h; Catalytic behavior;	98%
With ammonia; triethylamine In water at 20℃; for 2.5h;	98%

: 63-68-3
L-methionine

: 74197-40-3
3,5-dinitro-1-(4-nitrophenyl)-4-pyridone

A: 100-01-6
4-nitro-aniline

B: 92782-41-7
(S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-4-methylsulfanyl-butyric acid

Conditions

Conditions	Yield
In pyridine; water for 3h; Ambient temperature;	A n/a B 98%

...Expand

: 90-15-3
α-naphthol

: 64168-52-1
4'-nitrobenzenesulfenanilide

A: 68143-73-7
2-phenylthio-1-naphthol

B: 19133-53-0
4-(phenylthio)naphthalen-1-ol

C: 100-01-6
4-nitro-aniline

D: 103929-98-2
2,4-bis(phenylthio)naphthalen-1-ol

Conditions

Conditions	Yield
With trifluoroacetic acid In benzene for 0.166667h; Ambient temperature; Further byproducts given;	A 42% B 33% C 98% D 10%

...Expand

: 90-15-3
α-naphthol

: 64168-52-1
4'-nitrobenzenesulfenanilide

A: 68143-73-7
2-phenylthio-1-naphthol

B: 19133-53-0
4-(phenylthio)naphthalen-1-ol

C: 100-01-6
4-nitro-aniline

D: 882-33-7
diphenyldisulfane

Conditions

Conditions	Yield
With trifluoroacetic acid In benzene for 0.166667h; Ambient temperature; Further byproducts given;	A 42% B 33% C 98% D 14%

...Expand

: 90-15-3
α-naphthol

: 64168-52-1
4'-nitrobenzenesulfenanilide

A: 68143-73-7
2-phenylthio-1-naphthol

B: 19133-53-0
4-(phenylthio)naphthalen-1-ol

C: 100-01-6
4-nitro-aniline

D: 103929-98-2
2,4-bis(phenylthio)naphthalen-1-ol

E: 882-33-7
diphenyldisulfane

Conditions

Conditions	Yield
With trifluoroacetic acid In benzene for 0.166667h; Product distribution; Mechanism; 1.5 eqiv. TFA;	A 42% B 33% C 98% D 10% E 14%

...Expand

: 64168-52-1
4'-nitrobenzenesulfenanilide

A: 1212-08-4
S-Phenyl benzenethiosulfonate

B: 100-01-6
4-nitro-aniline

C: 882-33-7
diphenyldisulfane

Conditions

Conditions	Yield
With trifluoroacetic acid In benzene at 25℃; Product distribution; Mechanism; further sulfenanilide;	A 32% B 98% C 56%

...Expand

: 76-05-1
trifluoroacetic acid

: S,S-di-n-butyl-N-(4-nitrophenyl)imino-λ4-sulfane

A: 2168-93-6
butyl sulfoxide

B: 404-27-3
2,2,2-trifluoro-N-(4-nitrophenyl)acetamide

C: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
at 72℃; for 72h; Elimination; acylation; retro-Pummerer reaction;	A 79% B 98% C 2%

...Expand

: 104-04-1
N-(4-Nitrophenyl)acetamide

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With ammonium iodide; hydrazine hydrate In ethanol at 60℃; for 42h; Inert atmosphere; Sealed tube;	97%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In methanol for 1h; Product distribution; Further Variations:; Solvents; reaction time; Heating;	96%
With 40% potassium fluoride/alumina at 85℃; for 0.0666667h; Microwave irradiation; Neat (no solvent);	94%

: 3393-96-2
p-nitrobenzanilide

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In methanol for 1.5h; Product distribution; Further Variations:; Solvents; reaction time; Heating;	97%
In methanol

: 16169-16-7
4-Nitro-N-phenylhydroxylamine

: 88867-70-3
C11H14N2O4

A: 4485-08-9
4-nitrosonitrobenzene

B: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With iron(II) chloride In water; acetonitrile at 40℃; pH=4.7, ionic strength=0.5 M;	A 39% B 95%
With iron(II) chloride In water; acetonitrile at 40℃; Mechanism; pH=4.7, ionic strength=0.5 M;

...Expand

: 88867-70-3
C11H14N2O4

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With iron(II) chloride In water; acetonitrile at 40℃; pH=4.7, ionic strength=0.5 M;	95%
With FeCl2 or CuCl In water; acetonitrile at 40℃; Product distribution; Mechanism; pH=4.7, ionic strength=0.5 M;

: 108047-30-9
3-methyl-1-(4-nitrophenyl)-5-nitrouracil

: 74-89-5
methylamine

A: 41613-26-7
1,3-dimethyl-5-nitrouracil

B: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
In methanol for 0.5h; Ambient temperature;	A 95% B n/a

...Expand

: 1516-60-5
4-nitrophenyl azide

: 105-53-3
diethyl malonate

A: 5256-74-6
1,3-diethyl 2-diazopropanedioate

B: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With tetrabutylammonium perchlorate In N,N-dimethyl-formamide electrolytic reduction at a Pt gauze electrode at a potential of -0.30 V;	A 95% B 101 %

...Expand

: 78596-42-6
ethyl α-ethoxycarbonyl-β-(4-nitroanilino)acrylate

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With ethylenediamine In ethanol at 20℃; for 2.3h;	95%

: 110-86-1
pyridine

: 74197-40-3
3,5-dinitro-1-(4-nitrophenyl)-4-pyridone

A: 100-01-6
4-nitro-aniline

B: 139055-63-3
1-Hydroxy-3,5-dinitro-1H-pyridin-4-one; compound with pyridine

Conditions

Conditions	Yield
With hydroxylamine hydrochloride at 20℃; for 2h;	A 94% B 83%

...Expand

: 77863-74-2
C14H13NO5S

A: 100-32-3
di(p-nitrophenyl) disulfide

B: 77853-06-6
3-Ethoxy-benzenethiosulfonic acid; compound with ammonia

C: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With sulfur; ammonia at 100℃; for 2h; titanium autoclave;	A 47% B 94% C 40%

...Expand

: 88867-70-3
C11H14N2O4

: 823-86-9
N-(4-chlorophenyl)hydroxylamine

A: 932-98-9
1-chloro-4-nitroso-benzene

B: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With iron(II) chloride In water; acetonitrile at 40℃; pH=4.7, ionic strength=0.5 M;	A 53% B 94%
With iron(II) chloride In water; acetonitrile at 40℃; Mechanism; pH=4.7, ionic strength=0.5 M;

...Expand

: 98-95-3
nitrobenzene

A: 659-49-4
4-nitrosoaniline

B: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With pyrene; tetramethyl ammoniumhydroxide; benzamide; potassium carbonate In dimethyl sulfoxide at 90℃; for 2.08333 - 2.16667h; Conversion of starting material;	A 94% B 6%
With potassium hydroxide; pyrene; potassium carbonate; urea In dimethyl sulfoxide at 90℃; for 2.08333 - 2.16667h; Conversion of starting material;	A 87% B 12%
With urea, monopotassium salt; urea In dimethyl sulfoxide at 90℃; for 2h;	A 56% B 5.5%

: 62-53-3
aniline

: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With Vilsmeier reagent; potassium nitrate In neat (no solvent) at 100℃; under 1500.15 Torr; Reagent/catalyst; Temperature; Microwave irradiation;	93%
With nitric acid; sodium dodecyl-sulfate In water at 25℃; for 0.333333h; Micellar solution; Green chemistry; regioselective reaction;	86%
With nitric acid; sodium dodecyl-sulfate In acetonitrile at 24.84℃; for 3h; Micellar solution; regioselective reaction;	85%

: 110-86-1
pyridine

: 74197-40-3
3,5-dinitro-1-(4-nitrophenyl)-4-pyridone

A: 100-01-6
4-nitro-aniline

B: 4-aci-Nitro-4H-isoxazol-5-one; compound with pyridine

Conditions

Conditions	Yield
With hydroxylamine hydrochloride at 20℃; for 2h;	A 93% B 88%

...Expand

: 100-25-4
para-dinitrobenzene

A: 16169-16-7
4-Nitro-N-phenylhydroxylamine

B: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With 1,2-bis(mercaptomethyl)benzene; (Et4N) In acetonitrile at 26℃; for 1.5h;	A 93% B 2%
With D-glucose; bakers' yeast In phosphate buffer; ethanol at 30℃; for 0.5h; pH=6.5; Product distribution; Further Variations:; time;	A 83% B n/a
With sodium tetrahydroborate; selenium In ethanol at 23 - 26℃; for 0.25h;	A 81% B 16%
With 1,2-bis(mercaptomethyl)benzene; (Et4N) In acetonitrile at 26℃; for 1.5h; Product distribution;

: 77853-02-2
1,3-Dichloro-5-(4-nitro-benzenesulfonyl)-benzene

A: 100-32-3
di(p-nitrophenyl) disulfide

B: 77853-10-2
3,5-Dichloro-benzenethiosulfonic acid; compound with ammonia

C: 100-01-6
4-nitro-aniline

Conditions

Conditions	Yield
With sulfur; ammonia at 100℃; for 2h; titanium autoclave;	A 42% B 93% C 40%

...Expand

: 555-16-8
4-nitrobenzaldehdye

: 100-01-6
4-nitro-aniline

: 10480-05-4
N-(4-nitrobenzylidene)-4-nitroaniline

Conditions

Conditions	Yield
at 60℃; for 2h;	100%
at 83 - 85℃;	100%
With sulfuric acid In neat (no solvent) Microwave irradiation; Sealed tube; Green chemistry;	72%

: 100-52-7
benzaldehyde

: 100-01-6
4-nitro-aniline

: 785-81-9, 1613-94-1, 40339-44-4
4-nitro-N-(phenylmethylene)benzenamine

Conditions

Conditions	Yield
In toluene at 120℃; for 24h;	100%
With aqueous extract of pericarp of Sapindus trifoliatus fruits at 20℃; for 0.0333333h;	98%
sodium hydrogen sulfate; silica gel at 52 - 54℃; for 0.0222222h; microwave irradiation;	95%

: 100-01-6
4-nitro-aniline

: 141-75-3
butyryl chloride

: 54191-12-7
N-(4'-nitrophenyl)butyramide

Conditions

Conditions	Yield
With NMM In dichloromethane	100%
With triethylamine In dichloromethane at 20℃;	71%
With sodium hydroxide; acetone

: 100-01-6
4-nitro-aniline

: 98-59-9
p-toluenesulfonyl chloride

: 734-25-8
N-(4-nitrophenyl)-4-methylbenzenesulfonamide

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 4℃;	100%
With (Na1752K0.144Ca0365Mg0.065)(Al2044Si2774O96)*19.16H2O In ethanol at 25 - 30℃; for 2h; Sonication; Green chemistry;	96%
With pyridine In dichloromethane at 20℃; for 12h;	94%

: 100-01-6
4-nitro-aniline

: 625-36-5
2-chloropropionyl chloride

: 19313-88-3
3-chloro-N-(4-nitrophenyl)propanamide

Conditions

Conditions	Yield
at 0 - 50℃; Neat (no solvent);	100%
at 20 - 50℃;	100%
at 50℃; for 16h;	97%

: 100-01-6
4-nitro-aniline

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 78596-42-6
ethyl α-ethoxycarbonyl-β-(4-nitroanilino)acrylate

Conditions

Conditions	Yield
at 120℃; for 3h; Heating / reflux;	100%
for 0.025h; Gould-Jacob reaction; Irradiation;	98%
In ethanol at 28℃; for 6h;	95%

: 100-01-6
4-nitro-aniline

: 636-98-6
p-nitrobenzene iodide

Conditions

Conditions	Yield
With potassium iodide; 10-camphorsulfonic acid; sodium nitrite In acetic acid at 20℃; for 24h; Time;	100%
With Nitrogen dioxide; sodium iodide In acetonitrile at -20℃; for 10h;	98%
Stage #1: 4-nitro-aniline With toluene-4-sulfonic acid In water at 20℃; Stage #2: With potassium iodide In water at 20℃; for 1.5h;	95%

: 100-01-6
4-nitro-aniline

: 1516-60-5
4-nitrophenyl azide

Conditions

Conditions	Yield
Stage #1: 4-nitro-aniline With toluene-4-sulfonic acid; sodium nitrite In water at 20℃; for 0.333333h; Stage #2: With sodium azide In water at 20℃; Reagent/catalyst;	100%
Stage #1: 4-nitro-aniline With trifluoroacetic acid; sodium nitrite In water at 0℃; for 0.166667h; Stage #2: With sodium azide In water at 20℃; for 5h;	99%
Stage #1: 4-nitro-aniline With hydrogenchloride In water at 0℃; Stage #2: With sodium nitrite In water for 0.166667h; Further stages;	99%

: 100-01-6
4-nitro-aniline

: 100-05-0
4-nitrobenzenediazonium chloride

Conditions

Conditions	Yield
With nitrosylchloride under 750.075 Torr; for 24h;	100%
With sodium nitrite In hydrogenchloride; water at 0.2℃; Rate constant;
With hydrogenchloride; sodium nitrite In hydrogenchloride; water at 25℃; Rate constant;

: 100-01-6
4-nitro-aniline

: 100-00-5
4-chlorobenzonitrile

Conditions

Conditions	Yield
With t-butyl thionitrite; copper dichloride In acetonitrile at 25℃; for 2h;	100%
With t-butyl thionitrite; copper dichloride In acetonitrile at 25℃; for 0.0333333h; Product distribution; Mechanism; var. temperature, var. time, other copper(II) halides, other reagents, other substituted aniline derivatives;	98%
Stage #1: 4-nitro-aniline With tert.-butylnitrite In acetonitrile at 20℃; Sandmeyer Reaction; Flow reactor; Stage #2: With copper dichloride In ethylene glycol; acetonitrile at 82℃; Sandmeyer Reaction; Flow reactor;	91%

: 100-01-6
4-nitro-aniline

: 106-50-3
1,4-phenylenediamine

Conditions

Conditions	Yield
With palladium diacetate; carbon monoxide; triphenylphosphine In water; acetic acid at 56℃; under 532 Torr; for 11h;	100%
With triethylsilane; palladium dichloride In ethanol at 20℃; for 1h; Inert atmosphere;	100%
With 10% palladium on activated charcoal; hydrogen for 2h;	100%

: 100-01-6
4-nitro-aniline

: 135-19-3
β-naphthol

: 6410-10-2
para red

Conditions

Conditions	Yield
With potassium hydrogensulfate; water; sodium nitrite for 0.0333333h; Diazotization; coupling; microwave irradiation;	100%
With hydrogenchloride; sodium nitrite In water at 20℃; for 1h; Time;	99%
With hydrogenchloride; sodium nitrite In water at 20℃; for 0.0833333h; Reagent/catalyst; Temperature; Green chemistry;	99%

: 100-01-6
4-nitro-aniline

: 108-95-2
phenol

: 1435-60-5, 81944-71-0
4-(4'-hydroxyphenylazo)nitrobenzene

Conditions

Conditions	Yield
Stage #1: 4-nitro-aniline With hydrogenchloride; sodium nitrite In water at 2℃; for 1.5h; Stage #2: phenol With sodium hydroxide In water at 2 - 20℃; for 4h;	100%
Stage #1: 4-nitro-aniline With carboxyl- and nitrite- functionalized graphene quantum dots at 20℃; for 0.0833333h; Stage #2: phenol In water at 20℃; for 0.166667h;	96%
Stage #1: 4-nitro-aniline With hydrogenchloride In water; acetone at 0℃; Inert atmosphere; Stage #2: With sodium nitrite In water; acetone at 0℃; for 1h; Inert atmosphere; Stage #3: phenol With sodium carbonate; sodium hydroxide In water; acetone at 0 - 20℃; for 3h; Inert atmosphere;	92%

: 3652-48-0
ethyl 2-methyl-5-phenyl-1H-pyrrole-3-carboxylate

: 100-01-6
4-nitro-aniline

: ethyl 5-methyl-3-(4-nitrophenylazo)-2-phenylpyrrole-4-carboxylate

Conditions

Conditions	Yield
With hydrogenchloride; sodium acetate; sodium nitrite In acetic acid at 0℃; for 1h;	100%

: 123-11-5
4-methoxy-benzaldehyde

: 100-01-6
4-nitro-aniline

: 15450-66-5
N-(4-methoxybenzylidene)-4-nitroaniline

Conditions

Conditions	Yield
With pyrrolidine In dichloromethane at 20℃; for 16h; Molecular sieve;	100%
With TiO2 nanotubes at 20℃; for 8h; Neat (no solvent); Sunlight;	98%
sodium hydrogen sulfate; silica gel at 64 - 66℃; for 0.025h; microwave irradiation;	96%

: 117452-48-9, 117475-50-0
6,7-dideoxy-α,β-D-galacto-hept-6-enopyranose

: 100-01-6
4-nitro-aniline

: 128357-86-8
N-p-nitrophenyl-6,7-dideoxy-L-galacto-hept-6-enosylamine

Conditions

Conditions	Yield
In methanol; acetic acid at 110℃; for 0.166667h;	100%

: 100-01-6
4-nitro-aniline

: 103-80-0
phenylacetyl chloride

: 13140-77-7
N-(4-nitrophenyl)-2-phenylacetamide

Conditions

Conditions	Yield
With pyridine In tetrahydrofuran at 0 - 20℃; for 2h;	100%
With potassium phosphate In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;	95%
In dichloromethane at 20℃; for 1h;	70%

: 100-01-6
4-nitro-aniline

: 2258-42-6
Acetic formic anhydride

: 16135-31-2
p-nitroformanilide

Conditions

Conditions	Yield
In tetrahydrofuran at 0℃; for 0.25h;	100%
In tetrahydrofuran at 20℃; for 3h; Schlenk technique; Inert atmosphere;	77%
In tetrahydrofuran

: 100-01-6
4-nitro-aniline

: p-nitrobenzene diazonium nitrate

Conditions

Conditions	Yield
With Nitrogen dioxide In 1,4-dioxane at 10 - 40℃;	100%
With Nitrogen dioxide at 0℃; for 6h;	92%
With Nitrogen dioxide; N,N-dimethyl-formamide In N,N-dimethyl-formamide for 0.0833333h;	91%
With tributyl phosphate-NO2 In various solvent(s) at 10 - 15℃;	90%
With polyethylene glycol - NO2 In various solvent(s)	84%

: 33842-02-3, 529510-96-1
dichloromethylenedimethyliminium chloride

: 100-01-6
4-nitro-aniline

: [Chloro-(4-nitro-phenylamino)-methylene]-dimethyl-ammonium; chloride

Conditions

Conditions	Yield
at -20℃; for 1h; ball mill;	100%

: 104-88-1
4-chlorobenzaldehyde

: 100-01-6
4-nitro-aniline

: 5340-14-7
(4-chlorobenzylidene)(4-nitrophenyl)amine

Conditions

Conditions	Yield
for 36h; Ambient temperature;	100%
In neat (no solvent) at 20℃; for 72h;	80%
In ethanol for 2h; Reflux;	76%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 104-94-9
4-methoxy-aniline

: 100-01-6
4-nitro-aniline

: 97221-15-3
(E)-N-(4-methoxybenzylidene)-4-nitroaniline

Conditions

Conditions	Yield
In dichloromethane Condensation; Heating;	100%

...Expand

: 4316-35-2
acetophenone dimethyl acetal

: 100-01-6
4-nitro-aniline

: (4-nitrophenyl)(1-phenylethylidene)amine

Conditions

Conditions	Yield
In dichloromethane Condensation; Heating;	100%

: 100-01-6
4-nitro-aniline

: 77-76-9
2,2-dimethoxy-propane

: 22104-23-0
N-isopropylidene-4-nitro-aniline

Conditions

Conditions	Yield
In dichloromethane Condensation; Heating;	100%

: 32315-10-9
bis(trichloromethyl) carbonate

: 18144-47-3
tert-butyl 4-aminobenzoate

: 100-01-6
4-nitro-aniline

: 301317-92-0
1-(4'-nitrophenyl)-3-(4''-tert-butylcarboxyphenyl)urea

Conditions

Conditions	Yield
Stage #1: bis(trichloromethyl) carbonate; 4-nitro-aniline With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 0 - 20℃; for 0.833333h; Substitution; Stage #2: tert-butyl 4-aminobenzoate In tetrahydrofuran at 20℃; for 42h; Substitution;	100%

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: 100-01-6
4-nitro-aniline

: 14628-57-0
4-chloro-5-methoxy-2-methyl-2H-pyridazin-3-one

: 5-methoxy-2-methyl-4-(4-nitro-phenylamino)-2H-pyridazin-3-one

Conditions

Conditions	Yield
With potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate In toluene at 120℃; for 7h; Substitution; Amination;	100%

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