As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:100-32-3
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:100-32-3
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Cas:100-32-3
Min.Order:1 Kilogram
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:100-32-3
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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Cas:100-32-3
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry4,4'-Dinitrodiphenyl disulfide CAS:100-32-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
Cas:100-32-3
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:100-32-3
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:100-32-3
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:100-32-3
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inquiryOur advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Cas:100-32-3
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:100-32-3
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:100-32-3
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:100-32-3
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:100-32-3
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:100-32-3
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:100-32-3
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inquiry4,4'-Dinitrodiphenyl disulfideAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:100-32-3
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals
Cas:100-32-3
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
Cas:100-32-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryFandaChem, a China-based chemical company, specialize in exporting 4,4'-Dinitrodiphenyl disulfide cas 100-32-3 (Fandachem), Please contact us by email freely. Appearance:white crystalline powder Storage:Store in dry, dark and ven
Cas:100-32-3
Min.Order:1 Kilogram
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Type:Other
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:100-32-3
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With air In dimethyl sulfoxide at 80℃; | 100% |
1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione In chloroform at 20℃; for 0.0166667h; | 100% |
CoCl2 In acetonitrile Ambient temperature; | 99% |
(4-nitro-phenyl)-m-tolyl sulfone
A
di(p-nitrophenyl) disulfide
B
Toluene-3-thiosulfonic acid; compound with ammonia
C
4-nitro-aniline
Conditions | Yield |
---|---|
With sulfur; ammonia at 100℃; for 2h; titanium autoclave; | A 43% B 100% C 40% |
1-methoxy-4-((4-nitrophenyl)sulfonyl)benzene
A
di(p-nitrophenyl) disulfide
B
4-Methoxy-benzenethiosulfonic acid; compound with ammonia
C
4-nitro-aniline
Conditions | Yield |
---|---|
With sulfur; ammonia at 100℃; for 2h; titanium autoclave; | A 56% B 100% C 32% |
With sulfur; ammonia at 100℃; for 2h; Product distribution; titanium autoclave; various reactions temp. and amounts of S8; |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; potassium sulfide; iron oxide; potassium hydroxide In N,N-dimethyl-formamide at 120℃; for 0.5h; Inert atmosphere; Green chemistry; | 98% |
With dmap; nickel(II) chloride hexahydrate; potassium thioacyanate; N,N-dimethyl-formamide at 140℃; for 15h; | 92% |
With copper(l) iodide; hexachloroethane; sodium carbonate; thiourea In water at 120℃; for 13h; | 87% |
4-nitrophenyl sulfone
A
di(p-nitrophenyl) disulfide
B
bis(4-nitrophenyl)sulfide
C
4-Nitro-benzenethiosulfonic acid; compound with ammonia
Conditions | Yield |
---|---|
With sulfur; ammonia at 40℃; for 2h; titanium autoclave; | A 38% B n/a C 98% |
4-nitrophenylthiolate
di(p-nitrophenyl) disulfide
Conditions | Yield |
---|---|
With 2-bromo-2-nitro-1,3-propanediol In methanol for 48h; Irradiation; | 98% |
With 2-bromo-2-nitro-1,3-propanediol In methanol Mechanism; Product distribution; Irradiation; other reagent and solvent; | 98% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; potassium sulfide; iron oxide; potassium hydroxide In N,N-dimethyl-formamide at 120℃; for 0.5h; Inert atmosphere; Green chemistry; | 97% |
With sodium sulfide pentahydrate In N,N-dimethyl-formamide at 40 - 100℃; for 6h; Reagent/catalyst; Temperature; Solvent; Inert atmosphere; | 92.8% |
With sodium disulfide In 1-methyl-pyrrolidin-2-one | 69% |
Conditions | Yield |
---|---|
With ziconium(IV) oxychloride octahydrate; sodium iodide In water at 90℃; for 0.25h; | 95% |
With tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 20℃; for 20h; chemoselective reaction; | 91% |
With triphenylphosphine In tetrahydrofuran at 0℃; | 75% |
C18H18N4O8S2
A
di(p-nitrophenyl) disulfide
B
diethylazodicarboxylate - triphenylphosphine (DEAD-Ph3P)
Conditions | Yield |
---|---|
With triphenylphosphine In benzene at 20℃; for 1h; | A 95% B n/a |
C18H18N4O8S2
triphenylphosphine
A
di(p-nitrophenyl) disulfide
B
diethylazodicarboxylate - triphenylphosphine (DEAD-Ph3P)
Conditions | Yield |
---|---|
In benzene at 20℃; for 1h; | A 95% B n/a |
C14H13NO5S
A
di(p-nitrophenyl) disulfide
B
3-Ethoxy-benzenethiosulfonic acid; compound with ammonia
C
4-nitro-aniline
Conditions | Yield |
---|---|
With sulfur; ammonia at 100℃; for 2h; titanium autoclave; | A 47% B 94% C 40% |
para-nitrobenzenethiol
B
di(p-nitrophenyl) disulfide
C
tri(p-tolyl)bismuth
Conditions | Yield |
---|---|
In dichloromethane Bi compd. added to CH2Cl2 soln. of 4-nitrobenzenethiol (molar ratio 1:2) at -78°C; warmed to room temp. with stirring; concd. under reduced pressure; recrystd. from CH2Cl2-hexane; | A 92% B 92% C 94% |
Conditions | Yield |
---|---|
With sulfur; oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene In water; N,N-dimethyl-formamide at 100℃; under 3750.38 Torr; for 18h; Sealed tube; Schlenk technique; | 94% |
1,3-Dichloro-5-(4-nitro-benzenesulfonyl)-benzene
A
di(p-nitrophenyl) disulfide
B
3,5-Dichloro-benzenethiosulfonic acid; compound with ammonia
C
4-nitro-aniline
Conditions | Yield |
---|---|
With sulfur; ammonia at 100℃; for 2h; titanium autoclave; | A 42% B 93% C 40% |
p-nitrophenyl-N-(p-toluenesulfonyl)sulfinimidoyl chloride
triphenylphosphine
A
di(p-nitrophenyl) disulfide
B
Triphenylphosphine oxide
C
N-p-tolylsulfonylphosphine imide
Conditions | Yield |
---|---|
Stage #1: p-nitrophenyl-N-(p-toluenesulfonyl)sulfinimidoyl chloride; triphenylphosphine In benzene at 20℃; for 0.5h; Stage #2: With water In benzene for 5h; Further stages.; | A 86% B 93% C 82% |
Conditions | Yield |
---|---|
With dmap; nickel(II) chloride hexahydrate; potassium thioacyanate; N,N-dimethyl-formamide at 140℃; for 15h; | 92% |
With copper(l) iodide; hexachloroethane; sodium carbonate; thiourea In water at 120℃; for 11h; | 91% |
With 1,10-Phenanthroline; copper(II) choride dihydrate; tetrabutyl ammonium fluoride; caesium carbonate; sulfur In water at 100℃; for 24h; Sealed tube; | 86% |
Conditions | Yield |
---|---|
With triphenylphosphine In acetonitrile for 2h; Ambient temperature; | 90% |
With triethylamine In acetonitrile Ambient temperature; overnight; | 75% |
With cyclooctatetraene dianion bipotassium salt In tetrahydrofuran at -40℃; for 0.5h; Product distribution; | |
With cyclooctatetraene dianion bipotassium salt In tetrahydrofuran at -40℃; for 0.5h; Yield given; | |
Multi-step reaction with 2 steps 1: 70 percent / diethyl ether / 1 h / -50 - 20 °C 2: 85 percent / SeCl4 / 1,2-dimethoxy-ethane / 2 h / 0 °C View Scheme |
1-methoxy-3-(4-nitrobenzenesulfonyl)benzene
A
di(p-nitrophenyl) disulfide
B
3-Methoxy-benzenethiosulfonic acid; compound with ammonia
C
4-nitro-aniline
Conditions | Yield |
---|---|
With sulfur; ammonia at 100℃; for 2h; titanium autoclave; | A 55% B 90% C 33% |
N-(benzenesulfonyl)-3-phenyloxaziridine
para-nitrobenzenethiol
A
di(p-nitrophenyl) disulfide
B
N-benzylidenephenylsulfonamide
C
benzaldehyde
Conditions | Yield |
---|---|
for 4.5h; Product distribution; | A 90% B 75% C 30% |
4-Methoxybenzenethiol
para-nitrobenzenethiol
A
di(p-nitrophenyl) disulfide
B
4,4'-dimethoxyphenyl disulfide
C
1-(4-methoxyphenyl)-2-(4-nitrophenyl)disulfane
Conditions | Yield |
---|---|
Stage #1: 4-Methoxybenzenethiol; para-nitrobenzenethiol With dmap; water In ethanol at 20℃; for 0.0833333h; Stage #2: With iodine In ethanol at 70℃; for 3h; Sealed tube; | A 2% B 5% C 90% |
di(p-nitrophenyl) disulfide
Conditions | Yield |
---|---|
With iodine In dichloromethane | 86% |
p-nitro-N,N-bis(trimethylsilyl)benzenesulfenamide
A
di(p-nitrophenyl) disulfide
Conditions | Yield |
---|---|
With selenium tetrachloride In 1,2-dimethoxyethane at 0℃; for 2h; | A 85% B n/a |
4-nitrobenzenesulfenyl chloride
A
1-methylthio-4-nitro-benzene
B
di(p-nitrophenyl) disulfide
Conditions | Yield |
---|---|
With tetramethylstannane; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 25℃; for 4h; | A n/a B 84% |
thiophenol
para-nitrobenzenethiol
A
di(p-nitrophenyl) disulfide
B
4-nitrophenyl phenyl disulfide
C
diphenyldisulfane
Conditions | Yield |
---|---|
Stage #1: thiophenol; para-nitrobenzenethiol With dmap; water In ethanol at 20℃; for 0.0833333h; Stage #2: With iodine In ethanol at 70℃; for 3h; Sealed tube; | A 2% B 80% C 2% |
(4-nitro-phenyl)-o-tolyl sulfone
A
di(p-nitrophenyl) disulfide
B
Toluene-2-thiosulfonic acid; compound with ammonia
C
4-nitro-aniline
Conditions | Yield |
---|---|
With sulfur; ammonia at 100℃; for 1h; titanium autoclave; | A 32% B 79% C 18% |
triphenylphosphine
B
di(p-nitrophenyl) disulfide
C
Triphenylphosphine oxide
D
N-p-tolylsulfonylphosphine imide
Conditions | Yield |
---|---|
In benzene at 20℃; for 4h; | A 91.5 % Spectr. B 79% C 66% D 4% |
p-Chlorothiophenol
para-nitrobenzenethiol
A
4,4'-dichlorodiphenyl disulfide
B
di(p-nitrophenyl) disulfide
C
1-(4-chlorophenyl)-2-(4-nitrophenyl)disulfane
Conditions | Yield |
---|---|
Stage #1: p-Chlorothiophenol; para-nitrobenzenethiol With dmap; water In ethanol at 20℃; for 0.0833333h; Stage #2: With iodine In ethanol at 70℃; for 3h; Sealed tube; | A 5% B 2% C 79% |
para-nitrobenzenethiol
benzyl alcohol
A
di(p-nitrophenyl) disulfide
B
1-(benzylsulphanyl)-4-Nitrobenzene
Conditions | Yield |
---|---|
at 180℃; Catalytic behavior; Inert atmosphere; Autoclave; | A 17% B 78% |
3-methoxybenzenethiol
para-nitrobenzenethiol
A
di(p-nitrophenyl) disulfide
B
bis(3-methoxyphenyl)disulfide
Conditions | Yield |
---|---|
Stage #1: 3-methoxybenzenethiol; para-nitrobenzenethiol With dmap; water In ethanol at 20℃; for 0.0833333h; Stage #2: With iodine In ethanol at 70℃; for 3h; Sealed tube; | A 2% B 5% C 78% |
para-nitrobenzenethiol
1-dodecylthiol
A
didodecyl disulfide
B
di(p-nitrophenyl) disulfide
Conditions | Yield |
---|---|
Stage #1: para-nitrobenzenethiol; 1-dodecylthiol With dmap; water In ethanol at 20℃; for 0.0833333h; Stage #2: With iodine In ethanol at 70℃; for 3h; Sealed tube; | A 5% B 11% C 78% |
tris(3,4,5-trifluorophenyl)boroxine
di(p-nitrophenyl) disulfide
(3,4,5-trifluorophenyl)-4-nitrophenylsulfide
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; oxygen In water; dimethyl sulfoxide at 90℃; under 757.576 Torr; for 6.5h; | 99% |
Conditions | Yield |
---|---|
With magnesium In methanol for 0.166667h; Ambient temperature; | 98% |
With sodium tetrahydroborate In tetrahydrofuran; methanol at 50℃; for 1h; | 89% |
With sodium tetrahydroborate; lithium chloride In tetrahydrofuran at 0 - 35℃; | 85% |
Conditions | Yield |
---|---|
With potassium fluoride; chlorine In acetonitrile at 20℃; for 4.5h; | 98% |
With silver(II) fluoride In 1,1,2-Trichloro-1,2,2-trifluoroethane Heating; | |
With bis(fluoroxy)methane In acetonitrile at -20℃; |
2-methyl-1H-indole
di(p-nitrophenyl) disulfide
2-methyl-3-((4-nitrophenyl)thio)-1H-indole
Conditions | Yield |
---|---|
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 2h; regioselective reaction; | 98% |
With iron(III) trifluoride; iodine In acetonitrile at 80℃; for 36h; regioselective reaction; | 94% |
With sodium tetrafluoroborate; potassium iodide In acetonitrile at 60℃; for 6h; Electrolysis; | 82% |
With silver nitrate In ethanol; N,N-dimethyl-formamide at 70℃; for 8h; Sealed tube; | 63% |
Conditions | Yield |
---|---|
With palladium diacetate; copper(ll) bromide In N,N-dimethyl-formamide at 140℃; for 24h; Sealed tube; | 98% |
di(p-nitrophenyl) disulfide
Conditions | Yield |
---|---|
With copper diacetate; sodium carbonate In 1,4-dioxane at 130℃; for 12h; | 98% |
di(p-nitrophenyl) disulfide
Conditions | Yield |
---|---|
With Boc-DL-Leu-OH; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(l) oxide In dichloromethane at 90℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube; | 98% |
Conditions | Yield |
---|---|
With water; rongalite; potassium carbonate In N,N-dimethyl-formamide for 0.166667h; | 97% |
With disodium hydrogenphosphate; sodium dithionite In water; N,N-dimethyl-formamide at 20℃; for 0.2h; | 82% |
di(p-nitrophenyl) disulfide
phenylboronic acid
4-nitrophenyl phenyl sulfide
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; copper(l) iodide In water; dimethyl sulfoxide at 100℃; for 12h; | 97% |
With [2,2]bipyridinyl; copper(l) iodide; air In dimethyl sulfoxide at 100℃; for 12h; | 97% |
di(p-nitrophenyl) disulfide
tris(3-fluoro phenyl)boroxine
(3-fluorophenyl)-4-nitrophenylsulfide
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; oxygen In water; dimethyl sulfoxide at 90℃; under 757.576 Torr; for 7h; | 97% |
Conditions | Yield |
---|---|
With chlorine In tetrachloromethane at 60℃; for 3h; | 96% |
With chloroform; chlorine unter Ausschluss der Luftfeuchtigkeit; | |
With chlorine |
Conditions | Yield |
---|---|
With dihydrogen peroxide; methyltrioxorhenium(VII) In dichloromethane; acetonitrile at 20℃; for 1h; | 96% |
With dihydrogen peroxide; trichlorophosphate In water at 80℃; for 1.08333h; Micellar solution; | 93% |
With nitric acid | |
With nitric acid |
Conditions | Yield |
---|---|
With dihydrogen peroxide; zirconium(IV) chloride In water; acetonitrile at 25℃; for 0.0166667h; | 96% |
With N,N,N',N'-tetrachlorobenzene-1,3-disulphonamide; tetrabutyl-ammonium chloride; water In acetonitrile at 0 - 20℃; for 0.333333h; | 96% |
With trichloroisocyanuric acid; tetrabutylammomium bromide; water In acetonitrile at 0 - 20℃; for 0.333333h; | 96% |
N-chloroacetamide
di(p-nitrophenyl) disulfide
N,N'-diacetyl-p-nitrobenzenesulfinamidine
Conditions | Yield |
---|---|
With pyridine In benzene | 96% |
di(p-nitrophenyl) disulfide
benzyl bromide
1-(benzylsulphanyl)-4-Nitrobenzene
Conditions | Yield |
---|---|
With water; rongalite; potassium carbonate In N,N-dimethyl-formamide for 0.25h; | 96% |
With sodium hydroxide; Aminoiminomethanesulfinic acid; cetyltrimethylammonium chloride In tetrahydrofuran; water for 0.2h; Heating; | 92% |
With disodium hydrogenphosphate; sodium dithionite In water; N,N-dimethyl-formamide at 20℃; for 0.25h; | 73% |
di(p-nitrophenyl) disulfide
1-dodecylbromide
p-nitrophenyl n-dodecyl thioether
Conditions | Yield |
---|---|
With sodium hydroxide; Aminoiminomethanesulfinic acid; cetyltrimethylammonium chloride In tetrahydrofuran; water for 3.3h; Heating; | 96% |
di(p-nitrophenyl) disulfide
1-phenyl-2-bromoethane
1-nitro-4-[(2-phenylethyl)sulfanyl]benzene
Conditions | Yield |
---|---|
With sodium hydroxide; Aminoiminomethanesulfinic acid; cetyltrimethylammonium chloride In tetrahydrofuran; water for 2.1h; Heating; | 96% |
Conditions | Yield |
---|---|
With water; rongalite; potassium carbonate In N,N-dimethyl-formamide for 0.25h; | 96% |
di(p-nitrophenyl) disulfide
1-bromomethyl-4-nitro-benzene
1-nitro-4-(4-nitrophenylmethylthio)benzene
Conditions | Yield |
---|---|
With water; rongalite; potassium carbonate In N,N-dimethyl-formamide for 0.166667h; | 96% |
di(p-nitrophenyl) disulfide
2-phenylethynylaniline
3-((4-nitrophenyl)thio)-2-phenyl-1H-indole
Conditions | Yield |
---|---|
With air; palladium dichloride In dimethyl sulfoxide at 80℃; for 24h; | 96% |
With iodine In toluene at 110℃; for 8h; Schlenk technique; | 93% |
di(p-nitrophenyl) disulfide
acetic anhydride
1-acetylsulfanyl-4-nitro-benzene
Conditions | Yield |
---|---|
With rongalite; cesium fluoride In water; N,N-dimethyl-formamide at 20℃; for 0.0833333h; | 96% |
indole
di(p-nitrophenyl) disulfide
3-[(4-nitrophenyl)sulfanyl]-1H-indole
Conditions | Yield |
---|---|
With iron(III) trifluoride; iodine In acetonitrile at 80℃; for 36h; regioselective reaction; | 96% |
With iodine; dimethyl sulfoxide In carbonic acid dimethyl ester at 40℃; for 10h; | 92% |
Stage #1: di(p-nitrophenyl) disulfide With tetrabutylammomium bromide; triethylamine In dichloromethane for 1h; Cooling with ice; Green chemistry; Stage #2: indole In dichloromethane at 70℃; for 3.5h; Green chemistry; | 85% |
di(p-nitrophenyl) disulfide
4-methyl-benzaldehyde
S-(4-nitrophenyl) 4-methylbenzothioate
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; potassium carbonate In water at 100℃; for 2h; | 96% |
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