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inquiry4-NITROPHENYLSULFUR PENTAFLUORIDE,2613-27-6 Application:4-NITROPHENYLSULFUR PENTAFLUORIDE,2613-27-6
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inquiry4-NITROPHENYLSULFUR PENTAFLUORIDE,2613-27-6Appearance:white powder Storage:Room temperature. Package:normal packing Application:Pharmaceutical Intermediates, OLED Intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for smal
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inquiry1-nitro-4-(pentafluorosulfanyl)benzene
Conditions | Yield |
---|---|
With hydrogen fluoride; mercury(II) oxide at -30 - 20℃; Inert atmosphere; Sealed tube; | 81% |
With iodine pentafluoride In neat (no solvent) at 65℃; for 14h; Glovebox; Inert atmosphere; | 75% |
With silver carbonate at 70℃; Inert atmosphere; Glovebox; | 66% |
With zinc(II) fluoride at 150℃; for 72h; Inert atmosphere; | 36% |
With silver tetrafluoroborate In dichloromethane at 20℃; for 14h; Inert atmosphere; | 189.9 mg |
Conditions | Yield |
---|---|
With potassium fluoride; bis(fluoroxy)methane at -20 - -15℃; | 63% |
With silver(II) fluoride In various solvent(s) at 20 - 130℃; | 50% |
With fluorine In acetonitrile at -5℃; for 1h; Inert atmosphere; | 45% |
Conditions | Yield |
---|---|
With fluorine In acetonitrile at 20℃; | 60% |
With fluorine Ambient temperature; | 44% |
With bis(fluoroxy)methane In acetonitrile at -20 - 20℃; | |
With fluorine; cesium fluoride In acetonitrile at -30 - -25℃; | |
With potassium fluoride; bis(fluoroxy)methane In acetonitrile at -15℃; |
Conditions | Yield |
---|---|
In acetonitrile | 28% |
Multi-step reaction with 3 steps 1.1: sodium hydroxide / water / 0.5 h / Inert atmosphere 1.2: 14 h / 20 °C / Inert atmosphere 2.1: potassium fluoride; chlorine / acetonitrile / 20 °C / Inert atmosphere; Glovebox; Cooling with ice 3.1: iodine pentafluoride / neat (no solvent) / 14 h / 65 °C / Glovebox; Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide / water / 0.5 h / Inert atmosphere 1.2: 12 h / 20 °C / Inert atmosphere 2.1: potassium fluoride; chlorine / acetonitrile / 20 °C / Inert atmosphere; Glovebox; Cooling with ice 3.1: silver carbonate / 70 °C / Inert atmosphere; Glovebox View Scheme |
Conditions | Yield |
---|---|
Stage #1: 4-nitrobenzenesulfenyl chloride With bis(fluoroxy)methane In acetonitrile at -20 - -15℃; Stage #2: With cesium fluoride In acetonitrile | |
Stage #1: 4-nitrobenzenesulfenyl chloride With bis(fluoroxy)methane In acetonitrile at -20 - -15℃; Stage #2: With fluorine; cesium fluoride In acetonitrile at -30 - -25℃; | |
Multi-step reaction with 2 steps 1: potassium fluoride; chlorine / acetonitrile / 5 - 11 °C 2: zinc(II) fluoride / 72 h / 150 °C / Inert atmosphere View Scheme |
di(p-nitrophenyl) disulfide
A
1-nitro-4-(pentafluorosulfanyl)benzene
B
4-nitrophenylsulphur trifluoride
Conditions | Yield |
---|---|
With fluorine In acetonitrile at -35 - -25℃; |
di(p-nitrophenyl) disulfide
A
1-nitro-4-(pentafluorosulfanyl)benzene
B
4-nitrobenzenesulfonyl fluoride
Conditions | Yield |
---|---|
With silver(II) fluoride; copper at 60 - 125℃; for 8h; Sealed tube; | A 6.73 g B n/a |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium sulfide / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere 2.1: sodium hydroxide / water / 0.5 h / Inert atmosphere 2.2: 12 h / 20 °C / Inert atmosphere 3.1: potassium fluoride; chlorine / acetonitrile / 20 °C / Inert atmosphere; Glovebox; Cooling with ice 4.1: silver carbonate / 70 °C / Inert atmosphere; Glovebox View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride; iron In ethanol; water at 0 - 20℃; for 1h; | 100% |
With hydrogen; nickel In ethanol | 99% |
Stage #1: 1-nitro-4-(pentafluorosulfanyl)benzene With hydrogenchloride; tin(ll) chloride In water at 45 - 100℃; for 3.5h; Stage #2: With sodium hydroxide In dichloromethane; water at 0℃; | 99% |
1-nitro-4-(pentafluorosulfanyl)benzene
benzyl alcohol
(4-(benzyloxy)phenyl)pentafluoro-λ6-sulfane
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; | 96% |
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 1h; | 96% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 2,2-dimethylbutyric acid; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In toluene at 130℃; for 15h; Schlenk technique; Inert atmosphere; Sealed tube; | 95% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 2,2-dimethylbutyric acid; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In toluene at 130℃; for 15h; Schlenk technique; Inert atmosphere; Sealed tube; | 92% |
tert-Butyl chloroacetate
1-nitro-4-(pentafluorosulfanyl)benzene
tert-butyl [2-nitro-5-(pentafluoro-λ6-sulfanyl)phenyl]acetate
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; for 0.166667h; | 91% |
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; for 0.166667h; Vicarious Nucleophilic Substitution; | 80% |
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; Inert atmosphere; | 38% |
1-nitro-4-(pentafluorosulfanyl)benzene
2-nitro-5-(pentafluorosulfanyl)phenol
Conditions | Yield |
---|---|
With Cumene hydroperoxide; potassium tert-butylate; methylamine In tetrahydrofuran at -78 - -50℃; for 0.5h; | 91% |
With Cumene hydroperoxide; potassium tert-butylate; methylamine In tetrahydrofuran at -50℃; for 0.25h; | 90% |
With Cumene hydroperoxide; potassium tert-butylate; ammonia In tetrahydrofuran at -50℃; for 0.25h; | 76% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1h; | 87% |
In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; | 83% |
In N,N-dimethyl-formamide at 20℃; for 1h; | 83% |
1-nitro-4-(pentafluorosulfanyl)benzene
chloromethyl phenyl sulfone
pentafluoro(4-nitro-3-((phenylsulfonyl)methyl)phenyl)-λ6-sulfane
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at -40℃; for 0.166667h; Vicarious Nucleophilic Substitution; | 87% |
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; for 0.5h; Inert atmosphere; | 86% |
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; for 0.5h; | 86% |
With potassium tert-butylate In N,N-dimethyl-formamide at -40℃; for 0.5h; | 84% |
With potassium tert-butylate In N,N-dimethyl-formamide at -40℃; for 0.5h; | 84% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 2,2-dimethylbutyric acid; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In toluene at 130℃; for 15h; Reagent/catalyst; Temperature; Schlenk technique; Inert atmosphere; Sealed tube; | A 87% B 4% |
With bis(η3-allyl-μ-chloropalladium(II)); 2,2-dimethylbutyric acid; caesium carbonate; tricyclohexylphosphine tetrafluoroborate In toluene at 130℃; for 12h; Reagent/catalyst; Temperature; Schlenk technique; Inert atmosphere; Sealed tube; | A 18 %Spectr. B 41 %Spectr. |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 2,2-dimethylbutyric acid; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In toluene at 130℃; for 15h; Schlenk technique; Inert atmosphere; Sealed tube; | A 86% B 5% |
1-nitro-4-(pentafluorosulfanyl)benzene
2-bromo-4-(pentafluoro-λ6-sulfanyl)aniline
Conditions | Yield |
---|---|
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione In dichloromethane at 3 - 20℃; for 2h; | 85% |
Multi-step reaction with 2 steps 1: 99 percent / H2 / Raney nickel / ethanol 2: NBS / acetonitrile / 0 °C View Scheme |
diethyl chloromethylphosphonate
1-nitro-4-(pentafluorosulfanyl)benzene
diethyl 2-nitro-5-(pentafluorosulfanyl)benzylphosphonate
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at -60℃; for 0.166667h; | 84% |
With potassium tert-butylate In N,N-dimethyl-formamide at -60℃; for 0.5h; Vicarious Nucleophilic Substitution; | 77% |
Stage #1: diethyl chloromethylphosphonate; 1-nitro-4-(pentafluorosulfanyl)benzene With potassium tert-butylate In N,N-dimethyl-formamide at -60℃; for 0.166667h; Stage #2: With water Acidic conditions; |
octanol
1-nitro-4-(pentafluorosulfanyl)benzene
1-(n-octyloxy)-4-(pentafluorosulfanyl)benzene
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.3h; Inert atmosphere; | 83% |
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.333333h; | 83% |
dichloroacetic acid methyl ester
1-nitro-4-(pentafluorosulfanyl)benzene
C9H7ClF5NO4S
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; for 0.166667h; | 83% |
4-biphenylacetonitrile
1-nitro-4-(pentafluorosulfanyl)benzene
3-(biphenyl-4-yl)-5-(pentafluorosulfanyl)benzo[c]isoxazole
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 20℃; for 1h; | 83% |
1-nitro-4-(pentafluorosulfanyl)benzene
2-nitro-5-(pentafluorosulfanyl)aniline
Conditions | Yield |
---|---|
With potassium tert-butylate; N,N,N-trimethylhydrazinium iodide In dimethyl sulfoxide at 20℃; for 0.0833333h; | 82% |
With potassium tert-butylate; N,N,N-trimethylhydrazinium iodide In dimethyl sulfoxide | 82% |
1-nitro-4-(pentafluorosulfanyl)benzene
4-Ethynylaniline
Conditions | Yield |
---|---|
Stage #1: 4-Ethynylaniline With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.0166667h; Inert atmosphere; Stage #2: 1-nitro-4-(pentafluorosulfanyl)benzene In tetrahydrofuran; hexane at -120 - -110℃; for 0.166667h; Inert atmosphere; Stage #3: With potassium permanganate; ammonia In tetrahydrofuran; hexane at -110℃; for 0.0833333h; Inert atmosphere; | 78% |
1-nitro-4-(pentafluorosulfanyl)benzene
chloroacetic acid ethyl ester
C10H10F5NO4S
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; for 0.166667h; | 76% |
With potassium tert-butylate In N,N-dimethyl-formamide at -30℃; for 0.166667h; | 76% |
chloroform
1-nitro-4-(pentafluorosulfanyl)benzene
2-(dichloromethyl)-1-nitro-4-(pentafluorosulfanyl)benzene
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran; chloroform; N,N-dimethyl-formamide at -78℃; for 0.5h; Inert atmosphere; | 75% |
With potassium tert-butylate In tetrahydrofuran; N,N-dimethyl-formamide at -70℃; for 0.0333333h; | 74% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 2,2-dimethylbutyric acid; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In toluene at 130℃; for 15h; Schlenk technique; Inert atmosphere; Sealed tube; | A 75% B 17% |
1-nitro-4-(pentafluorosulfanyl)benzene
sodium ethanolate
1-ethoxy-4-(pentafluorosulfanyl)benzene
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; | 74% |
In N,N-dimethyl-formamide at 20℃; for 1h; | 74% |
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran; N,N-dimethyl-formamide at -70℃; for 0.0333333h; | 74% |
1-nitro-4-(pentafluorosulfanyl)benzene
phenoxyacetonitrile
2-(2-nitro-5-(pentafluorosulfanyl)phenyl)acetonitrile
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.166667h; | 74% |
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.166667h; | 74% |
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.5h; Vicarious Nucleophilic Substitution; | 41% |
Conditions | Yield |
---|---|
Stage #1: aniline With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.0166667h; Inert atmosphere; Stage #2: 1-nitro-4-(pentafluorosulfanyl)benzene In tetrahydrofuran; hexane at -120 - -110℃; for 0.166667h; Inert atmosphere; Stage #3: With potassium permanganate; ammonia In tetrahydrofuran; hexane at -110℃; for 0.0833333h; Reagent/catalyst; Temperature; Solvent; Inert atmosphere; | 73% |
Conditions | Yield |
---|---|
Stage #1: p-toluidine With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.0166667h; Inert atmosphere; Stage #2: 1-nitro-4-(pentafluorosulfanyl)benzene In tetrahydrofuran; hexane at -120 - -110℃; for 0.166667h; Inert atmosphere; Stage #3: With potassium permanganate; ammonia In tetrahydrofuran; hexane at -110℃; for 0.0833333h; Inert atmosphere; | 73% |
Conditions | Yield |
---|---|
Stage #1: 4-chloro-aniline With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.0166667h; Inert atmosphere; Stage #2: 1-nitro-4-(pentafluorosulfanyl)benzene In tetrahydrofuran; hexane at -120 - -110℃; for 0.166667h; Inert atmosphere; Stage #3: With potassium permanganate; ammonia In tetrahydrofuran; hexane at -110℃; for 0.0833333h; Inert atmosphere; | 72% |
propan-1-ol
1-nitro-4-(pentafluorosulfanyl)benzene
1-(n-propoxy)-4-(pentafluorosulfanyl)benzene
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; | 71% |
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.5h; | 71% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 2,2-dimethylbutyric acid; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In toluene at 130℃; for 15h; Schlenk technique; Inert atmosphere; Sealed tube; | 71% |
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