As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:529-20-4
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inquiryProduct description: Product name 2-Methylbenzaldehyde CAS number 529-20-4 Assay ≥98% Appearance Transparent liquid Capacity 200mt/year Application Organic synthesis intermed
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inquiryProduct name 2-Methylbenzaldehyde CAS 529-20-4 Other names 2-Methylbenzaldehyde 98%;o-Methylbenzald
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inquiry2-Methylbenzaldehyde CAS:529-20-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct name: 2-Methylbenzaldehyde CAS No.:529-20-4 Molecule Formula:C8H8O Molecule Weight:120.14 Purity: 99% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEMS
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inquiry2-Methylbenzaldehyde Chemical Properties Melting point -35 °C Boiling point 199-200 °C(lit.) density 1.039 g/mL at 25 °C(lit.) FEMA 3068 | TOLUALDEHYDES (MIXED O,M,P) refractive index n20/D 1.546(lit.) Fp 153 °
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
Conditions | Yield |
---|---|
With iodosylbenzene; Cl-CH2-PS supported 5-amino-1,10-phenanthroline-Ru In acetonitrile at 60℃; for 2h; | 100% |
With Oxone; [Mn(NO3)2(2,3,5,6-tetra(2-pyridyl)pyrazine)(H2O)]; tetrabutylammomium bromide In dichloromethane at 20℃; Catalytic behavior; Reagent/catalyst; | 100% |
With sym-collidinium chlorochromate; periodic acid In acetonitrile at 20℃; for 0.166667h; Time; Solvent; | 100% |
2-methylbenzyl trimethylsilyl ether
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With nitrogen dioxide at 20℃; for 0.0833333h; | 100% |
With allyltriphenylphopsphonium peroxodisulfate In acetonitrile for 0.25h; Heating; | 98% |
With trinitratocerium(IV) bromate for 0.33h; Heating; | 96% |
2-diacetoxymethyltoluene
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With sulphated zirconia In acetonitrile at 60℃; for 0.45h; Microwave irradiation; | 100% |
With rice husk supported FeCl3 nanoparticles In ethanol at 70℃; for 0.25h; | 96% |
With indium(III) bromide In water for 0.333333h; Heating; | 94% |
salicylaldoxime
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With water; 2-nitro-4,5-dichloropyridazin-3(2H)-one In methanol at 150℃; under 10336 Torr; for 0.166667h; Microwave irradiation; | 98% |
With potassium permanganate; 1-n-butyl-3-methylimidazolim bromide at 20℃; for 0.683333h; Ionic liquid; chemoselective reaction; | 95% |
With KMnO4/alumina at 50℃; for 0.666667h; | 90% |
Conditions | Yield |
---|---|
With water; sodium hydroxide at 20℃; for 0.05h; Microwave irradiation; | 97% |
With 4-methylmorpholine N-oxide; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride; potassium iodide at 100℃; for 0.0333333h; Microwave irradiation; Ionic liquid; | 92% |
With 4-methylmorpholine N-oxide In tetrahydrofuran at 20℃; for 15h; Reflux; | 75% |
2-(2-methylphenyl)-1,3-dithiolane
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With silica gel; ferric nitrate In hexane at 50℃; for 0.166667h; | 97% |
With indium (III) iodide; dihydrogen peroxide In water; toluene at 20℃; for 15h; Inert atmosphere; Sealed tube; | 86 mg |
o-MeC6H4CHNNHC6H5
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With water; silica gel; bis(trimethylsilyl)chromate In chloroform for 0.3h; Heating; | 97% |
With cetyltrimethylammonium peroxodisulphate In acetonitrile for 0.416667h; Reflux; | 94% |
Conditions | Yield |
---|---|
With iron; acetic acid; nickel dichloride In methanol; water for 0.666667h; Heating; | 95% |
With iron; acetic acid; nickel dichloride In methanol; water for 0.666667h; Product distribution; Heating; | 95% |
With formic acid; platinum(IV) oxide In water at 55 - 60℃; for 3h; | 90% |
2-(2-methylphenyl)-1,3-dioxolane
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With caro's acid; silica gel In acetonitrile at 20℃; for 0.333333h; | 95% |
With hydrogenchloride; acetone at 20℃; for 0.5h; | 11.5 g |
With hydrogenchloride; water In tetrahydrofuran for 2.5h; |
(2-methyl-phenyl)-(morpholin-4-yl)methanone
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With zirconocene dichloride; lithium tri-t-butoxyaluminum hydride In tetrahydrofuran at 20℃; for 0.0333333h; Inert atmosphere; | 95% |
Stage #1: (2-methyl-phenyl)-(morpholin-4-yl)methanone With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethanesulfonic acid ethyl ester In dichloromethane at 20℃; for 2h; Inert atmosphere; Stage #2: With lithium tri-t-butoxyaluminum hydride In tetrahydrofuran; dichloromethane at -78℃; for 4h; Inert atmosphere; | 83% |
(2-methylphenyl)(1-pyrrolidinyl)methanone
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
Stage #1: (2-methylphenyl)(1-pyrrolidinyl)methanone With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethanesulfonic acid ethyl ester In dichloromethane at 20℃; for 2h; Inert atmosphere; Stage #2: With lithium tri-t-butoxyaluminum hydride In tetrahydrofuran; dichloromethane at -78℃; for 4h; Inert atmosphere; | 95% |
2-(2-Methylphenyl)-1,3-dithian
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
Stage #1: 2-(2-Methylphenyl)-1,3-dithian With trichloroisocyanuric acid; silica gel at 20℃; for 0.05h; Stage #2: With water at 20℃; | 94% |
With quinolinium monofluorochromate(VI) In acetonitrile for 3h; Heating; | 94% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In neat (no solvent) at 20℃; for 1h; Milling; | 94% |
2-<2-Methyl-benzyloxy>-tetrahydro-pyran
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With allyltriphenylphopsphonium peroxodisulfate In acetonitrile for 0.25h; Heating; | 94% |
With dipotassium peroxodisulfate; molybdenum trioxide In water; acetonitrile for 0.34h; Reflux; | 90% |
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
Stage #1: C20H29NO With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethanesulfonic acid ethyl ester In dichloromethane at 20℃; for 2h; Inert atmosphere; Stage #2: With lithium tri-t-butoxyaluminum hydride In tetrahydrofuran; dichloromethane at -78℃; for 4h; Inert atmosphere; | 94% |
triformylamine
toluene
A
4-methyl-benzaldehyde
B
N-[bis(4-methylphenyl)methyl]formamide
C
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With aluminium trichloride at 0℃; for 5h; Condensation; formylation; | A n/a B 93% C n/a |
N,N-dibenzyl-2-methylbenzamide
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
Stage #1: N,N-dibenzyl-2-methylbenzamide With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethanesulfonic acid ethyl ester In dichloromethane at 45℃; for 4h; Inert atmosphere; Stage #2: With lithium tri-t-butoxyaluminum hydride In tetrahydrofuran; dichloromethane at -78℃; for 4h; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) In benzene for 0.166667h; Ambient temperature; | 92% |
With tri-n-butyl-tin hydride In 1-methyl-pyrrolidin-2-one at 20℃; Inert atmosphere; | 87% |
With polymethylhydrosiloxane; trifuran-2-yl-phosphane; tetrabutyl ammonium fluoride; potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) In tetrahydrofuran; water at 20℃; for 1h; | 83% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In water; acetonitrile at 25℃; for 10h; UV-irradiation; | 92% |
With potassium 12-tungstocobaltate(III) In water; acetonitrile for 0.166667h; Microwave irradiation; | 92% |
With mercury(II) fluoride; oxygen In acetonitrile at 25℃; for 24h; Irradiation; | 85% |
2-(o-tolyl)-1,3-oxathiolane
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With copper(II) nitrate monohydrate at 90℃; for 0.1h; | 92% |
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
Stage #1: N,N-dibutyl-2-methylbenzamide With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethanesulfonic acid ethyl ester In dichloromethane at 20℃; for 4h; Inert atmosphere; Stage #2: With lithium tri-t-butoxyaluminum hydride In tetrahydrofuran; dichloromethane at -78℃; for 4h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With carbon tetrabromide; oxygen In acetonitrile at 20℃; for 2h; Irradiation; Green chemistry; | 91% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In fluorobenzene; dimethyl sulfoxide at 85℃; for 16h; | 82% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 85℃; for 16h; | 82% |
carbon monoxide
toluene
A
bis(p-methylphenyl)-methanone
B
4,4'-dimethylbenzhydrol
C
4-methyl-benzaldehyde
D
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With hydrogen fluoride; boron trifluoride at 45℃; under 37503.8 - 60006 Torr; for 1h; Further byproducts.; | A n/a B n/a C 91% D 5% |
2-(2-methylbenzylidene)hydrazine carboxamide
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With potassium permanganate at 20℃; for 1.66667h; Ionic liquid; chemoselective reaction; | 91% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate; dicyclohexyl-carbodiimide at 100℃; for 2.5h; Sealed tube; | 91% |
With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; tricyclohexylphosphine In N,N-dimethyl-formamide at 80℃; for 10h; Inert atmosphere; Sealed tube; | 85% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; Inert atmosphere; Sealed tube; | 72% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; for 4h; Sealed tube; | 71% |
Conditions | Yield |
---|---|
With samarium diiodide; phosphoric acid In tetrahydrofuran for 0.000833333h; Ambient temperature; | 90% |
With lithium-tris(diethylamino)hydridoaluminate In tetrahydrofuran for 12h; Ambient temperature; | 86% |
2-methylphenyl aldehyde
Conditions | Yield |
---|---|
With hydrogenchloride In water; N,N-dimethyl-formamide at 50℃; for 1h; | 90% |
With hydrogenchloride; water at 50℃; for 1h; | 90% |
Conditions | Yield |
---|---|
With phenylsilane; cobalt(II) diacetate tetrahydrate; sodium triethylborohydride In 1,2-dimethoxyethane; toluene at 0℃; for 15h; Inert atmosphere; Schlenk technique; | 89% |
With naphthalene In tetrahydrofuran; hexane at 0℃; for 3h; | 82 % Chromat. |
With sodium diisobutyl(t-butoxy)aluminum hydride In tetrahydrofuran; hexane at 0℃; for 6h; | 83 % Chromat. |
Conditions | Yield |
---|---|
With palladium(II) acetylacetonate; hydrogen; 2,2-dimethylpropanoic anhydride; dicyclohexylphenylphosphine In tetrahydrofuran at 80℃; under 3750.38 Torr; for 20h; Inert atmosphere; | 88% |
With succinic acid anhydride; methylphenylsilane; C58H82O6P2; copper(II) nitrate In tetrahydrofuran at 55℃; for 12h; Schlenk technique; Inert atmosphere; | 75% |
With potassium phosphate; sodium hypophosphite; 2,2-dimethylpropanoic anhydride; palladium diacetate; tricyclohexylphosphine In tetrahydrofuran at 60℃; for 16h; | 70% |
Conditions | Yield |
---|---|
With bis-{4-methoxy-phenyl}-selenoxyde; sodium hydrogencarbonate In acetonitrile at 75℃; for 5h; | 88% |
With potassium hydrogencarbonate; dimethyl sulfoxide for 0.05h; Microwave irradiation; | 87% |
With manganese(IV) oxide In chloroform at 60℃; for 6h; | 58% |
Conditions | Yield |
---|---|
With zirconium dioxide hydrate; isopropyl alcohol at 60℃; for 0.25h; Meerwein-Ponndorf-Verley Reduction; | 100% |
With 2BH4(1-)*Zn(2+)*Cl2Na2 In acetonitrile at 20℃; for 0.0833333h; | 98% |
With hydrogen In methanol at 20℃; for 5h; chemoselective reaction; | 98% |
n-butyllithium
2-methylphenyl aldehyde
1-(2-methylphenyl)-1-pentanol
Conditions | Yield |
---|---|
With (S)-1-ethyl-3-morpholinopyrrolidine In tetrahydrofuran at -78℃; for 1h; Addition; | 100% |
In tetrahydrofuran; diethyl ether at -78 - 20℃; for 2h; | 89% |
With C16H18NO(1-)*Li(1+) In tetrahydrofuran at -78℃; for 2h; Solvent; Reagent/catalyst; Inert atmosphere; | 88% |
With carbon monoxide In tetrahydrofuran; diethyl ether at -135℃; for 2h; | 68% |
nitromethane
2-methylphenyl aldehyde
methyl-2 β-nitrostyrene
Conditions | Yield |
---|---|
ammonium acetate at 90℃; for 2h; | 100% |
With sodium hydroxide |
1,1-dimethylhydrazine
2-methylphenyl aldehyde
2-methylbenzaldehyde N,N-dimethylhydrazone
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; Inert atmosphere; | 100% |
With magnesium sulfate In dichloromethane at 20℃; for 16h; | 66% |
Conditions | Yield |
---|---|
With sulphated zirconia at 0℃; for 4.2h; regioselective reaction; | 100% |
1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione at 20℃; for 1.2h; | 98% |
With indium(III) bromide at 20℃; for 0.1h; | 97% |
carbon tetrabromide
2-methylphenyl aldehyde
1,1-dibromo-2-(2-methylphenyl)ethene
Conditions | Yield |
---|---|
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0℃; for 1h; Inert atmosphere; Stage #2: 2-methylphenyl aldehyde In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: 2-methylphenyl aldehyde In dichloromethane at 20℃; for 1h; Inert atmosphere; | 98% |
With triphenylphosphine In dichloromethane at 0℃; for 0.5h; | 91% |
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
With sodium sulfate In dichloromethane for 2h; | |
at 20℃; for 1h; | |
at 20℃; for 1h; |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); tri-tert-butyl phosphine; 1-(Prop-2-enyl)-1,2,3,4,5-pentamethylcyclopenta-2,4-dien In hexane; toluene at 0℃; | 100% |
With tri-tert-butyl phosphine; bis(1,5-cyclooctadiene)nickel (0) In tetrahydrofuran; hexane; water at 20℃; for 20h; | 81% |
Conditions | Yield |
---|---|
With potassium hydroxide In acetonitrile at 20℃; for 4h; Darzens condensation; | 100% |
With potassium hydroxide In dichloromethane at 20℃; Darzens condensation; | 75% |
Conditions | Yield |
---|---|
With potassium cyanide; 18-crown-6 ether; chiral salen-based titanium In dichloromethane at -40℃; for 24h; | 100% |
With 2,6-dimethylpyridine; 2C2H5O4S(1-)*C72H104N4O16V2(2+) In dichloromethane at -20℃; for 12h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 97% |
With 1H-imidazole; C2H5O4S(1-)*C36H54N2O4V(1+) In dichloromethane at -20℃; for 18h; Inert atmosphere; optical yield given as %ee; | 96% |
With potassium cyanide; 18-crown-6 ether; titanium(salen) complex In dichloromethane at -40℃; for 24h; |
2-methylphenyl aldehyde
methylamine
N-[(2-methylphenyl)methylene]methanamine
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
In methanol; dichloromethane for 18h; Molecular sieve; | 100% |
In ethanol at 0 - 40℃; | 90% |
2-methylphenyl aldehyde
2-methylbenzoic acid (2-methylphenyl)methyl ester
Conditions | Yield |
---|---|
With C18BF16(1-)*C34H53F2NiOP2(1+) In toluene at 60℃; for 1h; Glovebox; Inert atmosphere; | 100% |
With phenylmethanethiol; phenylmagnesium bromide In tetrahydrofuran; diethyl ether at 65℃; for 96h; Tishchenko reaction; Inert atmosphere; | 87% |
With Rh(PhBP3)(H)2(NCMe); hydrogen In toluene at 20℃; under 760.051 Torr; for 0.166667h; Tishchenko reaction; | 81% |
With Me2SiCp''2Th(n-C4H9) In benzene-d6 at 25℃; for 24h; Tishchenko reaction; chemoselective reaction; | 70% |
Th(NEtMe)4 In benzene-d6 at 20℃; for 48h; Tishchenko reaction; | 50 % Chromat. |
2-trimethylsilyl-1-phenyl-2-propen-1-one
2-methylphenyl aldehyde
C20H24O2Si
Conditions | Yield |
---|---|
With tris(2,4,6-trimethoxyphenyl)phosphine In propyl cyanide sila-Morita-Baylis-Hillman reaction; Inert atmosphere; | 100% |
2-methylphenyl aldehyde
tert-butyl (E,E)-3-[2-(2-methylbenzylideneamino)phenyl]propenoate
Conditions | Yield |
---|---|
With acetic acid In benzene for 12h; Molecular sieve; Inert atmosphere; optical yield given as %de; | 100% |
benzyl 2-amino-2,2-diphenylacetate
2-methylphenyl aldehyde
benzyl 2-(2-methylbenzylideneamino)-2,2-diphenylacetate
Conditions | Yield |
---|---|
In benzene Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
Stage #1: trimethylsilyl cyanide; 2-methylphenyl aldehyde; (S,S,S)-[Ru(2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl)bis(phenylglycinate)] In tetrahydrofuran; tert-butyl methyl ether at -78℃; for 0.166667h; Inert atmosphere; Stage #2: lithium chloride In tetrahydrofuran; tert-butyl methyl ether at -78℃; for 1h; Product distribution / selectivity; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
at 20℃; for 1h; | |
at 20℃; for 1h; |
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; 2,6-bis-[1-(2,6-diethylphenylimino)ethyl]pyridine iron(II) chloride In dichloromethane at 20℃; Mukaiyama Aldol Addition; Inert atmosphere; | 100% |
With silver hexafluoroantimonate; [RuCl2((4R)-2-[2-(diphenylphosphino)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole)2] In dichloromethane at 20℃; Mukaiyama Aldol Addition; | 92% |
With C33H29FeNO2P(1+)*I(1-) In acetonitrile at 20℃; for 0.25h; Mukaiyama aldol reaction; | 70% |
cis, trans-1,3-dimethylaminocyclohexane
2-methylphenyl aldehyde
C24H30N2
Conditions | Yield |
---|---|
In methanol at 20℃; Molecular sieve; | 100% |
In methanol at 20℃; Molecular sieve; |
Conditions | Yield |
---|---|
With zinc In tetrahydrofuran at 0℃; for 1h; | 100% |
With magnesium; mercury dichloride In diethyl ether Inert atmosphere; | 96% |
With 2,4,6-trimethyl-pyridine; bis(cyclopentadienyl)titanium dichloride; manganese; chloro-trimethyl-silane In tetrahydrofuran at 20℃; for 7h; Barbier Coupling Reaction; Inert atmosphere; chemoselective reaction; | 90% |
(R)-1-phenyl-ethyl-amine
2-methylphenyl aldehyde
(R)-N-(2-methylbenzylidene)-1-phenylethanamine
Conditions | Yield |
---|---|
In toluene at 100℃; for 2h; Inert atmosphere; | 100% |
With magnesium sulfate In dichloromethane at 20℃; for 24h; |
Conditions | Yield |
---|---|
Stage #1: N-prenyl-N-propargyltosylamide With ethylmagnesium bromide In tetrahydrofuran at 50℃; for 1h; Stage #2: 2-methylphenyl aldehyde In tetrahydrofuran at 20℃; for 3h; | 100% |
Stage #1: N-prenyl-N-propargyltosylamide With ethylmagnesium bromide In tetrahydrofuran at 50℃; for 1h; Stage #2: 2-methylphenyl aldehyde In tetrahydrofuran at 20℃; for 3h; |
dimethyl (2-oxo-2-(1H-pyrrol-1-yl)ethyl)phosphonate
2-methylphenyl aldehyde
(E)-1-(1H-pyrrol-1-yl)-3-(o-tolyl)prop-2-en-1-one
Conditions | Yield |
---|---|
Stage #1: dimethyl (2-oxo-2-(1H-pyrrol-1-yl)ethyl)phosphonate With N-ethyl-N,N-diisopropylamine; lithium chloride In acetonitrile at 0℃; for 0.333333h; Stage #2: 2-methylphenyl aldehyde In acetonitrile at 20℃; for 15h; | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 18h; Inert atmosphere; Molecular sieve; | 100% |
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