Hangzhou Yunuo Chemical Co., Ltd is located in Hangzhou city China. As a global supplier in the chemical industry, Yunuochem is to create added value for customers around the world. Sticking to such business idea of "Good faith wins th
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:52927-22-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:52927-22-7
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:52927-22-7
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:52927-22-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
Cas:52927-22-7
Min.Order:1 Kilogram
FOB Price: $0.9 / 1.0
Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 11 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.
Cas:52927-22-7
Min.Order:1 Gram
FOB Price: $7.0
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:52927-22-7
Min.Order:1 Kilogram
FOB Price: $100.0 / 150.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:52927-22-7
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:52927-22-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryChemical Name: 6-Cyano-2-naphthol CAS No.: 52927-22-7 Molecular Formula: C11H7NO Molecular weight: 169.18 Appearance: Off-white to pale brown powdersolid Appearance: pale brown powder solid Storage:Store in cool and dry place, away from sun light.
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:52927-22-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:52927-22-7
Min.Order:1 Kilogram
FOB Price: $24.0 / 27.0
Type:Trading Company
inquiry6-Cyano-2-naphthol CAS:52927-22-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:52927-22-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:52927-22-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:52927-22-7
Min.Order:1 Kilogram
FOB Price: $25.0 / 40.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:52927-22-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:52927-22-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:52927-22-7
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:52927-22-7
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:52927-22-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry6-Cyano-2-naphtholAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:Steroids, Cosmetics Ingredients, APIs, Intermediates, OLED&Batte
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:52927-22-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:52927-22-7
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:52927-22-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:52927-22-7
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiry6-cyanonaphthalen-2-yl 4-methylbenzenesulfonate
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With tetraethylammonium perchlorate; triethylamine In dimethyl sulfoxide at 20℃; for 6h; Electrolysis; Green chemistry; | 94% |
2-cyano-6-methoxynaphthalene
6-cyano-2-naphthol
Conditions | Yield |
---|---|
91% | |
With tetrachlorosilane; borontrifluoride acetic acid; lithium iodide In toluene; acetonitrile at 70℃; for 10h; | 83% |
With boron tribromide In dichloromethane at -78 - 20℃; for 16h; Inert atmosphere; | 69% |
With sodium cyanide In dimethyl sulfoxide at 160 - 170℃; for 12h; | 62% |
With boron tribromide |
trifluoromethanesulfonic acid 6-cyano-naphthalen-2-yl ester
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With tetraethylammonium perchlorate; triethylamine In dimethyl sulfoxide at 20℃; for 9h; Electrolysis; Green chemistry; | 91% |
6-bromo-naphthalen-2-ol
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With CuCN In N,N-dimethyl-formamide at 160 - 170℃; for 3h; | 83% |
56% | |
In ethanol; N,N-dimethyl-formamide | |
In ethanol; N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 160 - 170℃; for 4h; Inert atmosphere; | 83% |
In N,N-dimethyl-formamide at 135℃; for 18h; | 62% |
In N,N-dimethyl-formamide at 150℃; | 60% |
6-hydroxynaphthalene-2-carbaldehyde
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride In dimethyl sulfoxide at 100℃; for 1h; | 70% |
6-acetoxy-[2]naphthonitrile
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With potassium hydroxide |
acetate of α,α,α',α'-tetrabromo-3,4-xylenol
acrylonitrile
A
6-cyano-2-naphthol
B
7-hydroxynaphthalene-2-carbonitrile
Conditions | Yield |
---|---|
1) NaI, DMF; 2) hydrolysis; Yield given. Multistep reaction. Title compound not separated from byproducts; |
benzoate of α,α,α',α'-tetrabromo-3,4-xylenol
acrylonitrile
A
6-cyano-2-naphthol
B
7-hydroxynaphthalene-2-carbonitrile
Conditions | Yield |
---|---|
1) NaI, DMF; 2) NaOH, CH3OH; Yield given. Multistep reaction; | |
1) NaI, DMF; 2) NaOH, CH3OH; Yield given. Multistep reaction. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With pyridine; copper(II) sulfate In N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
With 1,3-dimethyl-2-imidazolidinone at 160℃; for 3h; Substitution; |
2-Bromo-6-methoxynaphthalene
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With boron tribromide demethylation; |
3,4-dimethylphenyl benzoate
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 91 percent / bromosuccinimide, azoisobutyronitrile / CCl4 / 12 h / Heating; Irradiation 2: 91 percent / NBS, azoisobutyronitrile / CCl4 / 12 h / Heating 3: 1) NaI, DMF; 2) NaOH, CH3OH View Scheme | |
Multi-step reaction with 2 steps 1: 88.5 percent / bromosuccinimide, azoisobutyronitrile / CCl4 / 25 h / Heating; Irradiation 2: 1) NaI, DMF; 2) NaOH, CH3OH View Scheme |
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / NBS, azoisobutyronitrile / CCl4 / 12 h / Heating 2: 1) NaI, DMF; 2) NaOH, CH3OH View Scheme |
6-bromonaphthalen-2-yl acetate
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper (II)-sulfate; pyridine / 180 - 190 °C 2: methanol. KOH-solution View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride; CaCl2 In water |
Conditions | Yield |
---|---|
With perchloric acid In water at 25℃; for 10h; Kinetics; Concentration; |
β-naphthol
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: bromine / acetic acid 1.2: 3 h / Reflux 2.1: N,N-dimethyl-formamide / 4 h / 160 °C View Scheme | |
Multi-step reaction with 2 steps 1: acetic acid; tin; bromine / 3 h / Reflux 2: N,N-dimethyl-formamide / 4 h / 160 - 170 °C / Inert atmosphere View Scheme |
6-methoxy-3,4-dihydro-1(2H)-naphthalenone
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C 1.2: 2 h / 20 °C 2.1: sodium azide; trifluorormethanesulfonic acid / acetonitrile / 1 h / 0 - 20 °C 3.1: sodium tetrahydroborate / ethanol / 2 h / 0 - 20 °C 4.1: toluene-4-sulfonic acid / toluene / 16 h / Reflux 5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 16 h / 90 °C 6.1: boron tribromide / dichloromethane / 16 h / -78 - 20 °C / Inert atmosphere View Scheme |
6-Methoxy-2-hydroxymethylen-1-tetralon
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: sodium azide; trifluorormethanesulfonic acid / acetonitrile / 1 h / 0 - 20 °C 2: sodium tetrahydroborate / ethanol / 2 h / 0 - 20 °C 3: toluene-4-sulfonic acid / toluene / 16 h / Reflux 4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 16 h / 90 °C 5: boron tribromide / dichloromethane / 16 h / -78 - 20 °C / Inert atmosphere View Scheme |
1-hydroxy-2-cyano-6-methoxy-1,2,3,4-tetrahydronaphthalene
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: toluene-4-sulfonic acid / toluene / 16 h / Reflux 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 16 h / 90 °C 3: boron tribromide / dichloromethane / 16 h / -78 - 20 °C / Inert atmosphere View Scheme |
6-methoxy-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carbonitrile
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: sodium tetrahydroborate / ethanol / 2 h / 0 - 20 °C 2: toluene-4-sulfonic acid / toluene / 16 h / Reflux 3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 16 h / 90 °C 4: boron tribromide / dichloromethane / 16 h / -78 - 20 °C / Inert atmosphere View Scheme |
6-methoxy-3,4-dihydronaphthalene-2-carbonitrile
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 16 h / 90 °C 2: boron tribromide / dichloromethane / 16 h / -78 - 20 °C / Inert atmosphere View Scheme |
6-Hydroxy-2-naphthoic acid
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: N,N-dimethyl-formamide; thionyl chloride / 5 h / 70 °C 2.1: ammonium hydroxide / tetrahydrofuran; water / 16 h / 25 °C 3.1: trifluoroacetic anhydride / tetrahydrofuran / 0.5 h / 0 - 25 °C 3.2: 16 h / 25 °C View Scheme |
6-hydroxynaphthalene-2-carboxamide
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Stage #1: 6-hydroxynaphthalene-2-carboxamide With trifluoroacetic anhydride In tetrahydrofuran at 0 - 25℃; for 0.5h; Stage #2: With pyridine In tetrahydrofuran at 25℃; for 16h; |
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: ammonium hydroxide / tetrahydrofuran; water / 16 h / 25 °C 2.1: trifluoroacetic anhydride / tetrahydrofuran / 0.5 h / 0 - 25 °C 2.2: 16 h / 25 °C View Scheme |
6-bromo-naphthalen-2-ol
4-cyanophenylboronic acid
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 80℃; for 8h; Suzuki-Miyaura Coupling; High pressure; Inert atmosphere; |
6-cyano-2-naphthol
6-(aminomethyl)naphthalen-2-ol
Conditions | Yield |
---|---|
With ammonia; hydrogen; nickel In methanol; water | 100% |
6-cyano-2-naphthol
D-cysteine hydrochloride
(S)-2-(6-hydroxynaphthalen-2-yl)-4,5-dihydrothiazole-4-carboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 80℃; for 5h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; | 100% |
6-cyano-2-naphthol
4-Methylbenzyl bromide
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; | 98% |
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-(((S)-(6-methoxyquinolin-4-yl)((1S,2S,4S,5R)-5-vinylquinuclidin-2-yl)methyl)amino)cyclobut-3-ene-1,2-dione In dichloromethane at 20℃; for 1h; stereoselective reaction; | 98% |
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-(((S)-(6-methoxyquinolin-4-yl)((1S,2S,4S,5R)-5-vinylquinuclidin-2-yl)methyl)amino)cyclobut-3-ene-1,2-dione In dichloromethane at 20℃; for 1h; stereoselective reaction; | 98% |
6-cyano-2-naphthol
4-methylphenylboronic acid
6-p-tolyl-2-naphthonitrile
Conditions | Yield |
---|---|
Stage #1: 6-cyano-2-naphthol With potassium phosphate; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate In 1,4-dioxane at 100℃; for 3h; Inert atmosphere; Stage #2: 4-methylphenylboronic acid With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In 1,4-dioxane at 100 - 110℃; Suzuki-Miyaura coupling; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With stannic bromide In dichloromethane at 20℃; for 24h; Friedel-Crafts Alkylation; Inert atmosphere; | 97% |
trifluoromethylsulfonic anhydride
6-cyano-2-naphthol
trifluoromethanesulfonic acid 6-cyano-naphthalen-2-yl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 48h; | 95% |
With triethylamine In dichloromethane at 20℃; | 93% |
With pyridine In dichloromethane at 20℃; | 79.1% |
6-cyano-2-naphthol
2,5,8,11-tetraoxatridecan-13-ol tosylate
Conditions | Yield |
---|---|
With potassium hydroxide In 1,2-dimethoxyethane at 80℃; for 16h; Williamson etherification; | 95% |
6-cyano-2-naphthol
p-toluenesulfonyl chloride
6-cyanonaphthalen-2-yl 4-methylbenzenesulfonate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; | 95% |
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; | 95% |
Stage #1: 6-cyano-2-naphthol With triethylamine In dichloromethane at 0℃; for 0.166667h; Stage #2: p-toluenesulfonyl chloride In dichloromethane at 20℃; for 4h; | 90% |
With dmap; triethylamine In dichloromethane at 20℃; |
6-cyano-2-naphthol
4-methoxycarbonylphenylboronic acid
methyl 4-(2-cyanonaphthalen-6-yl)benzoate
Conditions | Yield |
---|---|
Stage #1: 6-cyano-2-naphthol With potassium phosphate; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate In 1,4-dioxane at 100℃; for 3h; Inert atmosphere; Stage #2: 4-methoxycarbonylphenylboronic acid With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In 1,4-dioxane at 100 - 110℃; Suzuki-Miyaura coupling; Inert atmosphere; | 95% |
6-cyano-2-naphthol
Diphenylphosphine oxide
6-(diphenylphosphoryl)-2-naphthonitrile
Conditions | Yield |
---|---|
Stage #1: 6-cyano-2-naphthol With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate In acetonitrile at 100℃; for 3h; Inert atmosphere; Stage #2: Diphenylphosphine oxide With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In acetonitrile at 100℃; for 18h; Inert atmosphere; | 95% |
6-cyano-2-naphthol
6-(difluoromethoxy)-2-naphthonitrile
Conditions | Yield |
---|---|
With sodium hydroxide; phenol In N,N-dimethyl-formamide at 75℃; for 4h; Sealed tube; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With 1,3,4-triphenyl-1,2,4-triazolium hexafluorophosphate; potassium tert-butylate In chloroform at 20℃; for 4h; Inert atmosphere; | 95% |
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate In acetonitrile for 12h; Williamson Ether Synthesis; Reflux; | 95% |
6-cyano-2-naphthol
methanesulfonyl chloride
6-cyanonaphthalen-2-yl methanesulfonate
Conditions | Yield |
---|---|
Stage #1: 6-cyano-2-naphthol With triethylamine In toluene at 0℃; for 0.166667h; Stage #2: methanesulfonyl chloride In toluene at 20℃; for 12h; | 93% |
With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 70℃; for 4h; | 93% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; | 93% |
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; | 93% |
With potassium carbonate In acetonitrile at 80℃; | 93% |
1-ethynyl-2-methylbenzene
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone In chloroform; toluene at 80℃; for 2h; Inert atmosphere; Schlenk technique; | 93% |
trifluorormethanesulfonic acid
6-cyano-2-naphthol
trifluoromethanesulfonic acid 6-cyano-naphthalen-2-yl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 93% |
Conditions | Yield |
---|---|
With phosphorous acid In water; 1,2-dichloro-ethane at 100℃; for 18h; Schlenk technique; regioselective reaction; | 93% |
6-cyano-2-naphthol
5-bromo-6-hydroxy-2-naphthonitrile
Conditions | Yield |
---|---|
With bromine; acetic acid at 20℃; | 92% |
With bromine; acetic acid at 25℃; for 2.5h; | |
With N-Bromosuccinimide In acetonitrile at 0 - 20℃; for 4h; Inert atmosphere; | |
With pyridinium perbromide hydrobromide In acetonitrile at 0℃; | |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 0 - 25℃; Inert atmosphere; Schlenk technique; |
1-phenyl-3-(trimethylsilyl)prop-2-yn-1-yl acetate
6-cyano-2-naphthol
Conditions | Yield |
---|---|
With (S)-N-[(3,5-dimethylphenyl)(pyridin-2-yl)methylene]-1-[2-(diphenylphosphino)phenyl]ethanamine; copper(II) acetate monohydrate; N-ethyl-N,N-diisopropylamine In methanol at -20℃; for 12h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 92% |
Stage #1: 1-phenyl-3-(trimethylsilyl)prop-2-yn-1-yl acetate; 6-cyano-2-naphthol With (S)-N-[(3,5-dimethylphenyl)(pyridin-2-yl)methylene]-1-[2-(diphenylphosphino)phenyl]ethanamine; copper(II) acetate monohydrate In methanol for 1h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In methanol for 24h; Inert atmosphere; | 90% |
6-cyano-2-naphthol
Conditions | Yield |
---|---|
Stage #1: 6-cyano-2-naphthol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper(II) bis(trifluoromethanesulfonate) In acetic acid at 100℃; for 0.166667h; Stage #2: C10H9BrOS2 In acetic acid at 100℃; for 4h; chemoselective reaction; | 92% |
6-cyano-2-naphthol
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride
6-cyanonaphthalen-2-yl bis(2-oxo-3-oxazolidinyl)phosphoramide
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; Inert atmosphere; | 91% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View