Dayang Chem (Hangzhou) Co.,Ltd.
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:527-85-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryZhuozhou Wenxi import and Export Co., Ltd
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:527-85-5
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryShanghai Upbio Tech Co.,Ltd
1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:527-85-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Win-Win chemical Co.Ltd
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:527-85-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryGIHI CHEMICALS CO.,LIMITED
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Henan Allgreen Chemical Co.,Ltd
high qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Antimex Chemical Limied
2-MethylbenzamideAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:Sea/air/courier
Henan Tianfu Chemical Co., Ltd.
best price high quality Storage:Room Temperature Application:For pharmacy chemicals Transportation:by sea,air
BOC Sciences
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:yellowis to white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use
Hangzhou Fandachem Co.,Ltd
2-Methylbenzamide cas 527-85-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Hangzhou Sartort Biopharma Co., Ltd
Best quality with low priceAppearance:white powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
Hebei Quanhe Biotechnology Co. LTD
1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta
ZHEJIANG JIUZHOU CHEM CO.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Jilin haofei import and export trade Co.,Ltd
Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
Finetech Industry Limited
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the O-TOLUAMIDE, CAS:527-85-5 with the most competitive price and the best quality. We ca
Changzhou Foreign Trade Corp
CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio
NovaChemistry
high purity Application:Drug intermediates Materials intermediates and active molecules
Synthetic route
| Conditions | Yield |
|---|---|
| With C18H57O3P6Ru2(1+)*C6H5O(1-)*C6H6O; water In 1,4-dioxane for 24h; Time; Sealed tube; Inert atmosphere; Schlenk technique; | 99% |
| With sodium hydroxide; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate In dichloromethane for 1.6h; Ambient temperature; | 97% |
| With water; sodium carbonate; tricyclohexylphosphine; {Rh(OMe)(cod)}2 In isopropyl alcohol at 25℃; for 24h; | 96% |
-
-
20045-96-9
o-methylbenzoyl bromide
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| Stage #1: o-methylbenzoyl bromide With aluminum isopropoxide; dimethyl amine In Cyclooctan at 36℃; for 3h; Stage #2: With potassium sulfate; zinc 2-ethylhexanoate at 47℃; for 3.16667h; Temperature; | 98.8% |
| Conditions | Yield |
|---|---|
| Stage #1: ortho-methylbenzoic acid With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In tetrahydrofuran for 0.0166667h; Milling; Stage #2: With ammonium thiocyanate In tetrahydrofuran for 0.0833333h; Milling; | 98% |
| With ammonium hydroxide In ethyl acetate at 40℃; for 16h; Solvent; Temperature; Reagent/catalyst; Large scale; Green chemistry; | 97.7% |
| Multi-step reaction with 2 steps 1: phosphorus pentachloride / 120 °C View Scheme |
-
-
14683-79-5
salicylaldoxime
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With C55H45ClN5P2Ru(1+)*Cl(1-) In water at 110℃; for 12h; Sealed tube; | 98% |
| With [PdCl2{κ2-(P,N)-2-Ph2PC6H4CH=NOH}] In water at 100℃; for 24h; Inert atmosphere; Sealed tube; | 90% |
| With [RuCl2(η2-C6H6){P(NMe2)3}]; water at 100℃; for 7h; Inert atmosphere; Sealed tube; | 87% |
| With cis,cis,trans-[RuCl2{κ2-(P,N)-2-Ph2PC6H4CH=NOH}2] In water at 100℃; for 12h; Sealed tube; Inert atmosphere; | 82% |
| With zinc(II) chloride In n-heptane for 18h; Reflux; |
| Conditions | Yield |
|---|---|
| With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; silver trifluoroacetate; phenylhydrazine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In N,N-dimethyl-formamide at 70℃; for 12h; Reagent/catalyst; Solvent; | 96.6% |
| With tert.-butylhydroperoxide; ammonia; oxygen In water; N,N-dimethyl-formamide at 80℃; under 1520.1 Torr; for 5h; Green chemistry; | 89% |
| With tert.-butylhydroperoxide; ammonium hydroxide In water at 100℃; for 16h; | 87% |
| With tert.-butylhydroperoxide; tetraethylammonium iodide; ammonium bicarbonate In 1,2-dichloro-ethane at 70℃; for 22h; | 69% |
| Conditions | Yield |
|---|---|
| With hydroxylamine; C33H28F3N5O3Ru(1+)*Cl(1-) In water at 60℃; for 0.5h; Catalytic behavior; Sonication; | 96% |
| With C17H17BrClN2RuSe(1+)*F6P(1-); hydroxylamine hydrochloride; sodium hydroxide In toluene at 100℃; for 12h; Reagent/catalyst; Solvent; Temperature; | 94% |
| With tert.-butylhydroperoxide; titanium superoxide; saccharin In 1,4-dioxane; hexane at 90℃; for 1h; Green chemistry; | 91% |
| Conditions | Yield |
|---|---|
| With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); potassium tert-butylate In tert-butyl alcohol at 70℃; for 12h; | 95% |
| With tetra(n-butyl)ammonium hydroxide In water at 70℃; for 12h; Green chemistry; | 89% |
| With potassium tert-butylate; C36H24N2O12Ru3 In tert-butyl alcohol for 10h; Reflux; | 83% |
-
-
933-88-0
ortho-toluoyl chloride
-
-
58-61-7
adenosine
-
A
-
628-13-7
pyridine hydrochloride
-
B
-
104579-36-4
N6,2',3',5'-tetra-O-toluoyladenosine
-
C
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With methanol; ammonia In pyridine at 0℃; | A n/a B 93% C n/a |
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane; N-methoxylamine hydrochloride; sodium iodide; palladium dichloride In acetonitrile at 90℃; under 3800.26 Torr; for 8h; Autoclave; Inert atmosphere; | 93% |
| With 1,4-diaza-bicyclo[2.2.2]octane; palladium 10% on activated carbon; ammonium carbamate; potassium iodide In acetonitrile at 90℃; for 8h; Autoclave; Green chemistry; | 88% |
| With dichloro bis(acetonitrile) palladium(II); ammonium bicarbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In acetonitrile at 120℃; under 7500.75 Torr; for 3h; Autoclave; | > 99 %Chromat. |
| Conditions | Yield |
|---|---|
| With palladium diacetate; ammonium bicarbonate; dicyclohexyl-carbodiimide; triphenylphosphine In acetonitrile at 100℃; Inert atmosphere; | 93% |
| Conditions | Yield |
|---|---|
| With phosphate buffer at 30℃; for 5.5h; rhodococcus rhodocrous AJ270, pH 7.0; | A 7% B 92% |
| With potassium phosphate buffer at 30℃; for 5.5h; Rhodococcus sp. AJ270 cells; | A 6.6% B 92.4% |
-
-
577-16-2, 122382-54-1
2-Methylacetophenone
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With ammonia; water; iodine In tetrahydrofuran at 20℃; for 1h; Haller-Bauer reaction; | 92% |
| With tert.-butylhydroperoxide; ammonia; tetra-(n-butyl)ammonium iodide In water at 100℃; for 16h; Green chemistry; | 51% |
-
-
127459-91-0
(Z)-2-methylbenzaldoxime
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With aluminum oxide; methanesulfonic acid at 140℃; for 3h; Beckmann rearrangement; | 90% |
| Conditions | Yield |
|---|---|
| With water; potassium carbonate In dimethyl sulfoxide at 110℃; for 12h; | 90% |
| Conditions | Yield |
|---|---|
| With tris-(dibenzylideneacetone)dipalladium(0); (2R)-1-[(1R)-1-[bis(1,1-dimethylethyl)phosphino]ethyl]-2-(diphenylphosphino)ferrocene; ammonium carbamate; sodium hydrogencarbonate In 1,4-dioxane at 100℃; for 20h; Inert atmosphere; | 86% |
| With 2-(2'-pyridyl)(di(1-adamantyl)phosphino)benzene; ammonia; palladium diacetate In 1,4-dioxane at 120℃; under 1500.15 Torr; for 16h; Autoclave; | 70% |
| With ammonia; palladium diacetate; catacxium A In 1,4-dioxane at 100℃; under 3000.3 Torr; for 16h; Autoclave; | 90 %Chromat. |
| With 1,1'-bis-(diphenylphosphino)ferrocene; ammonia; palladium diacetate In 1,4-dioxane at 100℃; under 1500.15 Torr; for 16h; | 98 %Chromat. |
| Conditions | Yield |
|---|---|
| With hydroxylamine hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); tri tert-butylphosphoniumtetrafluoroborate In 1,4-dioxane at 110℃; for 0.333333h; microwave irradiation; | 84% |
| Conditions | Yield |
|---|---|
| With ammonium hydroxide; oxygen In tert-Amyl alcohol at 110℃; under 1500.15 Torr; for 16h; | A 82.8% B 10.4% |
| Conditions | Yield |
|---|---|
| With hydroxylamine hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); tri tert-butylphosphoniumtetrafluoroborate In 1,4-dioxane at 150℃; for 0.333333h; microwave irradiation; | 78% |
-
-
1628342-24-4
(R)-2-amino-3-(((2-methylbenzoyl)carbamothioyl)thio)propanoic acid
-
A
-
98169-56-3
(4R)-2-sulfanylidene-1,3-thiazolidine-4-carboxylic acid
-
B
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| In water for 1h; Reflux; | A n/a B 76% |
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; iron(III) chloride hexahydrate; tetrabutylammonium iodide; ammonium hydroxide In water at 80℃; for 18h; Sealed tube; | 76% |
| Conditions | Yield |
|---|---|
| With copper diacetate; palladium diacetate In water at 120℃; for 1h; Reagent/catalyst; Schlenk technique; Green chemistry; | A 48% B 75% |
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; ammonia; iodine In water at 100℃; for 3h; Sealed tube; Green chemistry; | 73% |
| Conditions | Yield |
|---|---|
| With [Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; hydroxylamine hydrochloride; sodium hydrogencarbonate In water at 100℃; for 7h; Inert atmosphere; Sealed tube; Green chemistry; | A n/a B 71% |
-
-
22364-68-7
2-tolylmethylnitrile
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; ammonium hydroxide; iodine In acetonitrile at 70℃; for 36h; Sealed tube; | 70% |
| With copper(I) oxide; oxygen; ammonium chloride; sodium hydroxide In acetonitrile at 120℃; under 760.051 Torr; for 48h; Schlenk technique; | 35% |
-
-
146448-53-5
N-<(4-Methylphenyl)sulfonyl>-2-methylbenzenecarboxamide
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With tetraethylammonium bromide In N,N-dimethyl-formamide at 20℃; | 69% |
| Conditions | Yield |
|---|---|
| With ammonia Inert atmosphere; | 62% |
| With ammonium hydroxide; diethyl ether | |
| With ammonium hydroxide In tetrahydrofuran at 20℃; for 2h; |
-
-
32622-24-5
N-phenyl-2-(2-methylphenyl)formamidine
-
-
100-51-6
benzyl alcohol
-
A
-
758640-21-0
N-Benzylaniline
-
B
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With potassium hydroxide In toluene at 120℃; for 15h; Schlenk technique; Glovebox; Inert atmosphere; Sealed tube; | A 62 %Chromat. B 58% |
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With ammonium carbonate In dimethyl sulfoxide at 25℃; for 6h; | 51% |
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; ammonia In water at 105℃; for 16h; | 50% |
| Conditions | Yield |
|---|---|
| With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; silver(I) acetate In N,N-dimethyl-formamide for 12h; Ambient temperature; or Hg(OAc)2, NBS-Hg(OAc)2; | 100% |
| With tetra-N-butylammonium tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 1.5h; Ambient temperature; | 97% |
| With sodium bromide In acetonitrile at 50℃; for 6h; Hofmann Rearrangement; Electrochemical reaction; Green chemistry; | 93% |
| Conditions | Yield |
|---|---|
| With iodobenzene; oxone; water In acetonitrile at 20℃; | 100% |
| With sodium hydrogen sulfate; [bis(acetoxy)iodo]benzene In water; acetonitrile at 20℃; for 0.583333h; | 85% |
| Conditions | Yield |
|---|---|
| With per-rhenic acid In water; 1,3,5-trimethyl-benzene for 24h; Heating; | 99% |
| With per-rhenic acid In water; 1,3,5-trimethyl-benzene for 24h; Heating; | 97% |
| With iron(II) chloride tetrahydrate; N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide In tetrahydrofuran at 70℃; for 2h; | 96% |
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With N-iodo-succinimide; trifluoroacetic acid at 20℃; for 3h; regioselective reaction; | 99% |
-
-
527-85-5
o-Methylbenzamid
-
-
76503-37-2
3-amido-4-methylbenzenesulfonyl chloride
| Conditions | Yield |
|---|---|
| With chlorosulfonic acid at 70℃; for 2h; | 98% |
-
-
603-35-0
triphenylphosphine
-
-
527-85-5
o-Methylbenzamid
-
-
95978-80-6
N-o-toluoyltriphenylphospha-λ5-azene
| Conditions | Yield |
|---|---|
| With diethylazodicarboxylate In tetrahydrofuran at 0 - 25℃; for 12h; | 97% |
| Conditions | Yield |
|---|---|
| With samarium diiodide; water In tetrahydrofuran for 0.00277778h; Ambient temperature; | 96% |
| With C24H20ClN2OPRu; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 10640.7 Torr; for 36h; Inert atmosphere; Schlenk technique; | 85% |
| With sodium amalgam; ethanol |
-
-
302-17-0
chloral hydrate
-
-
527-85-5
o-Methylbenzamid
-
-
51361-17-2
N-(2,2,2-trichloro-1-hydroxyethyl)-2-methylbenzamide
| Conditions | Yield |
|---|---|
| at 90 - 100℃; | 95% |
| Heating; |
-
-
651768-37-5
6-bromo-2-(2-methoxyethyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione
-
-
527-85-5
o-Methylbenzamid
| Conditions | Yield |
|---|---|
| With palladium [2'-(amino-κN)[1,1'-biphenyl]-2-yl-κC][[5-(diphenylphosphino)-9,9-dimethyl-9H-xanthen-4-yl]diphenylphosphine-κP](methanesulfonato-κO); caesium carbonate In 1,4-dioxane at 100℃; for 1.66667h; Inert atmosphere; | 95% |
-
-
91-01-0
1,1-Diphenylmethanol
-
-
527-85-5
o-Methylbenzamid
-
-
10254-11-2
N-(diphenylmethyl)-2-methylbenzamide
| Conditions | Yield |
|---|---|
| With Bromodiphenylmethane In neat (no solvent) at 130℃; for 24h; Temperature; Sealed tube; Green chemistry; | 94% |
| With silica perchloric acid In 1,4-dioxane for 5h; Reflux; | 82% |
-
-
527-85-5
o-Methylbenzamid
-
-
14865-38-4
o-tolylmethanamine monohydrochloride
| Conditions | Yield |
|---|---|
| Stage #1: o-Methylbenzamid With bis(cyclopentadienyl)dihydrozirconium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane at 20℃; under 760.051 Torr; for 24h; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 93% |
| Stage #1: o-Methylbenzamid With [(aNHC)KN(SiMe3)2]2; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 40℃; for 12h; Inert atmosphere; Glovebox; Schlenk technique; Stage #2: With water; sodium hydroxide In diethyl ether; toluene at 40℃; for 1h; Inert atmosphere; Glovebox; Schlenk technique; Stage #3: With hydrogenchloride In diethyl ether; water Inert atmosphere; Glovebox; Schlenk technique; | 89% |
| Stage #1: o-Methylbenzamid With phenylsilane; C28H18ClMnN2O2; potassium tert-butylate In tetrahydrofuran at 50℃; for 12h; Inert atmosphere; Glovebox; Stage #2: With sodium hydroxide In tetrahydrofuran for 3h; Inert atmosphere; Glovebox; Stage #3: With hydrogenchloride In methanol; diethyl ether Glovebox; Inert atmosphere; | 84% |
| Yield given. Multistep reaction; |
| Conditions | Yield |
|---|---|
| With t-BuBrettPhos; water; palladium diacetate; caesium carbonate In tert-butyl alcohol at 110℃; for 2h; Inert atmosphere; | 93% |
| Conditions | Yield |
|---|---|
| With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate In acetonitrile at 115℃; for 10h; Inert atmosphere; | 93% |
| Conditions | Yield |
|---|---|
| In toluene at 100℃; for 12h; | 93% |
| Conditions | Yield |
|---|---|
| With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 110℃; for 4h; Inert atmosphere; Sealed tube; | 92% |
| Conditions | Yield |
|---|---|
| With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate In tert-Amyl alcohol at 20 - 100℃; for 12.33h; Schlenk technique; Sealed tube; regioselective reaction; | 92% |
| Conditions | Yield |
|---|---|
| With tri(sec-butyl)borane; (DiMeIHeptCl)Pd(cinammyl)Cl; caesium carbonate In toluene at 80℃; for 24h; Inert atmosphere; Sealed tube; Schlenk technique; | 92% |
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