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Wuhan Jadechem International Trade Co.,Ltd.

1.Our own factory in Yingcheng, Hubei province, China. It has strong production capacity, perfect equipments, advanced technique and complete quality supervision system. Welcome to visit our factory at any convenient time for business or coope

Hot sell product Chloral hydrate 302-17-0

Cas:302-17-0

Min.Order:25 Kilogram

Negotiable

Type:Trading Company

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Chloral hydrate in stock

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance White to off-white needle crystalline solid Complies Arsenic &lt

High purity Chloral hydrate with high quality cas:302-17-0

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $8.0 / 20.0

Type:Trading Company

inquiry

Xi'an Quanao Biotech Co., Ltd.

Xi’an Quanao Biotech Co., Ltd. with 18 years experience in plant extract filed. Product grade: Medicine, Health care product, Cosmetics, Food, Beverage, Feed. Hot selling market: Europe, North America, South America, Middle East, Asia Pacifi

Quanao supply 99% Chloral hydrate Powder price cas:302-17-0

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $9.0 / 29.0

Type:Manufacturers

inquiry

Jinan Finer Chemical Co., Ltd

Product description: Product name Chloral hydrate CAS number 302-17-0 Assay ≥99% Appearance White crystalline powder Capacity 500mt/year Application Pharmaceutical/pesticide

Chloral hydrate

Cas:302-17-0

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Chloral Hydrate

Cas:302-17-0

Min.Order:1

Negotiable

Type:Other

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Hubei CuiRan Biotechnology Co., Ltd

Hubei CuiRan Biotechnology Co., Ltd is a leading company in the research, development, manufacture and marketing of High Quality Phytochemicals and Extracts(especially Active Ingredients from Traditional Chinese Medicine,Traditional Chinese Medicine)

Chloralhydrate

Cas:302-17-0

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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Wuhan Kemi-Works Chemical Co., Ltd

Good quality Chloral hydrate 302-17-0 manufacturer with stable offering ability Chemical nature Chloral hydrate CAS No 302-17-0 Molecular Formular C2H3Cl3O2 Molecular weight 165.4 Properties Assay 99% min Appea… W

Good quality Chloral hydrate 302-17-0 manufacturer with stable offering ability

Cas:302-17-0

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price API 99% Chloral hydrate 302-17-0 GMP Manufacturer

Cas:302-17-0

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chengdu Lemeitian Pharmaceutical Technology Co,. Ltd

ADVANTAGE: 1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day 2. The products are provided with COA, HPLC, NMR, quality assurance,

TCA

Cas:302-17-0

Min.Order:10 Metric Ton

Negotiable

Type:Manufacturers

inquiry

ANQING CHICO PHARMACEUTICAL CO.,LTD.

High quality. Factory supply. In stock. Best price.1.Quick response within 24 hours;2.Best quality in your requirement;?3.We pay more attention on delivery time, and usually ship on time;4.Under the premise of safety and effectiveness, we can produce

Chloral hydrate

Cas:302-17-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality Chloral hydrate

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

Hot sell product Chloral hydrate 302-17-0

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $1.0 / 3.0

Type:Trading Company

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Chloral hydrate

Cas:302-17-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hubei DiBo chemical co., LTD

Name:Chloral hydrate CAS no:302-17-0 Grade:Medical, scientific research, export Molecular formula:C2H3Cl3O2 Molecular weight:165.403 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data

Chloral hydrate/cas:302-17-0/Raw material supply

Cas:302-17-0

Min.Order:25 Kilogram

FOB Price: $1.0 / 3.0

Type:Other

inquiry

Henan Tianfu Chemical Co., Ltd.

Chloral hydrate Basic information Product Name: Chloral hydrate Synonyms: CHLORAL HYDRATE;'GROUND JOINT SEPARATION AID';1,1,1-trichloro-2,2-ethanediol;2,2,2-Trichloro-1,1-ethaned

TIANFU-CHEM CAS:302-17-0 Chloral hydrate

Cas:302-17-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Chloral hydrate

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 302-17-0 with best quality

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Name: Chloral hydrate Chemical name: 2,2,2- three -1,1- ethylene glycol Molecular formula: C2H3Cl3O2 Structure type: CAS .NO:302-17-0 Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resistant and airtight containers. P

Chloral hydrate CAS:302-17-0

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry pla

99% Purity Chloral Hydrate Powder CAS 302-17-0

Cas:302-17-0

Min.Order:100 Gram

Negotiable

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Chloral hydrate 302-17-0

Cas:302-17-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: Chloral hydrate CAS: 302-17-0 MF: C2H3Cl3O2 MW: 165.4 EINECS: 206-117-5 Mol File: 302-17-0.mol Chloral hydrate Structure Chloral hydrate Chemical Properties Melting point 57 °C(lit.) Boiling point 97 &deg

Chloral hydrate

Cas:302-17-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

2-Chloral hydrate 302-17-0

Cas:302-17-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

Chloral hydrate CAS: 302-17-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia

Chloral hydrate CAS: 302-17-0

Cas:302-17-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Terui OP New Material Technology Co., Ltd.

We generally use secure shipping methods that do not require you to do any customs clearance. Free shipping to your address without worrying about any customs issues. We have a professional customs clearance team to 100% guarantee the safe delivery o

Wholesale Chloral Hydrat CAS 302-17-0 with High Purity

Cas:302-17-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Chloral hydrate

Cas:302-17-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

HUBEI RISON CHEMICAL CO.,LTD.

Located in Wuhan City of Hubei Province, Wuhan Rison Trading co., Ltd is engaged in the supply of fine specialty chemicals. Our business includes metal surface treatment, such as nickel/zinc/copper plating, perfluoro chemicals, tin salts (stannous su

Hot sell product /Chloral hydrate (TCA)

Cas:302-17-0

Min.Order:500 Kilogram

Negotiable

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:302-17-0

Cas:302-17-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Lonwin Chemical Group Limited

Chloral hydrate CAS: 302-17-0 Specification items standard result appearance white to off-white needle crystalline solid complies arsenic <1pp

Factory supply Chloral hydrate

Cas:302-17-0

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

Chloral hydrate

Cas:302-17-0

Min.Order:1 Kilogram

FOB Price: $60.0 / 70.0

Type:Lab/Research institutions

inquiry

Synthetic route

chloral
75-87-6

chloral

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
In tetrachloromethane45%
With water Thermodynamic data; ΔH;
With water
In water
N,N-dichloro-p-toluenesulfonamide
473-34-7

N,N-dichloro-p-toluenesulfonamide

Trichloroethylene
79-01-6

Trichloroethylene

A

chloral hydrate
302-17-0

chloral hydrate

B

N-(2,2,2-trichloro-1-hydroxyethyl)4-methylbenzenesulfonamide
83790-89-0

N-(2,2,2-trichloro-1-hydroxyethyl)4-methylbenzenesulfonamide

C

N-(2,2,2-trichloro-1-p-toluenesulfonamidoethyl)-p-toluenesulfonamide
93018-67-8

N-(2,2,2-trichloro-1-p-toluenesulfonamidoethyl)-p-toluenesulfonamide

D

toluene-4-sulfonamide
70-55-3

toluene-4-sulfonamide

Conditions
ConditionsYield
With water; tin(IV) chloride at 20 - 22℃; for 1560h; Product distribution; other time, temperature, Lewis acid (AlCl3);A .11 g
B 37.9%
C 2.7%
D 2.9%
ethanol
64-17-5

ethanol

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With water; chlorine
chloroacetylene
593-63-5

chloroacetylene

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With sodium hypochlorite; water; boric acid
benzoic acid hydrazide
613-94-5

benzoic acid hydrazide

A

chloral hydrate
302-17-0

chloral hydrate

B

benzoic acid-[N'-(2,2,2-trichloro-1-hydroxy-ethyl)-hydrazide]

benzoic acid-[N'-(2,2,2-trichloro-1-hydroxy-ethyl)-hydrazide]

acetaldehyde
75-07-0

acetaldehyde

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With water Chlorieren;
paracetaldehyde
123-63-7

paracetaldehyde

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With water Chlorieren;
2-chloro-ethanol
107-07-3

2-chloro-ethanol

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With water; chlorine at 90℃;
With water; iodine; chlorine at 90℃;
formic acid ethyl ester
109-94-4

formic acid ethyl ester

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With sulfuryl dichloride at 170℃;
chloral
75-87-6

chloral

2,2-Dihydroxy-3-oxo-pent-4-enoic acid tert-butyl ester
147624-92-8

2,2-Dihydroxy-3-oxo-pent-4-enoic acid tert-butyl ester

A

chloral hydrate
302-17-0

chloral hydrate

B

2,3-Dioxo-pent-4-enoic acid tert-butyl ester
117917-40-5

2,3-Dioxo-pent-4-enoic acid tert-butyl ester

Conditions
ConditionsYield
In acetone Equilibrium constant; Thermodynamic data; ΔH;
water
7732-18-5

water

chloral
75-87-6

chloral

chloral hydrate
302-17-0

chloral hydrate

sulfuryl dichloride
7791-25-5

sulfuryl dichloride

formic acid ethyl ester
109-94-4

formic acid ethyl ester

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
at 170℃;
chloroacetylene
593-63-5

chloroacetylene

water
7732-18-5

water

metaboric acid
13460-50-9

metaboric acid

sodium hypochlorite

sodium hypochlorite

A

chloral hydrate
302-17-0

chloral hydrate

B

chloroacetic acid
79-11-8

chloroacetic acid

C

dichloroacetaldehyde hydrate

dichloroacetaldehyde hydrate

acetic acid-[4-(2,2,2-trichloro-1-hydroxy-ethoxy)-anilide]
15687-05-5

acetic acid-[4-(2,2,2-trichloro-1-hydroxy-ethoxy)-anilide]

water
7732-18-5

water

A

chloral hydrate
302-17-0

chloral hydrate

B

4-acetaminophenol
103-90-2

4-acetaminophenol

2,2-diphenyl-1-(2,2,2-trichloro-ethylidenamino)-ethanol

2,2-diphenyl-1-(2,2,2-trichloro-ethylidenamino)-ethanol

diluted aq.-ethanolic hydrochloric acid

diluted aq.-ethanolic hydrochloric acid

A

chloral hydrate
302-17-0

chloral hydrate

B

(2,2-diphenyl-ethylidene)-(2,2-diphenyl-vinyl)-amine
102603-74-7

(2,2-diphenyl-ethylidene)-(2,2-diphenyl-vinyl)-amine

1-bornyloxy-2,2,2-trichloro-ethanol
20752-32-3

1-bornyloxy-2,2,2-trichloro-ethanol

water
7732-18-5

water

A

chloral hydrate
302-17-0

chloral hydrate

rac-endo-borneol
6627-72-1

rac-endo-borneol

Conditions
ConditionsYield
chloral-l-borneolate;
chloral-d-borneolate;
Trichloroethylene
79-01-6

Trichloroethylene

medaka liver microsomes

medaka liver microsomes

A

1,1,1-trichloroethanol
115-20-8

1,1,1-trichloroethanol

B

chloral hydrate
302-17-0

chloral hydrate

C

trichloroacetic acid
76-03-9

trichloroacetic acid

Conditions
ConditionsYield
In acetone at 37℃; for 1h; Enzyme kinetics; Oxidation; hydroxylation; Enzymatic reaction;
N-(2,2,2-trichloro-1-p-toluenesulfonamidoethyl)-p-toluenesulfonamide
93018-67-8

N-(2,2,2-trichloro-1-p-toluenesulfonamidoethyl)-p-toluenesulfonamide

A

chloral hydrate
302-17-0

chloral hydrate

B

toluene-4-sulfonamide
70-55-3

toluene-4-sulfonamide

Conditions
ConditionsYield
With sodium hydroxide at 20℃; for 0.5h; Product distribution;
N-(2,2,2-trichloro-1-hydroxyethyl)benzenesulfonamide
75457-08-8

N-(2,2,2-trichloro-1-hydroxyethyl)benzenesulfonamide

A

benzenesulfonamide
98-10-2

benzenesulfonamide

B

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With sodium hydroxide at 20℃; for 0.5h; Product distribution;
N-(2,2,2-trichloro-1-p-chlorobenzenesulfonamidoethyl)-p-chlorobenzenesulfonamide
107905-40-8

N-(2,2,2-trichloro-1-p-chlorobenzenesulfonamidoethyl)-p-chlorobenzenesulfonamide

A

4-Chlorobenzenesulfonamide
98-64-6

4-Chlorobenzenesulfonamide

B

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With sodium hydroxide at 20℃; for 0.5h; Product distribution;
N-(2,2,2-trichloro-1-benzenesulfonamidoethyl)benzenesulfonamide
85095-84-7

N-(2,2,2-trichloro-1-benzenesulfonamidoethyl)benzenesulfonamide

A

benzenesulfonamide
98-10-2

benzenesulfonamide

B

chloral hydrate
302-17-0

chloral hydrate

Conditions
ConditionsYield
With sodium hydroxide at 20℃; for 0.5h; Product distribution;
L-alanin
56-41-7

L-alanin

A

α-picoline
109-06-8

α-picoline

B

chloral hydrate
302-17-0

chloral hydrate

C

2-ethylideneamino propanoic acid

2-ethylideneamino propanoic acid

D

cyclo(-DL-Ala-DL-Ala-)
5625-46-7

cyclo(-DL-Ala-DL-Ala-)

Conditions
ConditionsYield
With copper dichloride at 250℃; for 0.00555556h; Pyrolysis; Inert atmosphere;

A

α-picoline
109-06-8

α-picoline

B

chloral hydrate
302-17-0

chloral hydrate

C

2-ethylideneamino propanoic acid

2-ethylideneamino propanoic acid

D

cyclo(-DL-Ala-DL-Ala-)
5625-46-7

cyclo(-DL-Ala-DL-Ala-)

Conditions
ConditionsYield
at 250℃; for 0.00555556h; Pyrolysis; Inert atmosphere;
(2S)-2-(6-methoxy(2-naphthyl))propanoic acid
22204-53-1

(2S)-2-(6-methoxy(2-naphthyl))propanoic acid

A

chloral hydrate
302-17-0

chloral hydrate

B

chloroform
67-66-3

chloroform

C

1,1-Dichloroacetone
513-88-2

1,1-Dichloroacetone

D

1,1,1-trichloroacetone
918-00-3

1,1,1-trichloroacetone

Conditions
ConditionsYield
With chlorine In aq. phosphate buffer pH=7; Kinetics; pH-value; UV-irradiation;
chloral hydrate
302-17-0

chloral hydrate

1,1-dimethylethylurea
1118-12-3

1,1-dimethylethylurea

N-tert-butyl-N'-(2,2,2-trichloro-1-hydroxyethyl)urea
96010-48-9

N-tert-butyl-N'-(2,2,2-trichloro-1-hydroxyethyl)urea

Conditions
ConditionsYield
With hydrogenchloride In water for 15h;100%
chloral hydrate
302-17-0

chloral hydrate

1-[2-(3,4-Dichloro-phenyl)-ethyl]-[1,4]diazepane
150208-33-6

1-[2-(3,4-Dichloro-phenyl)-ethyl]-[1,4]diazepane

1-<2-(3,4-dichlorophenyl)ethyl>-4-formylhomopiperazine
150208-82-5

1-<2-(3,4-dichlorophenyl)ethyl>-4-formylhomopiperazine

Conditions
ConditionsYield
In toluene at 90℃; for 1.5h;100%
chloral hydrate
302-17-0

chloral hydrate

4-propylaniline
2696-84-6

4-propylaniline

5-Propylisatin
131609-60-4

5-Propylisatin

Conditions
ConditionsYield
Stage #1: chloral hydrate; 4-propylaniline With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In water for 0.0166667h; Reflux;
Stage #2: With sulfuric acid at 50 - 80℃;
100%
chloral hydrate
302-17-0

chloral hydrate

ethyl 1-(4-aminophenyl)cyclobutanecarboxylate hydrochloride

ethyl 1-(4-aminophenyl)cyclobutanecarboxylate hydrochloride

ethyl 2-[4-[[2-hydroxyiminoacetyl]amino]phenyl]cyclobutanecarboxylate
1309089-16-4

ethyl 2-[4-[[2-hydroxyiminoacetyl]amino]phenyl]cyclobutanecarboxylate

Conditions
ConditionsYield
Stage #1: chloral hydrate With sodium sulfate In water at 23℃; for 0.166667h;
Stage #2: ethyl 1-(4-aminophenyl)cyclobutanecarboxylate hydrochloride With hydroxylamine hydrochloride In water at 60℃; for 5h;
100%
chloral hydrate
302-17-0

chloral hydrate

3-bromo-2-methylaniline
55289-36-6

3-bromo-2-methylaniline

6-bromo-7-methyl-1H-indole-2,3-dione
129833-54-1

6-bromo-7-methyl-1H-indole-2,3-dione

Conditions
ConditionsYield
Stage #1: chloral hydrate; 3-bromo-2-methylaniline With hydrogenchloride; water; sodium sulfate at 20℃;
Stage #2: With hydroxylamine hydrochloride Reflux;
100%
Stage #1: chloral hydrate; 3-bromo-2-methylaniline With hydrogenchloride; sodium sulfate In water at 20℃;
Stage #2: With hydroxylamine hydrochloride In water Reflux;
100%
chloral hydrate
302-17-0

chloral hydrate

4-fluor-2-methylaniline
452-71-1

4-fluor-2-methylaniline

(2E)-N-(4-fluoro-2-methylphenyl)-2-(N-hydroxyimino)acetamide

(2E)-N-(4-fluoro-2-methylphenyl)-2-(N-hydroxyimino)acetamide

Conditions
ConditionsYield
Stage #1: chloral hydrate; 4-fluor-2-methylaniline With hydrogenchloride; sodium sulfate In water at 20℃;
Stage #2: With hydroxylamine hydrochloride In water Reflux;
100%
With hydroxylamine hydrochloride at 80℃; for 1h;47%
chloral hydrate
302-17-0

chloral hydrate

3-bromo-2-methylaniline
55289-36-6

3-bromo-2-methylaniline

(2E)-N-(3-bromo-2-methyl-phenyl)-2-hydroxyimino-acetamide

(2E)-N-(3-bromo-2-methyl-phenyl)-2-hydroxyimino-acetamide

Conditions
ConditionsYield
Stage #1: chloral hydrate; 3-bromo-2-methylaniline With hydrogenchloride; sodium sulfate In water at 20℃;
Stage #2: With hydroxylamine hydrochloride In water Reflux;
100%
chloral hydrate
302-17-0

chloral hydrate

chloral
75-87-6

chloral

Conditions
ConditionsYield
With phosphorus pentoxide; sulfuric acid99%
With diethyl ether; water; chlorine at 80℃;
With sulfuric acid
chloral hydrate
302-17-0

chloral hydrate

(S)-Malic acid
97-67-6

(S)-Malic acid

(2RS,5S)-5-carboxymethyl-2-trichloromethyl-4-oxo-1,3-dioxolane
196512-77-3

(2RS,5S)-5-carboxymethyl-2-trichloromethyl-4-oxo-1,3-dioxolane

Conditions
ConditionsYield
With sulfuric acid for 10h; Ambient temperature;99%
With sulfuric acid at 20℃; for 3h;93%
With sulfuric acid at 20℃; for 3h; Inert atmosphere;93%
In sulfuric acid at 0 - 20℃;52%
3-bromo-2-fluorobenzenamine
58534-95-5

3-bromo-2-fluorobenzenamine

chloral hydrate
302-17-0

chloral hydrate

N-(3-bromo-2-fluorophenyl)-2-(hydroxyimino)acetamide
1336963-99-5

N-(3-bromo-2-fluorophenyl)-2-(hydroxyimino)acetamide

Conditions
ConditionsYield
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In water at 55 - 90℃; for 3h;99%
Stage #1: 3-bromo-2-fluorobenzenamine; chloral hydrate With hydrogenchloride; sodium sulfate In water at 35℃;
Stage #2: With hydroxylamine hydrochloride at 90℃; for 16h;
61%
Stage #1: chloral hydrate With sodium sulfate In water at 35℃;
Stage #2: 3-bromo-2-fluorobenzenamine With hydrogenchloride; hydroxylamine hydrochloride In water at 90℃; for 16h;
61%
chloral hydrate
302-17-0

chloral hydrate

ethyl 3,5-dimethoxybenzoate
17275-82-0

ethyl 3,5-dimethoxybenzoate

4,6-dimethoxy-3-trichloromethyl-1-benzo[c]furanone
63585-71-7

4,6-dimethoxy-3-trichloromethyl-1-benzo[c]furanone

Conditions
ConditionsYield
With sulfuric acid for 4h;98%
With sulfuric acid
chloral hydrate
302-17-0

chloral hydrate

Propionamid
79-05-0

Propionamid

N-(2,2,2-trichloro-1-hydroxyethyl)propionamide
34243-50-0

N-(2,2,2-trichloro-1-hydroxyethyl)propionamide

Conditions
ConditionsYield
at 90 - 100℃;98%
chloral hydrate
302-17-0

chloral hydrate

Phenyl-phosphonic acid bis-(2,2,3,3,4,4,5,5-octafluoro-pentyl) ester
17792-50-6

Phenyl-phosphonic acid bis-(2,2,3,3,4,4,5,5-octafluoro-pentyl) ester

Phenyl-(2,2,2-trichloro-1-hydroxy-ethyl)-phosphinic acid 2,2,3,3,4,4,5,5-octafluoro-pentyl ester
122348-12-3

Phenyl-(2,2,2-trichloro-1-hydroxy-ethyl)-phosphinic acid 2,2,3,3,4,4,5,5-octafluoro-pentyl ester

Conditions
ConditionsYield
In benzene temp. not higher than 40 deg C;98%
chloral hydrate
302-17-0

chloral hydrate

Phenyl-phosphonic acid bis-(2,2,2-trifluoro-ethyl) ester
172422-37-6

Phenyl-phosphonic acid bis-(2,2,2-trifluoro-ethyl) ester

Phenyl-(2,2,2-trichloro-1-hydroxy-ethyl)-phosphinic acid 2,2,2-trifluoro-ethyl ester
122348-13-4

Phenyl-(2,2,2-trichloro-1-hydroxy-ethyl)-phosphinic acid 2,2,2-trifluoro-ethyl ester

Conditions
ConditionsYield
In benzene temp. not higher than 40 deg C;98%
chloral hydrate
302-17-0

chloral hydrate

2-(4-amino-phenyl)-2-methyl-propionic acid ethyl ester; hydrochloride

2-(4-amino-phenyl)-2-methyl-propionic acid ethyl ester; hydrochloride

ethyl 2-[4-[[(2E)-2-hydroxyiminoacetyl]amino]phenyl]-2-methylpropanoate
1309089-22-2

ethyl 2-[4-[[(2E)-2-hydroxyiminoacetyl]amino]phenyl]-2-methylpropanoate

Conditions
ConditionsYield
Stage #1: chloral hydrate With sodium sulfate In water at 23℃; for 0.166667h;
Stage #2: 2-(4-amino-phenyl)-2-methyl-propionic acid ethyl ester; hydrochloride With hydroxylamine hydrochloride In water at 60℃; for 5h;
98%
chloral hydrate
302-17-0

chloral hydrate

3-Methoxybenzoic acid
586-38-9

3-Methoxybenzoic acid

6-methoxy-3-(trichloromethyl)isobenzofuran-1(3H)-one
82735-28-2

6-methoxy-3-(trichloromethyl)isobenzofuran-1(3H)-one

Conditions
ConditionsYield
With sulfuric acid at 20℃; for 12h;97%
With sulfuric acid at 20℃; for 12h;83.6%
With sulfuric acid at 20℃; for 24h;63%
chloral hydrate
302-17-0

chloral hydrate

N-Methylurea
598-50-5

N-Methylurea

N-methyl-N'-(2,2,2-trichloro-1-hydroxyethyl)urea
1954-79-6

N-methyl-N'-(2,2,2-trichloro-1-hydroxyethyl)urea

Conditions
ConditionsYield
In water for 48h; Substitution;97%
With water
chloral hydrate
302-17-0

chloral hydrate

N,N'-Dimethylurea
96-31-1

N,N'-Dimethylurea

1-methyl-1-(1-hydroxy-2,2,2-trichloroethyl)-3-methyl urea

1-methyl-1-(1-hydroxy-2,2,2-trichloroethyl)-3-methyl urea

Conditions
ConditionsYield
With 3 A molecular sieve In 1,4-dioxane at 70℃; for 168h; Substitution;97%
chloral hydrate
302-17-0

chloral hydrate

2-iodo-[15N]aniline

2-iodo-[15N]aniline

C8H7IN(15)NO2

C8H7IN(15)NO2

Conditions
ConditionsYield
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate at 90℃;97%
chloral hydrate
302-17-0

chloral hydrate

chloral hydrate sodium salt

chloral hydrate sodium salt

Conditions
ConditionsYield
With sodium hydride In diethyl ether for 3h;97%
chloral hydrate
302-17-0

chloral hydrate

3-methyl-4-chloroaniline
7149-75-9

3-methyl-4-chloroaniline

N-(4-chloro-3-methylphenyl)-2-(hydroxyimino)acetamide
637347-65-0

N-(4-chloro-3-methylphenyl)-2-(hydroxyimino)acetamide

Conditions
ConditionsYield
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In water at 100℃; for 1h;97%
chloral hydrate
302-17-0

chloral hydrate

3-chloro-5-fluoroaniline hydrochloride
940054-43-3

3-chloro-5-fluoroaniline hydrochloride

N-(3-chloro-5-fluorophenyl)-2-hydroxyimino-acetamide
940054-44-4

N-(3-chloro-5-fluorophenyl)-2-hydroxyimino-acetamide

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium sulfate In water at 20℃; for 16.6667h; Heating / reflux;97%
chloral hydrate
302-17-0

chloral hydrate

C14H9F14O2P

C14H9F14O2P

A

2,2,3,3,4,4,4-heptafluorobutanol
375-01-9

2,2,3,3,4,4,4-heptafluorobutanol

B

C12H9Cl3F7O3P
1235818-81-1

C12H9Cl3F7O3P

Conditions
ConditionsYield
In benzene at 30 - 40℃; Abramov reaction; Inert atmosphere;A n/a
B 97%
chloral hydrate
302-17-0

chloral hydrate

2-fluoroaniline hydrochloride
51085-49-5

2-fluoroaniline hydrochloride

N-(2-fluorophenyl)-2-(hydroxyimino)acetamide
349-24-6

N-(2-fluorophenyl)-2-(hydroxyimino)acetamide

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium sulfate In water for 0.166667h; Reflux;97%
2-Fluoroaniline
348-54-9

2-Fluoroaniline

chloral hydrate
302-17-0

chloral hydrate

N-(2-Fluorophenyl)-2-hydroxyiminoacetamide
349-24-6

N-(2-Fluorophenyl)-2-hydroxyiminoacetamide

Conditions
ConditionsYield
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In water for 0.166667h; Heating;96%
With hydrogenchloride; hydroxylamine; sodium sulfate
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate at 80 - 90℃; for 2h;
Stage #1: 2-Fluoroaniline; chloral hydrate With hydrogenchloride; sodium sulfate In water at 20℃; for 5h;
Stage #2: With hydroxylamine hydrochloride In water at 60℃; for 1h;
chloral hydrate
302-17-0

chloral hydrate

malic acid
617-48-1

malic acid

Chloralide of malic acid
5050-56-6

Chloralide of malic acid

Conditions
ConditionsYield
With sulfuric acid96%
With sulfuric acid at 20℃; -chloralide;
chloral hydrate
302-17-0

chloral hydrate

benzamide
55-21-0

benzamide

N-(2,2,2-trichloro-1-hydroxyethyl)benzamide
6316-07-0

N-(2,2,2-trichloro-1-hydroxyethyl)benzamide

Conditions
ConditionsYield
at 90 - 100℃;96%
Heating;
chloral hydrate
302-17-0

chloral hydrate

C20H11F24O2P

C20H11F24O2P

A

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol
335-99-9

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol

B

1H,1H,7H-perfluoroheptyl 1-hydroxy-2,2,2-trichloroethyl(phenyl)phosphinate

1H,1H,7H-perfluoroheptyl 1-hydroxy-2,2,2-trichloroethyl(phenyl)phosphinate

Conditions
ConditionsYield
In benzene at 30 - 40℃; Abramov reaction; Inert atmosphere;A n/a
B 96%
5-bromo-3-fluoro-2-methoxyaniline
239122-51-1

5-bromo-3-fluoro-2-methoxyaniline

chloral hydrate
302-17-0

chloral hydrate

N-(5-bromo-3-fluoro-2-methoxy-phenyl)-2-[(E)-hydroxyimino]-acetamide
1616831-12-9

N-(5-bromo-3-fluoro-2-methoxy-phenyl)-2-[(E)-hydroxyimino]-acetamide

Conditions
ConditionsYield
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate In 1,4-dioxane; water at 50 - 70℃; for 15h;96%
chloral hydrate
302-17-0

chloral hydrate

1,3-Dimethoxybenzene
151-10-0

1,3-Dimethoxybenzene

1,1,1-trichloro-2,2-bis(2,4-dimethoxyphenyl)ethane
138002-56-9

1,1,1-trichloro-2,2-bis(2,4-dimethoxyphenyl)ethane

Conditions
ConditionsYield
95%
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