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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:2,2,3,3,4,4,4-Heptafluoro-1-butanol CA
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1-Butanol,2,2,3,3,4,4,4-heptafluoro- cas 375-01-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryConditions | Yield |
---|---|
With carbonylchlorohydrido[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen; sodium methylate In methanol at 40℃; under 7500.75 Torr; for 23h; Temperature; Autoclave; | 99% |
With copper oxide-chromium oxide at 210 - 230℃; under 73550.8 - 132391 Torr; Hydrogenation; | |
With sodium tetrahydroborate; sulfuric acid In methanol; water | |
In sodium tetrahydroborate |
Conditions | Yield |
---|---|
In benzene at 30 - 40℃; Abramov reaction; Inert atmosphere; | A n/a B 97% |
Conditions | Yield |
---|---|
With RuCl2(DPPEA)(±DAIPEN); hydrogen; sodium methylate In isopropyl alcohol at 80℃; under 750.075 - 15001.5 Torr; for 30h; Autoclave; | 92% |
formaldehyd
(heptafluoro n-propyl) magnesiumiodide
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
In further solvent(s) reaction in n-butyl ether at -25°C, 11 hours;; | 42% |
In further solvent(s) reaction in n-butyl ether at -25°C, 11 hours;; | 42% |
ethylmagnesium iodide
2,2,3,3,4,4,4-heptafluorobutanal
diethyl ether
A
2,2,3,3,4,4,4-heptafluorobutanol
B
(perfluor n-propyl) ethyl methanol
ethylmagnesium iodide
2,2,3,3,4,4,4-heptafluorobutanal
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
With diethyl ether |
heptafluorobutyric Acid
heptafluorobutyryl chloride
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether | |
With lithium aluminium tetrahydride; diethyl ether |
Conditions | Yield |
---|---|
With rhenium; water at 190℃; under 220652 Torr; Hydrogenation; |
heptafluorobutyric Acid
A
2,2,3,3,4,4,4-heptafluorobutanol
B
heptafluoro-butyric acid-(1H,1H-heptafluoro-butyl ester)
Conditions | Yield |
---|---|
With rhenium at 190℃; under 220652 Torr; Hydrogenation; |
heptafluorobutyryl chloride
A
2,2,3,3,4,4,4-heptafluorobutanol
B
2,2,3,3,4,4,4-heptafluoro-butane-1,1-diol
Conditions | Yield |
---|---|
With palladium on activated charcoal; diethyl ether Hydrogenation.an mit Chinolin und Schwefel desaktiviertem Palladium/Kohle; bei anschliessenden Behandlung mit Wasser; |
2,2,2-trifluoroethanol
A
2,2,3,3,4,4,4-heptafluorobutanol
B
(2,2,2-trifluoroethoxy)dimethylphenylsilane
Conditions | Yield |
---|---|
With potassium 2,2,2-trifluoroethoxide at 30℃; Rate constant; μ = 0.05 M with potassium trifluoroacetate; |
Conditions | Yield |
---|---|
With Na2CO3 buffer; sodium hydrogencarbonate In acetonitrile at 30℃; Rate constant; μ = 0.06 M (NaCl); |
Conditions | Yield |
---|---|
With dibutyl ether |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 0℃; |
methyl heptafluorobutyrate
A
1H-heptafluoro-1-methoxy-butan-1-ol
B
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
Stage #1: methyl heptafluorobutyrate With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In methanol Inert atmosphere; Glovebox; Stage #2: With hydrogen In methanol at 40℃; under 18751.9 Torr; for 24h; Catalytic behavior; Reagent/catalyst; Autoclave; Sealed tube; | A 60 %Spectr. B 35 %Chromat. |
With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)-amino]ruthenium(II); potassium tert-butylate; hydrogen In methanol at 40℃; under 18751.9 Torr; for 24h; Reagent/catalyst; |
Conditions | Yield |
---|---|
With sodium hydroxide In dimethyl sulfoxide at 60℃; for 4h; | 96.1% |
Conditions | Yield |
---|---|
With potassium tert-butylate In neat (no solvent) at 20℃; for 0.333333h; Michael Addition; Inert atmosphere; | 96% |
chloro-trimethyl-silane
2,2,3,3,4,4,4-heptafluorobutanol
2,2,3,3,4,4,4-heptafluorobutoxy trimethylsilane
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole In m-xylene Heating; | 95.2% |
With pyridine In dibutyl ether |
Conditions | Yield |
---|---|
With phosphoric acid In acetonitrile at 50℃; for 5h; | 94% |
Conditions | Yield |
---|---|
With lithium chloride; trichlorophosphate for 3.6h; bath temperature 160 deg C; | 93.8% |
With lithium chloride; trichlorophosphate at 160℃; for 3.6h; Product distribution; Further Variations:; Reagents; reaction time; | 93.8% |
With trichlorophosphate; bromoethane triphenylphosphine salt In ethanol for 6.9h; Heating; | 92.5% |
Conditions | Yield |
---|---|
at 20 - 25℃; | 93% |
4-toluenesulfonyl azide
2,2,3,3,4,4,4-heptafluorobutanol
4-n-methylphenylacetylene
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine In tetrahydrofuran at 20℃; for 10h; | 92% |
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine In tetrahydrofuran at 20℃; for 10h; | 91% |
Conditions | Yield |
---|---|
With diethylamino-sulfur trifluoride; triethylamine In dichloromethane at 20℃; for 16h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
Stage #1: C34H29BF12N2O2 With aluminum (III) chloride In dichloromethane at 0℃; for 2h; Inert atmosphere; Reflux; Stage #2: 2,2,3,3,4,4,4-heptafluorobutanol In dichloromethane for 5h; Inert atmosphere; Reflux; | 88% |
2,2,3,3,4,4,4-heptafluorobutanol
dimethyl 4-nitrophthalate
dimethyl 4-(2,2,3,3,4,4,4-heptafluorobutoxy)phthalate
Conditions | Yield |
---|---|
Stage #1: 2,2,3,3,4,4,4-heptafluorobutanol With sodium hydride In N,N-dimethyl-formamide at 20℃; Stage #2: dimethyl 4-nitrophthalate In N,N-dimethyl-formamide at 20℃; | 87% |
Conditions | Yield |
---|---|
With sodium carbonate In dichloromethane at 20℃; for 24h; | 87% |
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
Stage #1: 2,2,3,3,4,4,4-heptafluorobutanol With pyridine; di(succinimido) carbonate In N,N-dimethyl-formamide at 40℃; for 15h; Stage #2: Nα-(tert-butyloxycarbonyl)-(R)-lysine tert-butyl ester In N,N-dimethyl-formamide at 20 - 30℃; | 87% |
2,2,3,3,4,4,4-heptafluorobutanol
4,4'-bis(bromomethyl)-2,2'-bipyridine
4,4'-bis(n-C3F7CH2OH2)-2,2'-bpy
Conditions | Yield |
---|---|
Stage #1: 2,2,3,3,4,4,4-heptafluorobutanol With methanol; sodium methylate at 80℃; for 4h; Inert atmosphere; Stage #2: 4,4'-bis(bromomethyl)-2,2'-bipyridine In tetrahydrofuran Reflux; | 86.2% |
Stage #1: 2,2,3,3,4,4,4-heptafluorobutanol With sodium methylate In methanol Stage #2: 4,4'-bis(bromomethyl)-2,2'-bipyridine |
2,2,3,3,4,4,4-heptafluorobutanol
Nonafluorobutanesulfonyl fluoride
2,2,3,3,4,4,4-heptafluorobutyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
Conditions | Yield |
---|---|
With potassium hydroxide In water at 0 - 15℃; for 22h; | 86% |
With potassium hydroxide In water at 20 - 35℃; | |
With sodium hydroxide In water at 20 - 35℃; for 16h; Temperature; | 461 mg |
2,2,3,3,4,4,4-heptafluorobutanol
epichlorohydrin
1,3-bis(2,2,3,3,4,4,4-heptafluorobutoxy)-2-propanol
Conditions | Yield |
---|---|
With potassium hydroxide In water at 30 - 70℃; for 15h; | 86% |
With potassium carbonate at 70℃; for 2h; |
2,2,3,3,4,4,4-heptafluorobutanol
dec-9-en-1-yl methanesulfonate
Conditions | Yield |
---|---|
Stage #1: 2,2,3,3,4,4,4-heptafluorobutanol With sodium hydride In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; Stage #2: dec-9-en-1-yl methanesulfonate In tetrahydrofuran for 24h; Reflux; Inert atmosphere; | 86% |
Stage #1: 2,2,3,3,4,4,4-heptafluorobutanol With sodium hydride In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; Stage #2: dec-9-en-1-yl methanesulfonate In tetrahydrofuran for 24h; Reflux; Inert atmosphere; | 86% |
2,2,3,3,4,4,4-heptafluorobutanol
dec-9-en-1-yl methanesulfonate
Conditions | Yield |
---|---|
Stage #1: 2,2,3,3,4,4,4-heptafluorobutanol With sodium hydride In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; Stage #2: dec-9-en-1-yl methanesulfonate In tetrahydrofuran for 24h; Reflux; | 86% |
2,2,3,3,4,4,4-heptafluorobutanol
N-(11-undecanoic acid)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide
N-(2,2,3,3,4,4,4-heptafluorobutyl 11-undecanoate)-N’,N”-di(n-decyl)benzene-1,3,5-tricarboxamide
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-(dimethylamino)pyridinium tosylate In chloroform for 48h; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With potassium hydride In toluene at 20℃; for 22h; Inert atmosphere; Cooling with ice; | 85% |
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
With potassium hydride In toluene at 20℃; for 20h; Inert atmosphere; Cooling with ice; | 84% |
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 0 - 20℃; for 1.08333h; Schlenk technique; Inert atmosphere; | 83% |
P,P'-methanediyl-bis-phosphonic acid tetrachloride
2,2,3,3,4,4,4-heptafluorobutanol
Conditions | Yield |
---|---|
With 1H-tetrazole; N-ethyl-N,N-diisopropylamine In toluene at 20℃; | 82% |
phosgene
2,2,3,3,4,4,4-heptafluorobutanol
2,2,3,3,4,4,4-heptafluorobutyl chloroformate
Conditions | Yield |
---|---|
With amine In diethyl ether at 4 - 20℃; for 3.75h; | 82% |
2,2,3,3,4,4,4-heptafluorobutanol
1-methyl-6-bromoquinoxaline-2(1H)-one
Conditions | Yield |
---|---|
With bis-[(trifluoroacetoxy)iodo]benzene In chloroform at 25℃; for 2h; | 82% |
With bis-[(trifluoroacetoxy)iodo]benzene In neat (no solvent) at 35℃; for 1h; | 70% |
2,2,3,3,4,4,4-heptafluorobutanol
Trifluoromethanesulfonyl fluoride
triethylamine
A
2,2,3,3,4,4,4-heptafluorobutyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
In dichloromethane | A 81% B n/a |
In dichloromethane | A 81% B n/a |
In dichloromethane | |
In dichloromethane | |
In dichloromethane |
2,2,3,3,4,4,4-heptafluorobutanol
methanesulfonyl chloride
2,2,3,3,4,4,4-heptafluorobutyl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In chloroform for 6h; Ambient temperature; | 80% |
With sodium carbonate at 20℃; for 20h; | 76% |
With pyridine |
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