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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Triethylborane

Cas:97-94-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Triethyl Borane supplier in China

Cas:97-94-9

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Triethylborane

Cas:97-94-9

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Triethylborane

Cas:97-94-9

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

97-94-9 Triethylborane

Cas:97-94-9

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

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Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta

high quality 97-94-9 Triethylborane with best price

Cas:97-94-9

Min.Order:10 Gram

Negotiable

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:97-94-9

Cas:97-94-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Fandachem Co.,Ltd

Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Triethylborane; TEB CAS:97-94-9 , Please contact us by email freely. We are leading exporter in China. If you really need this cargo

Triethylborane; TEB CAS:97-94-9 from fandachem

Cas:97-94-9

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

afine+triethyl borane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Triethylborane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Triethylborane

Cas:97-94-9

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Triethyl Borane

Cas:97-94-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality Appearance:Clear colourless to light amber solution Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Interm

Triethylborane

Cas:97-94-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Siwei Development Group Ltd.

Product name: Triethyl Borane CAS No.:97-94-9 Molecule Formula:C6H15B Molecule Weight:97.99 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS

Best Quality Triethyl Borane

Cas:97-94-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

High purity Triethylborane

Cas:97-94-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

Triethylborane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Other

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JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

Triethyl Borane

Cas:97-94-9

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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DB BIOTECH CO., LTD

Q1: Are you a manufacturer Answer: Yes, we are factory founded on 2012.Q2: How to contact with us Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours.Q3:Which kind of payment terms do you

Triethylborane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Trading Company

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Triethylborane (ca. 11% in Tetrahydrofuran, ca. 1Mol/L)

Cas:97-94-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Triethyl Borane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory directly supply CAS 97-94-9 with competitive price

Cas:97-94-9

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Triethylborane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

Triethyl borane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Other

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

Name Triethylborane Molecular Structure Molecular Formula C6H15B Molecular Weight 97.99

Triethylborane

Cas:97-94-9

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

TIANFU-CHEM - TriethylboraneAppearance:Solid Storage:In Room Temperature Package:IN 25kg drums Application:Organic synthesis Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/

TIANFU-CHEM - Triethylborane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Koning Pharmchem Co., Ltd.

Triethylborane Application:97-94-9

Triethylborane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Trading Company

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Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

Triethylborane

Cas:97-94-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Beantown Chemical

in stock Application:97-94-9

Triethylborane solution, 1M in THF

Cas:97-94-9

Min.Order:0

Negotiable

Type:Trading Company

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HWRK Chem

in store Package:100ml Application:Organic Chemicals

Triethylborane (ca. 11% in Tetrahydrofuran, ca. 1mol/L)

Cas:97-94-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

triethylborane

Cas:97-94-9

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

ethyl bromide
74-96-4

ethyl bromide

trifluoroborane diethyl ether
109-63-7

trifluoroborane diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
With magnesium In diethyl ether byproducts: MgFBr, EtMgBr; react. of EtBr, Mg turnings, and BF3*Et2O (in 3.5:3.5:1 molar ratio) in Et2O for 2 h; not isolated; detected by NMR;100%
tetraethyldiborane

tetraethyldiborane

(phenylamino)diethylborane
22093-18-1

(phenylamino)diethylborane

A

1-phenyl-2,5-diethyl-1,2,5-azadiborolane
96080-50-1

1-phenyl-2,5-diethyl-1,2,5-azadiborolane

B

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
byproducts: hydrogene; High Pressure; 180°C 16 h and 200°C 9 h in autoclave shaking at 50 atm then 210-225°C 2 h; distn.;A 97.6%
B n/a
byproducts: hydrogene; High Pressure; 180°C 16 h and 200°C 9 h in autoclave shaking at 50 atm then 210-225°C 2 h; distn.;A 97.6%
B n/a
tetraethyldiboroxane
158817-73-3

tetraethyldiboroxane

A

bis(diethylboryl)sulfate
158817-74-4

bis(diethylboryl)sulfate

B

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
With SO3 In (2)H8-toluene under Ar, addn. of SO3 in (d8)-toluene to B-compd. in (d8)-toluene at 0°C, warmed to room temp.; detn. by (17)O-NMR;A 95%
B 5%
ethyl bromide
74-96-4

ethyl bromide

triethyl borate
150-46-9

triethyl borate

aluminium
7429-90-5

aluminium

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; N2; molar ratio EtBr:B(OEt)3:Al = 4.5:1:3.3, ultrasound treatment of EtBr and Al (-20°C), addn. of B(OEt)3 (room temp., during 10 min); distn.;91.4%
With iodine In neat (no solvent) Sonication; N2; molar ratio EtBr:B(OEt)3:Al:I2 = 0.65:0.166:0.476:0.0025, ultrasound treatment of EtBr, Al and I2 (-20°C), addn. of B(OEt)3 (room temp., during 10 min); distn.;90%
With iodine In neat (no solvent) Sonication; N2; molar ratio EtBr:B(OEt)3:Al:I2 = 0.65:0.166:0.476:0.005, ultrasoundtreatment of EtBr, Al and I2 (-20°C), addn. of B(OEt)3 (room temp., during 10 min); distn.;90.3%
sulfur
10544-50-0

sulfur

sodium triethylborohydride

sodium triethylborohydride

A

sodium sulfide

sodium sulfide

B

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In toluene byproducts: H2; Ar atmosphere, stirring (80-90°C, 8 h); washing (pentane), drying (0.1 Torr);A 91%
B n/a
ethene
74-85-1

ethene

diborane
19287-45-7

diborane

A

triethyl borane
97-94-9

triethyl borane

B

boron hydride
13766-26-2

boron hydride

Conditions
ConditionsYield
In neat (no solvent) byproducts: H2; Irradiation (UV/VIS); react. of B2H6 with C2H4 (1:12) at 320 Torr and irradiation with cw CO2laser for 2 s;A 91%
B n/a
In neat (no solvent) byproducts: H2; Irradiation (UV/VIS); react. B2H6 with C2H4 (1:9) at 320 Torr and irradiation with cw CO2 laser for 2 s;A 56%
B n/a
In neat (no solvent) byproducts: H2; Irradiation (UV/VIS); react. B2H6 with C2H4 (1:6) at 160 Torr and irradiation with cw CO2 laser for 2 s;A 34.5%
B n/a
triethyl borate
150-46-9

triethyl borate

triethyl-alane; compound with diethyl ether
13824-25-4, 14002-28-9

triethyl-alane; compound with diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al*Et2O introduced into a flask connected to a condenser containing alcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further20 min; distd.; gas chromy.;90%
N,N′-di-tertbutyl(phenylamidinato)chlorosilylene

N,N′-di-tertbutyl(phenylamidinato)chlorosilylene

[(1,2-bis(dimethylphosphine)ethane)2(PMe3)Fe]
1430654-19-5

[(1,2-bis(dimethylphosphine)ethane)2(PMe3)Fe]

A

triethyl borane
97-94-9

triethyl borane

C27H56FeN2P4Si
1430654-22-0

C27H56FeN2P4Si

Conditions
ConditionsYield
Stage #1: N,N′-di-tertbutyl(phenylamidinato)chlorosilylene; [(1,2-bis(dimethylphosphine)ethane)2(PMe3)Fe] In diethyl ether at -30 - 20℃; for 2h; Schlenk technique;
Stage #2: With lithium triethylborohydride at 0 - 20℃; for 3.33333h; Schlenk technique;
A n/a
B 89%
tetraethyldiborane(6)
12081-54-8

tetraethyldiborane(6)

indole
120-72-9

indole

A

(indolyl)diethylborane
28916-09-8

(indolyl)diethylborane

B

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
byproducts: H2; 90°C;A 87%
B n/a
diethylboron bromide
19162-10-8

diethylboron bromide

P-methyl-N,N'-bis(tert-butyl)diamidothiophosphonate
97536-05-5

P-methyl-N,N'-bis(tert-butyl)diamidothiophosphonate

A

triethyl borane
97-94-9

triethyl borane

B

1,3-di-tert-butyl-4-ethyl-2-methyl-1,3,2,4-diazaphosphaboretidine-2-sulfide
62948-90-7

1,3-di-tert-butyl-4-ethyl-2-methyl-1,3,2,4-diazaphosphaboretidine-2-sulfide

Conditions
ConditionsYield
With n-butyllithium In hexane N2 atmosphere; lithiation of amine with n-BuLi/hexane; refluxed for 20 h; addn. of a soln. of B compd. in hexane at -40°; slow warming to room temp.; filtration; fractional distn.; heating at 140°C for3 h in N2 stream with condensation;; fractional distn.; elem. anal.;;A 85%
B 82%
bis[tert-butyl(diethylboryl)amino]methylphosphanoxide
97536-02-2

bis[tert-butyl(diethylboryl)amino]methylphosphanoxide

A

1,3-di-tert-butyl-4-ethyl-2-methyl-1,3,2,4-diazaphosphaboretidine-2-oxide
97536-01-1

1,3-di-tert-butyl-4-ethyl-2-methyl-1,3,2,4-diazaphosphaboretidine-2-oxide

B

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) heating at 170-190°C for 5 h in a stream of N2; condensation of volatiles in a cool trap;; distn.; elem. anal.;;A 55%
B 85%
diethylboron bromide
19162-10-8

diethylboron bromide

1,2-bis(trimethylstannyl)benzene
14275-62-8

1,2-bis(trimethylstannyl)benzene

A

triethyl borane
97-94-9

triethyl borane

B

1,2-bis(diethylboryl)benzene
208246-80-4

1,2-bis(diethylboryl)benzene

Conditions
ConditionsYield
In pentane byproducts: (CH3)3SnBr; inert atmosphere, addn. of soln. of stannyl compound to refluxing soln. of Et2BBr, reflux ( 1 h); removement of volatiles (vacuum), addn. (pentane), pptn. (-78°C),filtration of (CH3)3SnBr (-78°C), removement of solvent (vacuum) , distillation;A n/a
B 84%
boric acid tributyl ester
688-74-4

boric acid tributyl ester

triethylaluminum
97-93-8

triethylaluminum

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al introduced into a flask connected to a condenser containingalcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further 20 min; distd.; gas chromy.;82.3%
tri-n-propyl borate
688-71-1

tri-n-propyl borate

triethyl-alane; compound with diethyl ether
13824-25-4, 14002-28-9

triethyl-alane; compound with diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al*Et2O introduced into a flask connected to a condenser containing alcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further20 min; distd.; gas chromy.;82.1%
tri-n-propyl borate
688-71-1

tri-n-propyl borate

triethylaluminum
97-93-8

triethylaluminum

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al introduced into a flask connected to a condenser containingalcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further 20 min; distd.; gas chromy.;80.1%
ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

trifluoroborane diethyl ether
109-63-7

trifluoroborane diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In diethyl ether at 50-60°C;80%
In diethyl ether at 50-60°C;80%
tetramethoxydiborane
7318-94-7

tetramethoxydiborane

triethylaluminum
97-93-8

triethylaluminum

A

triethyl borane
97-94-9

triethyl borane

B

tetraethyldiborane
21649-17-2

tetraethyldiborane

Conditions
ConditionsYield
In pentane byproducts: (C2H5)2AlOCH3; Al(C2H5)3 added to B2(OMe)4, stirred at -35°C, standing for 2 h at -30°C; solvent evapd. at -10°C bath temp., elem.anal.;A 20%
B 80%
triethyl borate
150-46-9

triethyl borate

triethylaluminum
97-93-8

triethylaluminum

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al introduced into a flask connected to a condenser containingalcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further 20 min; distd.; gas chromy.;78.8%
Triisopropyl borate
5419-55-6

Triisopropyl borate

triethylaluminum
97-93-8

triethylaluminum

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al introduced into a flask connected to a condenser containingalcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further 20 min; distd.; gas chromy.;75.1%
triisobutyl borate
13195-76-1

triisobutyl borate

triethylaluminum
97-93-8

triethylaluminum

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al introduced into a flask connected to a condenser containingalcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further 20 min; distd.; gas chromy.;75.1%
diethylchloroborane
5314-83-0

diethylchloroborane

sodium triethyl-1-propinylborate
14949-99-6

sodium triethyl-1-propinylborate

A

(C2H5)2(CH3)2C4B2(C2H5)2

(C2H5)2(CH3)2C4B2(C2H5)2

B

triethyl borane
97-94-9

triethyl borane

C

tetra-B-ethyl-B,B'-((Z)-1-ethyl-2-methyl-ethene-1,2-diyl)-bis-borane
138517-68-7

tetra-B-ethyl-B,B'-((Z)-1-ethyl-2-methyl-ethene-1,2-diyl)-bis-borane

Conditions
ConditionsYield
In diethyl ether byproducts: NaCl; dropping soln. of 38 mmol ClB(C2H5)2 in 20 ml diethyl ether to soln. of 37 mmol Na-salt in 40 ml diethyl ether within 20 min under Ar, rise in temp., reflux; refluxing for 4 h;; filtration; complete removal of solvent in vac. at <=40°C; distn. in vac.; product mixt. obtained; (11)B NMR spectroscopy; b. p.;;A 11-18
B 7-14
C 75%
In diethyl ether byproducts: NaCl; dropping soln. of 0.5 mol ClB(C2H5)2 in 100 ml diethyl ether to soln. of 0.49 mol Na-salt in 500 ml diethyl ether within 2 h under Ar, rise in temp., boiling; refluxing for 3 h;; filtration; distn. of solvent at atmospheric pressure at <=80°C; removal of remaining ether and B(C2H5)3 in vac. at <=50°C; distn. of residue in vac.; product mixt. obtained; (11)B NMR spectroscopy; b. p.;;A 31-58
B 22-26
C 20-43
Trimethyl borate
121-43-7

Trimethyl borate

triethylaluminum
97-93-8

triethylaluminum

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al introduced into a flask connected to a condenser containingalcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further 20 min; distd.; gas chromy.;74.2%
boric acid tributyl ester
688-74-4

boric acid tributyl ester

triethyl-alane; compound with diethyl ether
13824-25-4, 14002-28-9

triethyl-alane; compound with diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al*Et2O introduced into a flask connected to a condenser containing alcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further20 min; distd.; gas chromy.;69%
triisobutyl borate
13195-76-1

triisobutyl borate

triethyl-alane; compound with diethyl ether
13824-25-4, 14002-28-9

triethyl-alane; compound with diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al*Et2O introduced into a flask connected to a condenser containing alcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further20 min; distd.; gas chromy.;67%
ethyl bromide
74-96-4

ethyl bromide

Trimethyl borate
121-43-7

Trimethyl borate

aluminium
7429-90-5

aluminium

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
With iodine In neat (no solvent) Sonication; N2; ultrasound treatment of EtBr and Al, addn. of B-compd.;65%
Trimethyl borate
121-43-7

Trimethyl borate

triethyl-alane; compound with diethyl ether
13824-25-4, 14002-28-9

triethyl-alane; compound with diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al*Et2O introduced into a flask connected to a condenser containing alcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further20 min; distd.; gas chromy.;65%
triethylboroxine
3043-60-5

triethylboroxine

triethylaluminum
97-93-8

triethylaluminum

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In paraffin Product distribution / selectivity;63.3%
at 70℃; Product distribution / selectivity;44.7%
ethyl bromide
74-96-4

ethyl bromide

boric acid tributyl ester
688-74-4

boric acid tributyl ester

aluminium
7429-90-5

aluminium

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
With iodine In neat (no solvent) Sonication; N2; ultrasound treatment of EtBr and Al, addn. of B-compd.;58.5%
Triisopropyl borate
5419-55-6

Triisopropyl borate

triethyl-alane; compound with diethyl ether
13824-25-4, 14002-28-9

triethyl-alane; compound with diethyl ether

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
In neat (no solvent) Sonication; (N2), Et3Al*Et2O introduced into a flask connected to a condenser containing alcohol at -20°C, stirred and heated to 120°C in an oil bath, added alkyl borate dropwise during 10 min, stirred for further20 min; distd.; gas chromy.;57%
ethyl bromide
74-96-4

ethyl bromide

tri-n-propyl borate
688-71-1

tri-n-propyl borate

aluminium
7429-90-5

aluminium

triethyl borane
97-94-9

triethyl borane

Conditions
ConditionsYield
With iodine In neat (no solvent) Sonication; N2; ultrasound treatment of EtBr and Al, addn. of B-compd.;56.5%
triethyl borane
97-94-9

triethyl borane

N-Cyclohexylcyclododecylidenamin
79014-37-2

N-Cyclohexylcyclododecylidenamin

A

ethane
74-84-0

ethane

B

(Z/E)-(N-Cyclohexyl-1-cyclododecenylamino)diethylboran
74793-30-9

(Z/E)-(N-Cyclohexyl-1-cyclododecenylamino)diethylboran

Conditions
ConditionsYield
With diethylboryl-pivalate at 150℃; for 19h;A 100%
B 96%
With diethylboryl-pivalate at 110℃; for 24h; Product distribution; reactivity of 1h with pure diethyl(pivaloyloxy)borane, different reaction times;A 4.78 mmol
B n/a
triethyl borane
97-94-9

triethyl borane

(E)-1-methoxy-4-(2-nitrovinyl)benzene
3179-10-0, 5576-97-6

(E)-1-methoxy-4-(2-nitrovinyl)benzene

(E)-1-(but-1-en-1-yl)-4-methoxybenzene
18657-09-5

(E)-1-(but-1-en-1-yl)-4-methoxybenzene

Conditions
ConditionsYield
With air In tetrahydrofuran at 20℃;100%
In tetrahydrofuran for 5h; Heating;96%
With air In hexane; acetic acid
In tetrahydrofuran at 20℃; for 0.166667h;
triethyl borane
97-94-9

triethyl borane

1,1'-(2-nitroethene-1,1-diyl)dibenzene
5670-69-9

1,1'-(2-nitroethene-1,1-diyl)dibenzene

1,1-diphenyl-1-butene
1726-14-3

1,1-diphenyl-1-butene

Conditions
ConditionsYield
With (t-BuO)2 In tetrahydrofuran for 3h; Irradiation;100%
triethyl borane
97-94-9

triethyl borane

(E)-2-(4-methylphenyl)-1-nitroethene
101671-00-5

(E)-2-(4-methylphenyl)-1-nitroethene

(E)-1-(but-1-en-1-yl)-4-methylbenzene
54372-77-9, 7642-12-8, 91130-33-5

(E)-1-(but-1-en-1-yl)-4-methylbenzene

Conditions
ConditionsYield
In tetrahydrofuran for 2h; Heating;100%
triethyl borane
97-94-9

triethyl borane

(Z)-1,6-bis(trimethylsilyl)hexa-3-ene-1,5-diyne
92787-97-8

(Z)-1,6-bis(trimethylsilyl)hexa-3-ene-1,5-diyne

Diethyl-((1E,3Z)-1-ethyl-2,6-bis-trimethylsilanyl-hexa-1,3-dien-5-ynyl)-borane

Diethyl-((1E,3Z)-1-ethyl-2,6-bis-trimethylsilanyl-hexa-1,3-dien-5-ynyl)-borane

Conditions
ConditionsYield
at 100℃; for 48h;100%
triethyl borane
97-94-9

triethyl borane

1-[bis(diisopropylamino)boryl]imidazole
675837-54-4

1-[bis(diisopropylamino)boryl]imidazole

1-[bis(diisopropylamino)boryl]imidazole(N3-B)triethylborane

1-[bis(diisopropylamino)boryl]imidazole(N3-B)triethylborane

Conditions
ConditionsYield
In tetrahydrofuran at -78 - 20℃;100%
triethyl borane
97-94-9

triethyl borane

2-methylphenyl aldehyde
529-20-4

2-methylphenyl aldehyde

1-(2-methylphenyl)-1-propanol
61017-92-3

1-(2-methylphenyl)-1-propanol

Conditions
ConditionsYield
With bis(1,5-cyclooctadiene)nickel (0); tri-tert-butyl phosphine; 1-(Prop-2-enyl)-1,2,3,4,5-pentamethylcyclopenta-2,4-dien In hexane; toluene at 0℃;100%
With tri-tert-butyl phosphine; bis(1,5-cyclooctadiene)nickel (0) In tetrahydrofuran; hexane; water at 20℃; for 20h;81%
triethyl borane
97-94-9

triethyl borane

bis(dimethylsilylethynyl)dimethylsilane
123853-91-8

bis(dimethylsilylethynyl)dimethylsilane

4-ethyl-2-diethylboryl-1,1-dimethyl-2,5-bis(dimethylsilyl)-1-sila-2,4-cyclopentadiene

4-ethyl-2-diethylboryl-1,1-dimethyl-2,5-bis(dimethylsilyl)-1-sila-2,4-cyclopentadiene

Conditions
ConditionsYield
at 100℃; for 12h;100%
In neat (no solvent) under Ar; Si compd. added to BEt3, mixt. heated at 100°C for 12 h; volatiles removed under vac.;99%
triethyl borane
97-94-9

triethyl borane

4-methyl-N-(2-oxoethyl)-N-(prop-2-yn-1-yl)benzenesulfonamide
317842-50-5

4-methyl-N-(2-oxoethyl)-N-(prop-2-yn-1-yl)benzenesulfonamide

5-ethyl-1,2,3,6-tetrahydro-1-[(4-methylphenyl)sulfonyl]-pyridin-3-ol

5-ethyl-1,2,3,6-tetrahydro-1-[(4-methylphenyl)sulfonyl]-pyridin-3-ol

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; methanol at 65℃; for 9h;100%
triethyl borane
97-94-9

triethyl borane

(trimethyl)(3-methylbut-3-en-1-ynyl)silane
18387-60-5

(trimethyl)(3-methylbut-3-en-1-ynyl)silane

(Z)-4-(diethylboryl)-2-methyl-3-(trimethylsilyl)-1,3-hexadiene
111869-79-5

(Z)-4-(diethylboryl)-2-methyl-3-(trimethylsilyl)-1,3-hexadiene

Conditions
ConditionsYield
In neat (no solvent) trialkylborane racts with silylalkine at 140°C (24 h) in autoclav;100%
In neat (no solvent) trialkylborane racts with silylalkine for 126 h at 100°C; volatiles are removed, distn. at 0.001 Torr; elem. anal.;58%
triethyl borane
97-94-9

triethyl borane

1-Phenyl-2-(trimethylsilyl)acetylene
2170-06-1

1-Phenyl-2-(trimethylsilyl)acetylene

(E)-2-diethylboryl-1-phenyl-1-trimethylsilyl-1-butene
125212-51-3

(E)-2-diethylboryl-1-phenyl-1-trimethylsilyl-1-butene

Conditions
ConditionsYield
In neat (no solvent) trialkylborane racts with silylalkine at 125°C (16 h) and at 150°C (5 h) in autoclav;100%
In neat (no solvent) trialkylborane racts with silylalkine for 60 h at 100°C; volatiles are removed, distn. at 0.001 Torr; elem. anal.;71%
(η2-2-tert-butyl-1-phosphaacetylene)(trimethylphosphane)zirconocene
126898-91-7

(η2-2-tert-butyl-1-phosphaacetylene)(trimethylphosphane)zirconocene

[Zr(C5H5)2(HCCHPCC(CH3)3)]

[Zr(C5H5)2(HCCHPCC(CH3)3)]

triethyl borane
97-94-9

triethyl borane

[(Zr(C5H5)2)2((CH3)3CCP)2(C2H2)]

[(Zr(C5H5)2)2((CH3)3CCP)2(C2H2)]

Conditions
ConditionsYield
In toluene byproducts: Me3P*BEt3; equimolar mixture; warming (-78 to 20°C);100%
(CH3)2Si(CCSn(CH3)3)(CC)C(CH3)3
153331-55-6

(CH3)2Si(CCSn(CH3)3)(CC)C(CH3)3

triethyl borane
97-94-9

triethyl borane

CB(C2H5)2C(C2H5)C(Sn(CH3)3)Si(CH3)2CC(CH3)3
153331-60-3

CB(C2H5)2C(C2H5)C(Sn(CH3)3)Si(CH3)2CC(CH3)3

Conditions
ConditionsYield
In toluene N2; addn. of 80 mmol BEt3 to a solution of 20 mmol trimethylstannylethinylsilane; stirring for 1 h at room temperature;; removal of the volatiles at 5E-3 Torr;;100%
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