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Cas:97-96-1
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Cas:97-96-1
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Cas:97-96-1
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Cas:97-96-1
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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Cas:97-96-1
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inquiryAt Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
please contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant information Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated place Package:as your needs A
Butanal, 2-ethyl- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
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Cas:97-96-1
Min.Order:20 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1,1-diacetoxy-2-ethyl-butane
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With 2,6-dicarboxypyridinium chlorochromate In acetonitrile at 20℃; for 0.25h; | 96% |
N-(Benzylidene)-2-ethyl-1-butenylamine
A
2-Ethylbutyraldehyde
B
benzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride In dichloromethane for 1h; Heating; | A 93% B n/a |
N-(4-Chlorobenzylidene)-2-ethyl-1-butenylamine
A
2-Ethylbutyraldehyde
B
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride In dichloromethane for 1h; Heating; | A 87% B n/a |
Conditions | Yield |
---|---|
With phosphoric acid at 100℃; for 3h; | 78% |
carbon monoxide
2-pentene
A
2-Ethylbutyraldehyde
B
2-methylvaleraldehyde
C
hexanal
Conditions | Yield |
---|---|
With hydrogen In methoxybenzene at 120℃; under 37503 Torr; for 6h; Product distribution; Further Variations:; Reagents; Pressures; Temperatures; | A n/a B n/a C 20% |
5,5-diethyl-3-nitroso-oxazolidin-2-one
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With potassium hydroxide |
(E)-2-ethyl-2-butenal
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With ethanol; palladium Hydrogenation; |
Conditions | Yield |
---|---|
With copper chromite at 260℃; |
2-ethyl-2-hydroxy-1-butanol
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With sulfuric acid |
3-ethoxymethyl-pentan-3-ol
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With sulfuric acid |
2-vinyl-crotonaldehyde
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With nickel diacetate; iron; acetic acid |
2-ethylcrotonaldehyde
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen at 60℃; for 5h; | |
With nickel Hydrogenation; |
Conditions | Yield |
---|---|
at 110 - 115℃; | |
at 110 - 115℃; |
Conditions | Yield |
---|---|
at 110 - 115℃; |
ethylmagnesium bromide
2-Chloro-N,N-diethylacetamide
A
2-Ethylbutyraldehyde
B
3-diethylaminomethyl-pentan-3-ol
D
N,N-diethyl-2-diethylaminoacetamide
Conditions | Yield |
---|---|
(i) Mg, BrCH2CH2Br, Et2O, (ii) /BRN= 1209224/, (iii) aq. HCl, Et2O; Multistep reaction; |
Conditions | Yield |
---|---|
With perchloric acid In benzene | |
With hydrogen cation | |
With water; sodium chloride; hydrogenchloride at 25℃; Rate constant; isotope effects investigated; |
2-ethyl-N,N-dimethyl-butyramide
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With lithium diethoxyaluminum hydride In diethyl ether |
Conditions | Yield |
---|---|
In acetonitrile | |
(i) MeCN, (ii) aq. NaOAc, AcOH; Multistep reaction; |
Conditions | Yield |
---|---|
(i) MeLi, Et2O, THF, CH2Cl2, (ii) /BRN= 635749/, (iii) NaBO3*4H2O; Multistep reaction; | |
Yield given. Multistep reaction; |
(E)-pent-2-ene
carbon monoxide
A
2-Ethylbutyraldehyde
B
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With hydrogen; cobaltcluster at 150℃; under 51154.1 - 57829.6 Torr; for 22.5h; Mechanism; Product distribution; determination of selectivity, velocity and decomposition of cluster; also with phosphanes; other temperatures, pressures and times; | |
With hydrogen; acetylacetonatodicarbonylrhodium(l) In dichloromethane at 120℃; under 15514.9 Torr; for 16h; |
Conditions | Yield |
---|---|
In water at 20℃; Rate constant; Thermodynamic data; ΔH++, ΔS++; | |
In water at 19.9℃; Rate constant; pH = 4 - 5; |
2-chloro-2-ethylbutyraldehyde
benzylamine
A
2-Ethylbutyraldehyde
B
benzaldehyde
Conditions | Yield |
---|---|
multistep reaction; other substrates; |
Conditions | Yield |
---|---|
With acetylacetonatodicarbonylrhodium(l); hydrogen; (R,S)-binaphos In benzene at 60℃; under 76000 Torr; for 40h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With acetylacetonatodicarbonylrhodium(l); hydrogen; (R,S)-binaphos In benzene at 60℃; under 76000 Torr; for 40h; Yields of byproduct given; |
Conditions | Yield |
---|---|
With acetic acid; quinolinium chlorochromate(VI) at 19.85℃; Kinetics; Further Variations:; Temperatures; Oxidation; |
Conditions | Yield |
---|---|
With 1-penten; η5-pentamethylcyclopentadienylbis(η2-propene)rhodium(I) In benzene at 80℃; for 5h; Isomerization; |
Conditions | Yield |
---|---|
at 110 - 115℃; |
diethyl ether
2-pentene
A
2-Ethylbutyraldehyde
B
2-methylvaleraldehyde
Conditions | Yield |
---|---|
at 125℃; under 220652 Torr; |
Conditions | Yield |
---|---|
at 125℃; under 220652 Torr; |
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
With phenyldimethylsilyl chloride; zinc; bis(cyclopentadienyl)vanadium dichloride In tetrahydrofuran at 20℃; for 13h; Reduction; | 100% |
2-Ethylbutyraldehyde
2-amino-5-chloro-α-(2'-chlorophenyl)benzyl alcohol
[5-chloro-2-(2-ethyl-butylamino)-phenyl]-(2-chloro-phenyl)-methanol
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
Stage #1: 2-Ethylbutyraldehyde; diethylzinc With (Sp,S)-5-[C6H11-CH(Me)-N=C(Me)]-4-OH-[2.2]paracyclophane In hexane at 0℃; for 14h; Stage #2: acetic anhydride In hexane at 20℃; for 24h; Further stages.; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-Phenyl-1-butyne With zinc trifluoromethanesulfonate; triethylamine; (1S,2S)-2-N,N-dimethylamino-1-(p-nitrophenyl)-3-(tert-butyldimethylsilyloxy)propan-1-ol In toluene for 0.25h; Stage #2: 2-Ethylbutyraldehyde In toluene at 25℃; for 2h; Further stages.; | 99% |
With (difluoromethanesulfonyloxy)zincio difluoromethanesulfonate; triethylamine; (1S,2S)-2-N,N-dimethylamino-1-(p-nitrophenyl)-3-(tert-butyldimethylsilyloxy)propan-1-ol In toluene at 25℃; for 2h; | 83% |
Conditions | Yield |
---|---|
Stage #1: phenylacetylene With zinc trifluoromethanesulfonate; triethylamine; (1S,2S)-2-N,N-dimethylamino-1-(p-nitrophenyl)-3-(tert-butyldimethylsilyloxy)propan-1-ol In toluene for 0.25h; Stage #2: 2-Ethylbutyraldehyde In toluene at 25℃; for 2h; Further stages.; | 99% |
With (difluoromethanesulfonyloxy)zincio difluoromethanesulfonate; triethylamine; (1S,2S)-2-N,N-dimethylamino-1-(p-nitrophenyl)-3-(tert-butyldimethylsilyloxy)propan-1-ol In toluene at 25℃; for 2h; | 89% |
2-Ethylbutyraldehyde
trimethylsilylacetylene
dibenzylamine
(-)-N,N-dibenzyl-4-ethyl-1-(trimethylsilyl)hex-1-yn-3-amine
Conditions | Yield |
---|---|
With (R)-1-(2-(diphenylphosphanyl)naphthalen-1-yl)isoquinoline; 4 A molecular sieve; copper(I) bromide In toluene at 20℃; | 99% |
With (R)-1-(2-(diphenylphosphanyl)naphthalen-1-yl)isoquinoline; 4 A molecular sieve; copper(I) bromide In decane; toluene at 20℃; for 144h; | 99% |
With (R)-1-(2-(diphenylphosphanyl)naphthalen-1-yl)isoquinoline; copper(I) bromide In toluene at 20℃; | 95% |
2-Ethylbutyraldehyde
trimethylsilylacetylene
dibenzylamine
(+/-)-N,N-dibenzyl-4-ethyl-1-(trimethylsilyl)hex-1-yn-3-amine
Conditions | Yield |
---|---|
With 4 A molecular sieve; copper(I) bromide In decane; toluene at 20℃; | 99% |
With 4 A molecular sieve; copper(I) bromide In toluene at 20℃; | 99% |
With decane; 4 A molecular sieve; copper(I) bromide In toluene at 20℃; | 86% |
Conditions | Yield |
---|---|
With phenylsilane; pyridine N-oxide; dibutyltin chloride In tetrahydrofuran at 20℃; for 20h; | 99% |
Conditions | Yield |
---|---|
With silica gel In ethanol at 20℃; Ultrasound irradiation; | 99% |
2-Ethylbutyraldehyde
N-phenyl-maleimide
(R)-2-(2,5-dioxo-1-phenylpyrrolidin-3-yl)-2-ethylbutanal
Conditions | Yield |
---|---|
With 1-[(1R,2R)-2-aminocyclohexyl]-3-[4-(n-perfluorooctyl)phenyl]-thiourea; benzoic acid In dichloromethane at 20℃; for 168h; asymmetric Michael addition; optical yield given as %ee; enantioselective reaction; | 99% |
With 1-((1R,2R)-2-aminocyclohexyl)-3-(3,5-bis(trifluoromethyl)phenyl)thiourea; benzoic acid In dichloromethane at 20℃; for 3h; asymmetric Michael addition; optical yield given as %ee; enantioselective reaction; | 95% |
With 1H-imidazole; 1-[(1S,2S)-2-aminocyclohexyl]-2,3-diisopropylguanidine In water; N,N-dimethyl-formamide at 0℃; for 96h; Michael Addition; enantioselective reaction; | 85% |
Conditions | Yield |
---|---|
With tetrabutoxytitanium; water; 2,4-di-tert-butyl-6-({[(1S)-1-(hydroxymethyl)-2-methylpropyl]imino}methyl)phenol In dichloromethane at 20℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With titanium(IV) tetrabutoxide; triethylsilyl chloride In dichloromethane at 20℃; | A n/a B 99% |
2-Ethylbutyraldehyde
2-bromo-3,3,3-trifluoropropene
5-ethyl-1,1,1-trifluoro-2-heptyn-4-ol
Conditions | Yield |
---|---|
Stage #1: 2-bromo-3,3,3-trifluoropropene With n-butyllithium; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; hexane at -78℃; for 0.333333h; Inert atmosphere; Stage #2: 2-Ethylbutyraldehyde In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; | 99% |
2-Ethylbutyraldehyde
pentan-3-yl formate
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 1h; | 99% |
2-Ethylbutyraldehyde
2-ethylbutyl 2-ethylbutanoate
Conditions | Yield |
---|---|
With C18BF16(1-)*C34H53F2NiOP2(1+) In toluene at 20℃; for 1h; Glovebox; Inert atmosphere; | 98% |
With aluminum ethoxide | |
With aluminum isopropoxide |
2-Ethylbutyraldehyde
1-(diethylphosphono)decan-2-one
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 50℃; for 1h; | 98% |
With sodium hydride In tetrahydrofuran at 50℃; for 1h; other aldehydes and β-ketophosphonates; variation of conditions; |
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 12h; | 98% |
2-Ethylbutyraldehyde
diethyl [1-amine(4-methoxyphenyl)methyl]phosphonate
diethyl {[(E)-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 3h; Heating; | 98% |
2-Ethylbutyraldehyde
[Amino-(4-bromo-phenyl)-methyl]-phosphonic acid diethyl ester
diethyl (4-bromophenyl){[(E)-2-ethyl-1-butylidene]amino}methylphosphonate
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 3h; Heating; | 98% |
2-Ethylbutyraldehyde
(S)-1-phenyl-ethylamine
potassium cyanide
(2S)-3-ethyl-2-{[(1S)-1-phenylethyl]amino}pentanenitrile
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water at 20℃; for 72h; Strecker reaction; | 98% |
(E)-1-(4-tolylthio)-3,3,3-trifluoroprop-1-ene
2-Ethylbutyraldehyde
Conditions | Yield |
---|---|
Stage #1: (E)-1-(4-tolylthio)-3,3,3-trifluoroprop-1-ene With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran; hexane at -78℃; Stage #2: 2-Ethylbutyraldehyde In tetrahydrofuran; hexane at -78℃; for 0.25h; Further stages.; | 98% |
Stage #1: (E)-1-(4-tolylthio)-3,3,3-trifluoroprop-1-ene With N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran at -78 - 20℃; Inert atmosphere; Stage #2: With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.166667h; Inert atmosphere; Stage #3: 2-Ethylbutyraldehyde Further stages; | 98% |
Conditions | Yield |
---|---|
With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine In dichloromethane at -78℃; optical yield given as %de; stereoselective reaction; | 98% |
2-Ethylbutyraldehyde
N-phenyl-maleimide
(S)-2-(2,5-dioxo-1-phenylpyrrolidin-3-yl)-2-ethylbutanal
Conditions | Yield |
---|---|
With (S)-3-amino-3-phenylpropanoic acid; caesium carbonate In dichloromethane at 20℃; for 48h; Michael Addition; enantioselective reaction; | 98% |
Stage #1: 2-Ethylbutyraldehyde With tert-butyl (2S,3R)-2-amino-3-hydroxybutanoate; potassium hydroxide In dichloromethane at 23℃; for 0.0333333h; Michael addition; Stage #2: N-phenyl-maleimide In dichloromethane at 23℃; for 6h; Michael addition; optical yield given as %ee; enantioselective reaction; | 96% |
With NH2-Phg-(D-Pro)-Gly-Leu-OH In acetonitrile at 20℃; for 72h; Michael Addition; enantioselective reaction; | 95% |
With (R)-3-phenyl-3-aminopropionic acid; potassium hydroxide In dichloromethane at 20℃; for 48h; Michael Addition; enantioselective reaction; |
2-Ethylbutyraldehyde
trimethylsilyl cyanide
3-ethyl-2-(trimethylsilyloxy)pentanenitrile
Conditions | Yield |
---|---|
With rasta resin-PPh3BnCl In chloroform at 50℃; for 0.5h; Inert atmosphere; | 97% |
zinc(II) iodide at 90 - 100℃; for 3h; | 82% |
With zinc(II) iodide | |
With potassium carbonate In diethyl ether at 20℃; for 6h; Inert atmosphere; |
2-Ethylbutyraldehyde
1-phenylethyl isocyanide
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide In benzene for 2h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
With magnesium sulfate; triethylamine In dichloromethane for 1h; Ambient temperature; | 97% |
2-Ethylbutyraldehyde
aminomethylphosphonic acid diethyl ester
diethyl {[(E)-2-ethyl-1-butylidene]amino}methylphosphonate
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 3h; Heating; | 97% |
With magnesium sulfate In dichloromethane Yield given; |
2-Ethylbutyraldehyde
diethyl 1-aminophenylmethylphosphonate
diethyl {[(E)-2-ethyl-1-butylidene]amino}(phenyl)methylphosphonate
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 3h; Heating; | 97% |
2-Ethylbutyraldehyde
trimethylsilylacetylene
dibenzylamine
N,N-dibenzyl-4-ethyl-1-(trimethylsilyl)-1-heptyn-3-amine
Conditions | Yield |
---|---|
With (R)-1-(2-(diphenylphosphanyl)naphthalen-1-yl)isoquinoline; 4 A molecular sieve; copper(I) bromide In decane; toluene at 20℃; | 97% |
Conditions | Yield |
---|---|
With C36H44N4O4S2; copper(I) bromide In methanol at 20℃; for 36h; Henry reaction; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 97% |
With 4-methyl-N-[(1R)-2-{[(1S,2S)-2-{[(2R)-2-(4-methylbenzenesulfonamido)-2-phenylethyl]amino}-1,2-diphenylethy]amino}-1-phenylethyl]benzene-1-sulfonamido; copper(II) acetate monohydrate In ethanol at 20℃; for 48h; Henry reaction; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 89% |
With C32H20N4O2 In methanol at 20℃; for 8h; Reagent/catalyst; Henry Nitro Aldol Condensation; enantioselective reaction; | 89% |
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