As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:66-25-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Cas:66-25-1
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryProduct description: Product name N-Hexanal CAS number 66-25-1 Assay ≥99% Appearance Colorless liquid Capacity 200mt/year Application Flavors and fragrances More inf
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Caproaldehyde Basic information Product Name: Caproaldehyde Synonyms: 1-pentanecarbaldehyde;butacetin;Capronaldehyd;femanumber2557;hexan-1-al;hexanaldehyde;hexoicaldehyde;Kapronaldehyd
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
N-Hexanal CAS: 66-25-1 Specification Product name N-Hexanal CAS number 66-25-1 Assay ≥99% Appearance Colorless liquid Capacity 200mt/year Application Flavors and fragranc
Cas:66-25-1
Min.Order:1 Kilogram
FOB Price: $100.0 / 150.0
Type:Other
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:66-25-1
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
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Cas:66-25-1
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryHexanal Basic information Product Name: Hexanal Synonyms: Natural Hexaldehyde;butacetin;Capronaldehyd;femanumber2557;hexan-1-al;hexanaldehyde;hexoicaldehyde;Kaprona
Cas:66-25-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryAlmost colorless transparent liquid, in oil and gas and grass apple fragrance. Boiling point 131 ℃, flash point 32 ℃, freezing point ~ 56.3 ℃. Soluble in ethanol, propylene glycol, most of the volatile oil, poorly soluble in water. Natural produ
span lang="EN-US" style="font-size: 9.0pt;font-family:"Arial",sans-serif;color:#4D4D4D">As a leading manufacturer and supplier of chemicals in china, weckchem not only supply popular chemicals, but also weckchem’s r&d center off
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Cas:66-25-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryBaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art
Hangzhou KieRaychem Co.,Ltd.is located in Yuhang District of Hangzhou City and specialized in the chemical product customization, development, sales, import and export. Current business is focused on fine chemicals, pharmaceutical materials and int
Conditions | Yield |
---|---|
With 4 A molecular sieve; tetrabutylammonium periodite; sodium ruthenate(VI) In dichloromethane at 20℃; for 24h; Oxidation; | 100% |
With 4 A molecular sieve; tetrabutylammonium perchlorate; Ru-Cu-Al-hydrotalcite In toluene at 60℃; for 24h; | 100% |
With iodosylbenzene; Cl-CH2-PS supported 5-amino-1,10-phenanthroline-Ru In acetonitrile at 60℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With water In tetrahydrofuran; diethyl ether at 80℃; under 6000.6 Torr; Inert atmosphere; Autoclave; | 100% |
With dibromotriphenylphosphorane In dichloromethane at -50℃; for 1h; | 74% |
With 6C72H112O8*8H2O In chloroform-d1; water for 1h; Inert atmosphere; |
1,1-hexanediol diacetate
hexanal
Conditions | Yield |
---|---|
With beta zeolite modified with chlorosulphonic acid (28 wtpercent) In ethanol at 50℃; for 0.0833333h; | 100% |
With ethanol at 50℃; for 0.166667h; chemoselective reaction; | 98% |
With (NH4)3PW12O40 In methanol at 20℃; for 2h; | 92% |
Conditions | Yield |
---|---|
With water In tetrahydrofuran; diethyl ether at 80℃; under 6000.6 Torr; Inert atmosphere; Autoclave; | 100% |
Conditions | Yield |
---|---|
With thexylchloroborane-Me2SO4 In dichloromethane for 0.25h; Ambient temperature; | 99% |
With thexylchloroborane-Me2SO4 In dichloromethane for 0.25h; Product distribution; Ambient temperature; other aliphatic and aromatic acids, other products, other times; | 99% |
With thexylbromoborane dimethyl sulfide complex In carbon disulfide; dichloromethane at -20 - 20℃; for 1h; | 94% |
hexanoic acid Li-salt
hexanal
Conditions | Yield |
---|---|
With 9-borabicyclo[3.3.1]nonane dimer In tetrahydrofuran for 1h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With hydrogen; sodium dodecyl-sulfate; palladium diacetate In tetrahydrofuran; water at 20℃; under 760.051 Torr; for 0.5h; Reagent/catalyst; chemoselective reaction; | 98% |
With N,N,N,N,N,N-hexamethylphosphoric triamide; diisobutylaluminium hydride In tetrahydrofuran; hexane at 0℃; for 1h; | 89% |
With hydrogen In isopropyl alcohol at 110℃; under 22502.3 Torr; for 3h; Autoclave; | 35.2% |
N-methoxy-N-methyl hexanamide
hexanal
Conditions | Yield |
---|---|
With lithium diisobutyl-tert-butoxyaluminum hydride In tetrahydrofuran; hexane at 0℃; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 97% |
With benzoic acid ethyl ester; copper diisobutyl-t-butoxyaluminum hydride In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; chemoselective reaction; | 99 %Chromat. |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide In dichloromethane; water at 0℃; Electrolysis; Saturated solution; | A n/a B 95% |
With calcium dichloride dihydrate; oxone; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water In dichloromethane at 20℃; for 2.5h; Catalytic behavior; Reagent/catalyst; Time; Solvent; Overall yield = 59 %Chromat.; | A 91% B 9% |
With oxone; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; water In dichloromethane at 20℃; for 4h; Catalytic behavior; Overall yield = 7 %Chromat.; | A 9% B 52% |
isopropyl amyl carbinol
hexanal
Conditions | Yield |
---|---|
With lead(IV) acetate; lithium chloride In benzene at 80℃; | 95% |
Conditions | Yield |
---|---|
With chloro(cyclopentadienyl)[bis(diphenylphosphino)methane]ruthenium; water In isopropyl alcohol at 100℃; for 12h; | 95% |
With water; C46H53F3N4O4P2RuS In acetone at 69 - 72℃; for 36h; Product distribution; Further Variations:; Catalysts; Reagents; anti-Markovnikov hydration; | 96 % Spectr. |
With water; ruthenium In benzene-d6 at 70℃; Product distribution; Further Variations:; Catalysts; |
Conditions | Yield |
---|---|
With aluminium trichloride; tetramethylammonium chlorochromate In acetonitrile for 1h; Heating; | 94% |
Conditions | Yield |
---|---|
With 4-methylmorpholine N-oxide; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride; potassium iodide at 100℃; for 0.0833333h; Microwave irradiation; Ionic liquid; | 94% |
With dihydrogen peroxide In ethanol for 7h; Reflux; Green chemistry; | 62% |
1,1'-bis(phenylthio)hexane
hexanal
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid In dichloromethane for 1h; Ambient temperature; | 92% |
Conditions | Yield |
---|---|
With water; Dess-Martin periodane In dichloromethane at 5℃; for 0.5h; | 92% |
With molybdenum(V) chloride; zinc In acetonitrile at 20℃; for 0.333333h; | 78% |
With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate; acetic acid In water at 40 - 45℃; for 5h; | 70% |
With iodine at 45 - 60℃; for 0.183333h; Reagent/catalyst; Microwave irradiation; | 70% |
trans-2-Octene
hexanal
Conditions | Yield |
---|---|
With cobalt(II) 5,10,15,20-tetraphenylporphyrin; naphthalene; oxygen; isovaleraldehyde at 80℃; under 760.051 Torr; for 6h; | 92% |
Stage #1: trans-2-Octene With cis-[Ru(2,9-Me2phen)2(OH2)2](PF6)2 In acetonitrile at 55℃; for 0.5h; Stage #2: With dihydrogen peroxide In acetonitrile for 8h; | |
Multi-step reaction with 3 steps 1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere 2: sulfuric acid / acetonitrile; water / 20 °C 3: C21H12Cl6NO4V / toluene / 3 h / 100 °C / 760.05 Torr View Scheme |
hexanoxytrimethylsilane
hexanal
Conditions | Yield |
---|---|
With aluminium trichloride; tetramethylammonium chlorochromate In acetonitrile for 1.33333h; Heating; | 90% |
Conditions | Yield |
---|---|
With 20 % Pd(OH)2/C; hydrogen In benzene at 20℃; for 0.5h; | 90% |
sodium caproate
hexanal
Conditions | Yield |
---|---|
With 9-borabicyclo[3.3.1]nonane dimer In tetrahydrofuran for 0.5h; Ambient temperature; | 87% |
Conditions | Yield |
---|---|
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 3h; | 86% |
With diethyl ether; lithium diethoxyaluminum hydride | |
With sodium diethylpiperidinohydroaluminate In tetrahydrofuran at 0℃; for 3h; | 96 % Chromat. |
2-n-pentyl-1,3-dithiolane
hexanal
Conditions | Yield |
---|---|
With sodium nitrate; sulfuric acid; silica gel In dichloromethane at 20℃; for 0.416667h; | 86% |
With polystyryl-mercury trifluoroacetate; water In dichloromethane at 23℃; for 96h; Product distribution; var. temp., and time, var. solvents; other thioacetals and thioketals; | 42 % Chromat. |
Conditions | Yield |
---|---|
With sodium paraperiodate; sulfuric acid In water at 20℃; for 0.5h; | 85% |
Conditions | Yield |
---|---|
With acetylacetonatodicarbonylrhodium(l); hydrogen; triphenylphosphine In neat (no solvent) at 80℃; under 7500.75 Torr; for 1h; Catalytic behavior; Time; Autoclave; | A 11.1% B 83.7% |
With hydrogen; (polymer-PPh2)2Ru(CO)3 In benzene at 140℃; under 51714.8 Torr; for 20h; Product distribution; further temperature, pressure; other catalysts; | |
With water; dodecacarbonyltetrairidium In methanol at 150℃; under 41371.8 Torr; for 0.5h; Product distribution; other group 8 transition-metal catalysts; |
hexanal
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 20℃; under 760.051 Torr; for 31h; Irradiation; Green chemistry; | 83% |
Conditions | Yield |
---|---|
With sodium hydroxide; thexylbromoborane dimethyl sulfide complex; dihydrogen peroxide Product distribution; directive effect of thexylhaloborane-methyl sulfide in the hydroboration of alkynes; further reagents; multistep reaction; | A n/a B 82% |
With water; ; (pentafluorophenyl)diphenylphosphine In isopropyl alcohol at 65℃; for 12h; Title compound not separated from byproducts; | A 3.0 % Chromat. B 71 % Chromat. |
Stage #1: hex-1-yne With aniline; bis(trimethylsilyl)acetylenetitanocene In toluene at 85℃; for 24h; Stage #2: With hydrogenchloride Title compound not separated from byproducts; | |
With C35H44F3N5O3PtS In benzene-d6; water; acetone for 24h; Glovebox; Sealed tube; Heating; Inert atmosphere; | A 21 %Spectr. B 79 %Spectr. |
Conditions | Yield |
---|---|
With sodium tris(tert-butoxo)aluminium hydride In tetrahydrofuran; diethylene glycol dimethyl ether at -78℃; for 1h; | 81% |
Stage #1: Hexanoyl chloride With aluminium hydride In tetrahydrofuran at 20℃; for 1h; Metallation; Stage #2: With pyridinium chlorochromate In tetrahydrofuran; dichloromethane at 20℃; for 6h; Oxidation; | 81% |
With tri-n-butyl-tin hydride; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride In tetrahydrofuran at 25℃; for 0.25h; | 80% |
benzyl hexyl ether
A
1-hexyl nitrite
B
benzaldehyde
C
hexanal
D
hexan-1-ol
Conditions | Yield |
---|---|
With nitric acid In dichloromethane at 20℃; for 1h; Further byproducts given; | A n/a B 81% C n/a D n/a |
tri-n-butyl-tin hydride
A
4,5-dimethyl-2-(tributylstannylsulfanyl)-thiazole
B
hexanal
Conditions | Yield |
---|---|
In benzene-d6 at 20℃; for 0.5h; Inert atmosphere; UV-irradiation; | A 81% B 71% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium carbonate In methanol; water for 8h; Ambient temperature; | 80% |
With sodium perborate for 6h; Ionic liquid; | 75% |
Stage #1: 1-nitrohexane With potassium hydroxide In methanol Nef reaction; Continuous flow conditions; Stage #2: With potassium permanganate; water In methanol at 25℃; Nef reaction; Sonication; Continuous flow conditions; chemoselective reaction; | 74% |
With sodium hydroxide; sodium chlorite; tetra(n-butyl)ammonium hydrogensulfate In dichloromethane for 0.7h; Ambient temperature; Yield given; | |
Multi-step reaction with 2 steps 1: 56 percent / AcONH4 / acetic acid / 10 h / 100 °C 2: aq. H2O2; OH(-); 1-butyl-3-methylimidazolim trifluoromethanesulfonate / 16 h / 25 °C View Scheme |
Conditions | Yield |
---|---|
distannoxane 1a In benzene for 0.5h; Mechanism; Product distribution; Heating; other distannoxane catalysts, other aldehydes, other alcohol, other solvents, other reaction times; | 100% |
With 9.0 wt% H4[SiW12O40] on SiO2 In neat (no solvent) at 60℃; for 6h; Reagent/catalyst; chemoselective reaction; | 99% |
With Kaolinitic clay In benzene for 2h; Heating; | 90% |
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran; tert-butyl alcohol at 0 - 20℃; for 24h; Henry reaction; | 100% |
With potassium tert-butylate In tetrahydrofuran; tert-butyl alcohol Addition; | 99% |
With (S,S)-1,2-diaminocyclohexane; copper(II) acetate monohydrate In ethanol at 20℃; for 12h; Henry reaction; Inert atmosphere; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; trans-Re(O)Cl2(OC(CH3)2C(CH3)2O)2P(Ph)3; oxygen In acetonitrile at 30℃; under 760.051 Torr; for 1.1h; | 100% |
With diphenyl diselenide; dihydrogen peroxide In water at 20℃; for 3h; Green chemistry; | 99% |
With N-hydroxyphthalimide; oxygen In acetonitrile at 30℃; for 3h; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
With Na-phosphate buffer; horse liver NADH; NAD; sodium formate; <(C5Me5)Rh(bpy-5-OAc)(H2O)>Cl2 at 25℃; for 30h; Product distribution; Mechanism; other ketones, other times, other temperatures, other enzymes; | 100% |
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 0.0833333h; Product distribution; other aldehydes, ketones, carboxylic acids (also sodium salts), acid chlorides, esters, lactones, epoxides, amides, nitriles, nitrogen and sulfur compounds; var. temp., time and ratio of reagents; | 100% |
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
Stage #1: propargyl alcohol With n-butyllithium In tetrahydrofuran; hexane at -40℃; for 0.333333h; Inert atmosphere; Stage #2: hexanal With cerium(III) chloride In tetrahydrofuran; hexane Reagent/catalyst; | 100% |
With n-butyllithium In tetrahydrofuran at -78℃; | 93% |
Stage #1: propargyl alcohol With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: hexanal In tetrahydrofuran; hexane at -78 - 0℃; for 2h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With indium In water for 3h; | 100% |
With zinc In tetrahydrofuran | 47% |
With indium In N,N-dimethyl-formamide |
[3-(2-Methyl-[1,3]dioxolan-2-yl)-1-methylsulfanyl-propyl]-phosphonic acid diethyl ester
hexanal
{2-Hydroxy-1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-1-methylsulfanyl-heptyl}-phosphonic acid diethyl ester
Conditions | Yield |
---|---|
With n-butyllithium | 100% |
(3,3-diisopropoxy-propyl)-triphenyl-phosphonium bromide
hexanal
(Z)-3-nonenal diisopropyl acetal
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran for 12h; -100 deg C to RT; | 100% |
With sodium hexamethyldisilazane 1.) THF, toluene, RT, 1 h, 2.) from -100 to 0 deg C, 4 h; Yield given. Multistep reaction; | |
With sodium hexamethyldisilazane 1.) THF, room temp., 1 h; HMPA, 0 deg C, 1 h, 2.) -100 deg C to room temp., overnight; Yield given. Multistep reaction; |
2-methylseleno-2-phenylselenopropan
hexanal
A
butyl methyl selenide
B
(phenylseleno)-2-propane
C
2-phenylseleno-2-methyl octane-3-ol
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.2h; | A 100% B 10% C 90% |
hexanal
N-(2-methoxyphenyl)-2-<(tributylstannyl)methyl>propenamide
4-hydroxy-N-(2-methoxyphenyl)-2-methylenenonanamide
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at -78 - 0℃; for 4h; | 100% |
Conditions | Yield |
---|---|
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: hexanal In tetrahydrofuran; hexane at -78 - 20℃; for 3h; | 100% |
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: hexanal In tetrahydrofuran; hexane at 0℃; for 4h; | 96% |
With n-butyllithium In hexane at 25℃; for 1.5h; | 80% |
hexanal
2-(n-butyl)-2-octenal
Conditions | Yield |
---|---|
With 1,3-dimethylimidazolim iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,4-dioxane for 3h; Heating; | 100% |
With N-benzyl-N,N,N-triethylammonium chloride; 1-chloro-1-fluoromethyl phenyl sulfone In tetrahydrofuran at 20℃; for 4h; | 85% |
With L-Tryptophan In water at 20℃; for 3h; Catalytic behavior; Solvent; Sealed tube; Green chemistry; | 78% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane Ambient temperature; other reagents: H2SO4, TiCl4, SnCl4, trimethylsilyl triflate; | 100% |
hexanal
(1S,5S,6S,7R)-6,7-epoxy-6-[(E)-2'-carbobenzyloxy-1'-vinyl]-2-oxabicyclo[3.3.0]octan-3-one
(1S,5R,7R,2'R,S,3'R,S)-7-hydroxy-6-[(E,Z)-3'-hydroxyoct-2'-carbobenzyloxy-1'-ylidene]-2-oxabicyclo[3.3.0]octan-3-one
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran at -78℃; for 0.833333h; Condensation; | 100% |
hexanal
(3R)-6,8-dibenzyloxy-9-hydroxy-3-methyl-3,4-dihydro-2H-anthracen-1-one
6,8-bis-benzyloxy-9-hydroxy-2-(1-hydroxy-hexyl)-3-methyl-3,4-dihydro-2H-anthracen-1-one
Conditions | Yield |
---|---|
Stage #1: (3R)-6,8-dibenzyloxy-9-hydroxy-3-methyl-3,4-dihydro-2H-anthracen-1-one With TEA; t-butyldimethylsiyl triflate In dichloromethane Stage #2: hexanal With boron trifluoride diethyl etherate at -70℃; | 100% |
hexanal
(5-hexyl-furan-3-yloxy)-trimethyl-silane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at -78℃; for 1h; | 100% |
hexanal
methyl 2-cyanoacetate
(E)-2-cyano-oct-2-enoic acid methyl ester
Conditions | Yield |
---|---|
With piperidine; acetic acid at 20℃; for 14h; | 100% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; zinc trifluoromethanesulfonate; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 25℃; for 12h; Horner-Wadsworth-Emmons reaction; | 100% |
6-({4-[(4-methoxyphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one
hexanal
6-(hexyl{4-[(4-methoxyphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one
Conditions | Yield |
---|---|
Stage #1: 6-({4-[(4-methoxyphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one; hexanal With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 70℃; for 24h; Stage #2: With sodium hydrogencarbonate In water; 1,2-dichloro-ethane | 100% |
styrene
sorbic Acid
hexanal
(1RS,2SR)-2-(1-hydroxyhexyl)-3,5-hexadienoic acid
Conditions | Yield |
---|---|
In tetrahydrofuran; water; diisopropylamine; pentane | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; Molecular sieve; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With : H-D-Pro-Pro-Glu supported on polyethyleneglycol-polystyrene (TentaGel resin) In chloroform; isopropyl alcohol at -15℃; for 19h; optical yield given as %ee; enantioselective reaction; | 100% |
With 4-methyl-morpholine; C16H26N4O5 In neat (no solvent) at 20℃; for 24h; stereoselective reaction; | 100% |
With 4-methyl-morpholine; H-D-Pro-L-Pro-L-Glu-NH2*TFA In chloroform; isopropyl alcohol at 20℃; optical yield given as %ee; enantioselective reaction; | 98% |
Conditions | Yield |
---|---|
With water; sodium sulfate at 20℃; for 7h; Passerini Condensation; | 100% |
Conditions | Yield |
---|---|
With water; sodium tosylate at 20℃; for 7h; Passerini Condensation; | 100% |
Conditions | Yield |
---|---|
With sodium butanolate In butan-1-ol Reflux; | 100% |
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