100% owned factory, regulatory compliance and be audited.Appearance:white powder Application:Commercial
Cas:3095-95-2
Min.Order:0
Negotiable
Type:Manufacturers
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:3095-95-2
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:3095-95-2
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:3095-95-2
Min.Order:1
Negotiable
Type:Other
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:3095-95-2
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:3095-95-2
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryHenan Tianfu Chemical Co., Ltd. is located in Zhengzhou High-tech Development Zone with import and export license. We passed ISO 9001:2008 in 2009, and won "High-tech Enterprise" by provincial government in 2013.The objective of the com
Cas:3095-95-2
Min.Order:1 Gram
FOB Price: $1000.0
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:3095-95-2
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:3095-95-2
Min.Order:1 Kilogram
FOB Price: $21.0 / 23.0
Type:Trading Company
inquiryCAS NO. 3095-95-2 MF NO. C6H13O5P MF Weight: 196.14 Apperance colorless liquid Purity 98% Boiling
Cas:3095-95-2
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:3095-95-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:3095-95-2
Min.Order:1 Kilogram
FOB Price: $137.0 / 142.0
Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:3095-95-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
Cas:3095-95-2
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:3095-95-2
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:3095-95-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:3095-95-2
Min.Order:100 Gram
Negotiable
Type:Other
inquiryHigh purity 3095-95-2 (Diethoxyphosphoryl)acetic acid for sale compectitive price Molecular Formula C6H13O5P Molar Mass 196.14 Density 1.220 g/mL at 25 °C (lit.) Boling Point 150 °C/0.05 mmHg
Cas:3095-95-2
Min.Order:1 Gram
Negotiable
Type:Other
inquiryProduct name: DIETHYLPHOSPHONOACETIC ACID Synonyms: DIETHYLPHOSPHONOACETIC ACID;DIETHYLPHOSPHONOETHANOIC ACID;(DIETHOXYPHOSPHINOYL)ACETIC ACID;DIETHYLCARBOXYMETHYLPHOSPHONATE;Diethylcarboxymethylphosphonate
Cas:3095-95-2
Min.Order:1 Gram
FOB Price: $1.0
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:3095-95-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:3095-95-2
Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquiryProduct Name: DIETHYLPHOSPHONOACETIC ACID Synonyms: DIETHYLPHOSPHONOACETIC ACID;DIETHYLPHOSPHONOETHANOIC ACID;(DIETHOXYPHOSPHINOYL)ACETIC ACID;DIETHYLCARBOXYMETHYLPHOSPHONATE;Diethylcarboxymethylphosphonate, 98 %;2-diethoxyphosphorylacetate;Die
Cas:3095-95-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryBoiling point 150 ° C / 0.05mmhg (lit.) Density 1.220g/mlat25 ° C (lit.) Refractive index N20 / D1 445(lit.) Flash point > 230 ° f Keep in dark place, sealed in dry, room temperature Acidity coefficient (PKA) 3.48 ± 0.10 (p
Cas:3095-95-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryNanjing Fred Technology Co., Ltd. is a professional R&D and manufacturer of API and pharmaceutical intermediates. DIETHYLPHOSPHONOACETIC ACID is one of the most competitive products in our company. We can supply it with good quality and best
Cas:3095-95-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:3095-95-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Cas:3095-95-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:3095-95-2
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With potassium hydroxide In ethanol; water at 20℃; | 100% |
With water; sodium hydroxide In ethanol at 20℃; Inert atmosphere; | 97% |
With hydrogenchloride; potassium hydroxide 1.) aq. EtOH, 20 h; | 95% |
Conditions | Yield |
---|---|
With 1% Pd/C; hydrogen In ethyl acetate | 99% |
With hydrogen; palladium on activated charcoal | |
With hydrogen; palladium on activated charcoal In ethanol |
Conditions | Yield |
---|---|
In toluene Michaelis-Arbuzov Synthesis; Reflux; | 68% |
C12H27O5PSi
diethylphosphonoacetic acid
Conditions | Yield |
---|---|
With hydrogen fluoride In acetonitrile | 62% |
Conditions | Yield |
---|---|
With phosphate buffer; immobilized enzyme preparation from Rhodococcus sp for 168h; Ambient temperature; pH 7.0; | 41% |
tert-butyl diethylphosphonoacetate
diethylphosphonoacetic acid
Conditions | Yield |
---|---|
With hydrogenchloride |
diethoxyphosphoryl-acetic acid ethyl ester
A
diethylphosphonoacetic acid
B
phosphonoacetic acid
C
phosphonoacetic acid ethyl ester
Conditions | Yield |
---|---|
With potassium hydroxide In water Product distribution; various reagents; |
Conditions | Yield |
---|---|
With n-butyllithium 1.) ether, THF, -65 deg C, 30 min, 2.) ether, -65 deg C, 5 min; -65 deg C to room temp., 2 h; Yield given. Multistep reaction; | |
With n-butyllithium 1.) THF, hexane, -78 deg C to -20 deg C, 30 min, 2.) THF, -78 deg C to -10 deg C, 2 h; Multistep reaction; | |
With n-butyllithium at -78℃; |
carbon dioxide
diethyl-1-magnesium chloride methanephosphonate
diethylphosphonoacetic acid
Conditions | Yield |
---|---|
With water 1.) ether, -70 deg. C.; 2.) ether, room. temp.; Yield given. Multistep reaction; |
Methyl diethylphosphonoacetate
A
diethylphosphonoacetic acid
B
diethylphosphinylacethydroxamic acid
Conditions | Yield |
---|---|
With sodium hydroxide; hydroxylamine hydrochloride In water at 20℃; for 18h; pH=12; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With sodium hydroxide; hydroxylamine hydrochloride In water at 20℃; for 72h; pH=12; Title compound not separated from byproducts; |
diethyl iodomethanephosphonate
diethylphosphonoacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: isopropylmagnesium chloride / tetrahydrofuran / 0.75 h / -70 °C 2: 2.) H2O / 1.) ether, -70 deg. C.; 2.) ether, room. temp. View Scheme |
Diethyl phosphonate
bromoacetic acid
diethylphosphonoacetic acid
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol; water |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water |
diethylphosphonoacetic acid
(-)-menthol
(diethoxy-phosphoryl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; Inert atmosphere; | 100% |
With triethylamine; 2-chloropyridinium iodide |
diethylphosphonoacetic acid
diethyl (2-chloro-2-oxoethyl)phosphonate
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In benzene for 1h; | 100% |
With thionyl chloride at 20℃; for 2h; Inert atmosphere; | 92% |
With thionyl chloride at 20℃; for 2h; Inert atmosphere; | 92% |
diethylphosphonoacetic acid
tert-butyl alcohol
tert-butyl diethylphosphonoacetate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 0.25h; | 100% |
With dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 0.25h; Product distribution; Further Variations:; Reaction partners; Reagents; Solvents; | 100% |
With sulfuric acid In various solvent(s) for 12h; | 90% |
With dicyclohexyl-carbodiimide In acetonitrile at 25℃; for 1h; |
diethylphosphonoacetic acid
allyl alcohol
allyl diethylphosphonoacetate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 18h; Esterification; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With dmap; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate In dichloromethane at 20℃; for 48h; | 100% |
With dmap; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate In dichloromethane | 99% |
diethylphosphonoacetic acid
4-(Dimethylamino)butylamine
[(4-dimethylamino-butylcarbamoyl)-methyl]-phosphonic acid diethyl ester
Conditions | Yield |
---|---|
With N'-methyl polystyrene; N-cyclohexylcarbodimide; benzotriazol-1-ol; tris(2-amimoethyl)amine polystyrene In dichloromethane; N,N-dimethyl acetamide at 20℃; for 24h; | 100% |
diethylphosphonoacetic acid
Conditions | Yield |
---|---|
With dmap; PS-carbodiimide; 4-(dimethylamino)pyridine hydrochloride In chloroform for 0.5h; | 100% |
diethylphosphonoacetic acid
4-bromo-phenol
(para-bromophenyl)diethylphosphonoacetate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide; dmap In dichloromethane at 0 - 20℃; for 10h; Addition; | 100% |
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; zinc trifluoromethanesulfonate; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 25℃; for 12h; Horner-Wadsworth-Emmons reaction; | 100% |
diethylphosphonoacetic acid
cyclohexanol
cyclohexyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With dicyclohexyl-carbodiimide In dichloromethane for 0.25h; |
diethylphosphonoacetic acid
diethyl[2-({(3E)-1-[(6-fluoro-2-naphthyl)methyl]-pyrrolidin-3-yl}amino)-2-oxoethyl]phosphonate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 3.5h; | 100% |
diethylphosphonoacetic acid
cyclopropanemethylamine
diethyl {[(cyclopropylmethyl)carbamoyl]methyl}phosphonate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; water for 12h; | 100% |
diethylphosphonoacetic acid
(2-(2-(2-(4-(1-aminobutyl)phenoxy)ethoxy)ethoxy)ethyl)imidodicarbonic acid bis(tert-butyl) ester
(2-(2-(2-(4-(1-(2-(diethoxyphosphoryl)acetamido)butyl)phenoxy)ethoxy)ethoxy)ethyl)imidodicarbonic acid bis(tert-butyl) ester
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 3h; Inert atmosphere; | 100% |
diethylphosphonoacetic acid
(2R,3S,6S)-7-(benzyloxy)-1-((tert-butyldimethylsilyl)oxy)-2,6-dimethyl-5-methyleneheptan-3-ol
(2R,3S,6S)-7-(benzyloxy)-1-((tert-butyldimethylsilyl)oxy)-2,6-dimethyl-5-methyleneheptan-3-yl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; | 100% |
diethylphosphonoacetic acid
(2S,3S,6S)-7-(benzyloxy)-1-((tert-butyldimethylsilyl)oxy)-2,6-dimethyl-5-methyleneheptan-3-ol
(2S,3S,6S)-7-(benzyloxy)-1-((tert-butyldimethylsilyl)oxy)-2,6-dimethyl-5-methyleneheptan-3-yl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; | 100% |
diethylphosphonoacetic acid
2-phenylethanol
phenethyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; |
diethylphosphonoacetic acid
2-(4-Methoxyphenyl)ethanol
4-methoxyphenethyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; |
diethylphosphonoacetic acid
3,4-methylenedioxyphenethyl alcohol
2-(1,3-benzodioxol-5-yl)ethyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; |
diethylphosphonoacetic acid
(RS)-2-phenyl-1-propanol
2-phenylpropyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; |
diethylphosphonoacetic acid
n-heptan1ol
heptyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; |
diethylphosphonoacetic acid
3-trimethylsilyl-1-propanol
3-(trimethylsilyl)propyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; |
diethylphosphonoacetic acid
1-amino-cyclopentanemethanol
cyclopentylmethyl 2-(diethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; |
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
diethylphosphonoacetic acid
2-(4-dimethylaminophenyl)ethyl alcohol
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
diethylphosphonoacetic acid
2-methyl-propan-1-ol
diethyl <(iso-butoxycarbonyl)methyl>phosphonate
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere; | 100% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In toluene at 20℃; for 4h; Inert atmosphere; | 95% |
diethylphosphonoacetic acid
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; toluene at 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 71h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; Inert atmosphere; | 100% |
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