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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 72320-38-8 with best quality

Cas:72320-38-8

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

1-Propanol, 3-azido-

Cas:72320-38-8

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1-Propanol, 3-azido-

Cas:72320-38-8

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Antimex Chemical Limied

Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin

1-Propanol, 3-azido-

Cas:72320-38-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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SAGECHEM LIMITED

3-Azidopropanol 72320-38-8 Application:3-Azidopropanol 72320-38-8

3-Azidopropanol

Cas:72320-38-8

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hubei Jiutian Bio-medical Technology Co., Ltd

Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin

1-Propanol, 3-azido-

Cas:72320-38-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Scochem Technology Co., Ltd.

High quality suppliers Application:healing drugs

3-Azido-1-propanol

Cas:72320-38-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1-Propanol, 3-azido-

Cas:72320-38-8

Min.Order:0

Negotiable

Type:Trading Company

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

3-Azido-1-propanol

Cas:72320-38-8

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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veloxis pharmaceuticals

1-Propanol, 3-azido- CAS No.: 72320-38-8 Storage:as prescribe by the manufaurer Package:pack as requested

1-Propanol, 3-azido-

Cas:72320-38-8

Min.Order:100 Kilogram

Negotiable

Type:Trading Company

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Synthetic route

1-bromo-3-propanol
627-18-9

1-bromo-3-propanol

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In water at 60℃;99%
With sodium azide In water at 80℃; for 72h; Inert atmosphere; Schlenk technique;98%
With sodium azide In N,N-dimethyl-formamide at 90℃;97%
1-chloro-3-hydroxypropane
627-30-5

1-chloro-3-hydroxypropane

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In N,N-dimethyl-formamide at 60℃; for 24h; Substitution;99%
With sodium azide In water for 16h; Reflux;99%
With sodium azide In water at 80℃; for 15h;99%
3-hydroxypropyl methanesulfonate
24590-50-9

3-hydroxypropyl methanesulfonate

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In N,N-dimethyl-formamide at 80℃; for 8h;70%
acrolein
107-02-8

acrolein

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate; sodium azide 1.) H2O, AcOH, 5 deg C, 1 h, 2.) Et2O, H2O, 20 deg C, 45 min; Yield given. Multistep reaction;
2-(3-azidopropoxy)tetrahydro-2H-pyran
1056188-13-6

2-(3-azidopropoxy)tetrahydro-2H-pyran

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With Amberlyst H-15 In methanol at 45℃; for 3h; Hydrolysis;
diethyl ether
60-29-7

diethyl ether

1-chloro-3-hydroxypropane
627-30-5

1-chloro-3-hydroxypropane

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide8.7 g (71.4%)
1-azido-3-t-butylsiloxypropane

1-azido-3-t-butylsiloxypropane

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In tetrahydrofuran
H2 O-EtOH

H2 O-EtOH

1-chloro-3-hydroxypropane
627-30-5

1-chloro-3-hydroxypropane

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium hydroxide; sodium iodide98.6 g (92%)
3-azidopropanal
58503-60-9

3-azidopropanal

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate In water at 20℃; for 0.75h;
2-chloro-ethanol
107-07-3

2-chloro-ethanol

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In water for 22h; Reflux;
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

hexanal
66-25-1

hexanal

2-Pentyl-5,6-dihydro-4H-[1,3]oxazine

2-Pentyl-5,6-dihydro-4H-[1,3]oxazine

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In dichloromethane Ambient temperature; other reagents: H2SO4, TiCl4, SnCl4, trimethylsilyl triflate;100%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

3-azidopropanal
58503-60-9

3-azidopropanal

Conditions
ConditionsYield
With Dess-Martin periodane In dichloromethane at 20℃; for 1h;100%
With pyridinium chlorochromate In dichloromethane at 25℃; for 2h;98%
With pyridinium chlorochromate In dichloromethane at 20℃; for 2h;
With pyridinium chlorochromate In dichloromethane for 2h; Inert atmosphere;
Propiolaldehyde diethyl acetal
10160-87-9

Propiolaldehyde diethyl acetal

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

3-[4-(diethoxymethyl)-1,2,3-triazol-1-yl]propan-1-ol

3-[4-(diethoxymethyl)-1,2,3-triazol-1-yl]propan-1-ol

Conditions
ConditionsYield
Amberlyst A-21*CuI In dichloromethane at 20℃; for 12h; Huisgen cycloaddition;99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

phenylacetylene
536-74-3

phenylacetylene

1-(3-hydroxy-n-propyl)-4-phenyl-1H-1,2,3-triazole
1034194-27-8

1-(3-hydroxy-n-propyl)-4-phenyl-1H-1,2,3-triazole

Conditions
ConditionsYield
With Amberlyst A21*copper(I) iodide for 0.5h; Huisgen cycloaddition; Neat (no solvent);99%
With copper(l) iodide at 70℃; for 0.5h; Reagent/catalyst;97%
With copper (I) acetate In cyclohexane at 20℃; for 2h;96%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

Propiolic acid
471-25-0

Propiolic acid

1-(3-hydroxypropyl)-1H-[1,2,3]triazole-4-carboxylic acid
1101852-31-6

1-(3-hydroxypropyl)-1H-[1,2,3]triazole-4-carboxylic acid

Conditions
ConditionsYield
With ascorbic acid; tris[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-ylmethyl]amine In water; tert-butyl alcohol at 20℃; for 10h;99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

4,6-O-di-tert-butylsilylidene-3-O-levulinoyl-1-O-(N-phenyltrifluoroacetimidoyl)-2-N-trichloroacetamido-α/β-D-glucopyranoside
1154463-83-8

4,6-O-di-tert-butylsilylidene-3-O-levulinoyl-1-O-(N-phenyltrifluoroacetimidoyl)-2-N-trichloroacetamido-α/β-D-glucopyranoside

3-azidopropyl 4,6-O-di(tert-butyl)silylidene-1,2-dideoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside
1158797-01-3

3-azidopropyl 4,6-O-di(tert-butyl)silylidene-1,2-dideoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In dichloromethane at 0 - 20℃; for 1h; Molecular sieve;99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

C13H12N4O
1245932-54-0

C13H12N4O

C16H19N7O2
1245932-57-3

C16H19N7O2

Conditions
ConditionsYield
With Amberlyst A-21*CuI In dichloromethane at 20℃; for 18h; Huisgen's cycloaddition;99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

4-n-methylphenylacetylene
766-97-2

4-n-methylphenylacetylene

3-[4-(4-methylphenyl)-1H-1,2,3-triazol-1-yl]propan-1-ol

3-[4-(4-methylphenyl)-1H-1,2,3-triazol-1-yl]propan-1-ol

Conditions
ConditionsYield
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS);99%
With copper(l) iodide at 70℃; for 0.5h; Reagent/catalyst;97%
With copper(II) sulfate; sodium L-ascorbate In methanol; water at 40℃; for 24h;
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

4-trifluoromethylphenylacetylene
705-31-7

4-trifluoromethylphenylacetylene

3-{4-[4-(trifluoromethyl)phenyl]-1H-1,2,3-triazol-1-yl}propan-1-ol

3-{4-[4-(trifluoromethyl)phenyl]-1H-1,2,3-triazol-1-yl}propan-1-ol

Conditions
ConditionsYield
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS);99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

4-methoxyphenylacetylen
768-60-5

4-methoxyphenylacetylen

3-[4-(4-methoxyphenyl)-1H-1, 2, 3-triazol-1-yl]propan-1-ol

3-[4-(4-methoxyphenyl)-1H-1, 2, 3-triazol-1-yl]propan-1-ol

Conditions
ConditionsYield
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS);99%
With copper(II) sulfate; sodium L-ascorbate In methanol; water at 40℃; for 24h;
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

(2,3,4-trimethoxyphenyl)acetylene
1140509-00-7

(2,3,4-trimethoxyphenyl)acetylene

3-[4-(2,3,4-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl]propan-1-ol

3-[4-(2,3,4-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl]propan-1-ol

Conditions
ConditionsYield
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS);99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

1-(2,3,4-trimethoxyphenyl)prop-2-yn-1-ol

1-(2,3,4-trimethoxyphenyl)prop-2-yn-1-ol

3-{4-[hydroxy(2,3,4-trimethoxyphenyl)methyl]-1H-1,2,3-triazol-1-yl}propan-1-ol

3-{4-[hydroxy(2,3,4-trimethoxyphenyl)methyl]-1H-1,2,3-triazol-1-yl}propan-1-ol

Conditions
ConditionsYield
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS);99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

propargyl alcohol methyl ether
627-41-8

propargyl alcohol methyl ether

C7H13N3O2

C7H13N3O2

Conditions
ConditionsYield
With copper(II) sulfate In tetrahydrofuran; water at 20℃;99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

N3-(2-fluorobenzoyl)-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-(2-fluorobenzoyl)-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-(2-fluorobenzoyl)-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

N3-(2-fluorobenzoyl)-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation;99%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

N3-benzoyl-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-benzoyl-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-benzoyl-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

N3-benzoyl-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation;98%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

toluenesulfonic acid 3-azidopropyl ester
153207-76-2

toluenesulfonic acid 3-azidopropyl ester

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 16h; Schlenk technique; Inert atmosphere;97%
With triethylamine In dichloromethane at 4 - 20℃; for 6.06667h;80%
With triethylamine In dichloromethane at 20℃; Inert atmosphere;78.8%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

cyclopentanone
120-92-3

cyclopentanone

1-(3'-hydroxypropyl)piperidin-2-one
71533-22-7

1-(3'-hydroxypropyl)piperidin-2-one

Conditions
ConditionsYield
Stage #1: 3-azidopropan-1-ol; cyclopentanone With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 17.5h; Boyer reaction;
Stage #2: With sodium hydrogencarbonate at 20℃; for 0.5h; Hydrolysis;
97%
6,9,12,15,18-penta[4-(hept-6-ynylsulfanyl)phenyl]-1,6,9,12,15,18-hexahydro(C60)[5,6]fullerene
959417-35-7

6,9,12,15,18-penta[4-(hept-6-ynylsulfanyl)phenyl]-1,6,9,12,15,18-hexahydro(C60)[5,6]fullerene

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

6,9,12,15,18-penta(4-{5-[1-(3-hydroxypropyl)-1,2,3-triazolyl]pentylsulfanyl}phenyl)-1,6,9,12,15,18-hexahydro(C60)[5,6]fullerene

6,9,12,15,18-penta(4-{5-[1-(3-hydroxypropyl)-1,2,3-triazolyl]pentylsulfanyl}phenyl)-1,6,9,12,15,18-hexahydro(C60)[5,6]fullerene

Conditions
ConditionsYield
With copper(I) bromide dimethylsulfide complex; N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 20℃; for 24h; Huisgen cycloaddition;97%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-benzoyl-D-glucopyranosyl trichloroacetimidate
1056442-08-0

2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-benzoyl-D-glucopyranosyl trichloroacetimidate

3-azidopropyl 2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside
1144493-12-8

3-azidopropyl 2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Conditions
ConditionsYield
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 2h; Molecular sieve;97%
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 1.5h; Molecular sieve;97%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

2-ethynylbenzaldehyde
38846-64-9

2-ethynylbenzaldehyde

4-(2-formylphenyl)-1-(3-hydroxypropyl)-1,2,3-triazole

4-(2-formylphenyl)-1-(3-hydroxypropyl)-1,2,3-triazole

Conditions
ConditionsYield
With cobalt at 70℃; for 2h; Reagent/catalyst;97%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

3-(3-(prop-2-yn-1-yloxy)-2-((3-(prop-2-yn-1-yloxy)-2,2-bis((prop-2-yn-1yloxy)methyl)propoxy)methyl)-2-((prop-2-yn-1-yloxy)methyl)propoxy)prop-1-yne

3-(3-(prop-2-yn-1-yloxy)-2-((3-(prop-2-yn-1-yloxy)-2,2-bis((prop-2-yn-1yloxy)methyl)propoxy)methyl)-2-((prop-2-yn-1-yloxy)methyl)propoxy)prop-1-yne

C46H76N18O13

C46H76N18O13

Conditions
ConditionsYield
With copper(II) sulfate In 1,4-dioxane; water97%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

N3-(2-fluorobenzyl)-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-(2-fluorobenzyl)-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-(2-fluorobenzyl)-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

N3-(2-fluorobenzyl)-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation;97%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

N,N,N-tris(prop-2-ynyl)amino-undecahydro-closo-dodecaborate(1-) tetramethylammonium

N,N,N-tris(prop-2-ynyl)amino-undecahydro-closo-dodecaborate(1-) tetramethylammonium

N,N,N-tris[1-(3-hydroxypropyl)(1,2,3-triazol-4-yl)methyl]amino-undecahydro-closo-dodecaborate(1-) tetramethylammonium

N,N,N-tris[1-(3-hydroxypropyl)(1,2,3-triazol-4-yl)methyl]amino-undecahydro-closo-dodecaborate(1-) tetramethylammonium

Conditions
ConditionsYield
With sodium ascorbate; copper diacetate In acetonitrile to soln. of borate were added Cu(CH3O2)2 and sodium ascorbate at room temp., azidopropanol was added dropwise with stirring, mixt. was stirred for 6 h; mixt. was filtered, Et2O was added, ppt. was removed by filtration and Et2O was added to filtrate, ppt. was filtered; elem.anal.;96%
2-Adamantanone
700-58-3

2-Adamantanone

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

(1R,3R,8S)-4-(3′-hydroxypropyl)-4-azatricyclo[4.3.1.1]-undecan-5-one

(1R,3R,8S)-4-(3′-hydroxypropyl)-4-azatricyclo[4.3.1.1]-undecan-5-one

Conditions
ConditionsYield
With trifluorormethanesulfonic acid at 20℃; for 1h; Schmidt Reaction; Inert atmosphere; Sealed tube;96%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

N3-benzyl-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-benzyl-N1-(prop-2-yn-1-yl)quinazoline-2,4-dione

N3-benzyl-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

N3-benzyl-N1-{[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-yl]methyl}quinazoline-2,4-dione

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation;96%
propargyl β-D-glucopyranoside
34272-03-2, 151168-59-1, 151168-60-4

propargyl β-D-glucopyranoside

3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

C12H21N3O7

C12H21N3O7

Conditions
ConditionsYield
With isopropyl alcohol In water at 20℃; for 6h; Sealed tube; Irradiation; Inert atmosphere;96%
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

cyclohexanone
108-94-1

cyclohexanone

hexahydro-1-(3′-hydroxypropyl)-2H-azepin-2-one
91115-29-6

hexahydro-1-(3′-hydroxypropyl)-2H-azepin-2-one

Conditions
ConditionsYield
With trifluorormethanesulfonic acid at 20℃; for 1h; Schmidt Reaction; Inert atmosphere; Sealed tube;95%
With boron trifluoride diethyl etherate In dichloromethane for 3h;90%
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 3.5h;71%
With potassium hydroxide; boron trifluoride diethyl etherate 1.) CH2Cl2, 0 deg C, 1 h; reflux, 72 h, 2.) 24 h; Yield given; Multistep reaction;
3-azidopropan-1-ol
72320-38-8

3-azidopropan-1-ol

1-phenyl-4-cyclohexanone
4894-75-1

1-phenyl-4-cyclohexanone

1-(3′-hydroxypropyl)-5-phenylazepan-2-one

1-(3′-hydroxypropyl)-5-phenylazepan-2-one

Conditions
ConditionsYield
With trifluorormethanesulfonic acid at 20℃; for 1h; Reagent/catalyst; Schmidt Reaction; Inert atmosphere; Sealed tube;95%

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