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Cas:72320-38-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
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Cas:72320-38-8
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:72320-38-8
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryOur own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin
3-Azidopropanol 72320-38-8 Application:3-Azidopropanol 72320-38-8
Cas:72320-38-8
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:72320-38-8
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiry1-Propanol, 3-azido- CAS No.: 72320-38-8 Storage:as prescribe by the manufaurer Package:pack as requested
1-bromo-3-propanol
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium azide In water at 60℃; | 99% |
With sodium azide In water at 80℃; for 72h; Inert atmosphere; Schlenk technique; | 98% |
With sodium azide In N,N-dimethyl-formamide at 90℃; | 97% |
1-chloro-3-hydroxypropane
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 60℃; for 24h; Substitution; | 99% |
With sodium azide In water for 16h; Reflux; | 99% |
With sodium azide In water at 80℃; for 15h; | 99% |
3-hydroxypropyl methanesulfonate
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 80℃; for 8h; | 70% |
acrolein
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate; sodium azide 1.) H2O, AcOH, 5 deg C, 1 h, 2.) Et2O, H2O, 20 deg C, 45 min; Yield given. Multistep reaction; |
2-(3-azidopropoxy)tetrahydro-2H-pyran
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With Amberlyst H-15 In methanol at 45℃; for 3h; Hydrolysis; |
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide | 8.7 g (71.4%) |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium iodide | 98.6 g (92%) |
3-azidopropanal
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In water at 20℃; for 0.75h; |
2-chloro-ethanol
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium azide In water for 22h; Reflux; |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane Ambient temperature; other reagents: H2SO4, TiCl4, SnCl4, trimethylsilyl triflate; | 100% |
3-azidopropan-1-ol
3-azidopropanal
Conditions | Yield |
---|---|
With Dess-Martin periodane In dichloromethane at 20℃; for 1h; | 100% |
With pyridinium chlorochromate In dichloromethane at 25℃; for 2h; | 98% |
With pyridinium chlorochromate In dichloromethane at 20℃; for 2h; | |
With pyridinium chlorochromate In dichloromethane for 2h; Inert atmosphere; |
Propiolaldehyde diethyl acetal
3-azidopropan-1-ol
Conditions | Yield |
---|---|
Amberlyst A-21*CuI In dichloromethane at 20℃; for 12h; Huisgen cycloaddition; | 99% |
3-azidopropan-1-ol
phenylacetylene
1-(3-hydroxy-n-propyl)-4-phenyl-1H-1,2,3-triazole
Conditions | Yield |
---|---|
With Amberlyst A21*copper(I) iodide for 0.5h; Huisgen cycloaddition; Neat (no solvent); | 99% |
With copper(l) iodide at 70℃; for 0.5h; Reagent/catalyst; | 97% |
With copper (I) acetate In cyclohexane at 20℃; for 2h; | 96% |
3-azidopropan-1-ol
Propiolic acid
1-(3-hydroxypropyl)-1H-[1,2,3]triazole-4-carboxylic acid
Conditions | Yield |
---|---|
With ascorbic acid; tris[1-(3-hydroxypropyl)-1H-1,2,3-triazol-4-ylmethyl]amine In water; tert-butyl alcohol at 20℃; for 10h; | 99% |
3-azidopropan-1-ol
4,6-O-di-tert-butylsilylidene-3-O-levulinoyl-1-O-(N-phenyltrifluoroacetimidoyl)-2-N-trichloroacetamido-α/β-D-glucopyranoside
3-azidopropyl 4,6-O-di(tert-butyl)silylidene-1,2-dideoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 0 - 20℃; for 1h; Molecular sieve; | 99% |
Conditions | Yield |
---|---|
With Amberlyst A-21*CuI In dichloromethane at 20℃; for 18h; Huisgen's cycloaddition; | 99% |
3-azidopropan-1-ol
4-n-methylphenylacetylene
Conditions | Yield |
---|---|
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS); | 99% |
With copper(l) iodide at 70℃; for 0.5h; Reagent/catalyst; | 97% |
With copper(II) sulfate; sodium L-ascorbate In methanol; water at 40℃; for 24h; |
3-azidopropan-1-ol
4-trifluoromethylphenylacetylene
Conditions | Yield |
---|---|
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS); | 99% |
3-azidopropan-1-ol
4-methoxyphenylacetylen
Conditions | Yield |
---|---|
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS); | 99% |
With copper(II) sulfate; sodium L-ascorbate In methanol; water at 40℃; for 24h; |
3-azidopropan-1-ol
(2,3,4-trimethoxyphenyl)acetylene
Conditions | Yield |
---|---|
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS); | 99% |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With CuI supported on Amberlyst A-21 In dichloromethane at 20℃; Combinatorial reaction / High throughput screening (HTS); | 99% |
Conditions | Yield |
---|---|
With copper(II) sulfate In tetrahydrofuran; water at 20℃; | 99% |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation; | 99% |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation; | 98% |
3-azidopropan-1-ol
p-toluenesulfonyl chloride
toluenesulfonic acid 3-azidopropyl ester
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 16h; Schlenk technique; Inert atmosphere; | 97% |
With triethylamine In dichloromethane at 4 - 20℃; for 6.06667h; | 80% |
With triethylamine In dichloromethane at 20℃; Inert atmosphere; | 78.8% |
3-azidopropan-1-ol
cyclopentanone
1-(3'-hydroxypropyl)piperidin-2-one
Conditions | Yield |
---|---|
Stage #1: 3-azidopropan-1-ol; cyclopentanone With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 17.5h; Boyer reaction; Stage #2: With sodium hydrogencarbonate at 20℃; for 0.5h; Hydrolysis; | 97% |
6,9,12,15,18-penta[4-(hept-6-ynylsulfanyl)phenyl]-1,6,9,12,15,18-hexahydro(C60)[5,6]fullerene
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With copper(I) bromide dimethylsulfide complex; N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 20℃; for 24h; Huisgen cycloaddition; | 97% |
3-azidopropan-1-ol
2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-benzoyl-D-glucopyranosyl trichloroacetimidate
3-azidopropyl 2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 2h; Molecular sieve; | 97% |
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 1.5h; Molecular sieve; | 97% |
3-azidopropan-1-ol
2-ethynylbenzaldehyde
Conditions | Yield |
---|---|
With cobalt at 70℃; for 2h; Reagent/catalyst; | 97% |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With copper(II) sulfate In 1,4-dioxane; water | 97% |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation; | 97% |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium ascorbate; copper diacetate In acetonitrile to soln. of borate were added Cu(CH3O2)2 and sodium ascorbate at room temp., azidopropanol was added dropwise with stirring, mixt. was stirred for 6 h; mixt. was filtered, Et2O was added, ppt. was removed by filtration and Et2O was added to filtrate, ppt. was filtered; elem.anal.; | 96% |
2-Adamantanone
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 20℃; for 1h; Schmidt Reaction; Inert atmosphere; Sealed tube; | 96% |
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In ethanol; water at 40 - 45℃; for 0.5h; Temperature; Huisgen Cycloaddition; Microwave irradiation; | 96% |
propargyl β-D-glucopyranoside
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With isopropyl alcohol In water at 20℃; for 6h; Sealed tube; Irradiation; Inert atmosphere; | 96% |
3-azidopropan-1-ol
cyclohexanone
hexahydro-1-(3′-hydroxypropyl)-2H-azepin-2-one
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 20℃; for 1h; Schmidt Reaction; Inert atmosphere; Sealed tube; | 95% |
With boron trifluoride diethyl etherate In dichloromethane for 3h; | 90% |
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; for 3.5h; | 71% |
With potassium hydroxide; boron trifluoride diethyl etherate 1.) CH2Cl2, 0 deg C, 1 h; reflux, 72 h, 2.) 24 h; Yield given; Multistep reaction; |
3-azidopropan-1-ol
1-phenyl-4-cyclohexanone
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 20℃; for 1h; Reagent/catalyst; Schmidt Reaction; Inert atmosphere; Sealed tube; | 95% |
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