CAS No.627-30-5,3-Chloro-1-propanol Suppliers,MSDS download

Jinan Finer Chemical Co., Ltd

Product description: Product name 3-Chloro-1-propanol CAS number 627-30-5 Assay ≥99% Appearance Colorless transparent liquid Capacity 200mt/year Application Organic synthesis

3-Chloro-1-propanol

Cas:627-30-5

Min.Order:1 Kilogram

FOB Price: $12.0

Type:Lab/Research institutions

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Hunan Russell Chemicals Technology Co.,Ltd

low price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China

1-Chloro-3-hydroxypropane, 98% 627-30-5

Cas:627-30-5

Min.Order:0

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Type:Trading Company

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#627-30-5;CAT#A833956

Cas:627-30-5

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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Synthetic route

: 504-63-2
trimethyleneglycol

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With hydrogenchloride; benzenesulfonic acid In water at 50 - 90℃; for 13h; Large scale;	96%
With hydrogenchloride at 150 - 170℃;	60%
With disulfur dichloride at 100℃;

: 625-36-5
2-chloropropionyl chloride

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With sodium tetrahydroborate; lithium perchlorate In acetonitrile for 0.666667h;	87%

: 89031-82-3
1-(t-Butyldimethylsilyloxy)-3-chloro-propane

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With zinc tetrafluoroborate In water for 16h; Ambient temperature;	85%

: 623-71-2
ethyl 3-chloropropanoate

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With lithium borohydride; Trimethyl borate In diethyl ether for 0.5h; Heating;	84%
With lithium borohydride; Trimethyl borate In diethyl ether for 0.5h; Heating;	84%
With Ν,Ν-dimethylethylamine alane In tetrahydrofuran; toluene at 0℃; for 0.25h;	99 % Chromat.
With lithium aluminium tetrahydride In diethyl ether 1.) 0 deg C, 30 min, 2.) 3 h, room temp.;

: 504-63-2
trimethyleneglycol

A: 142-28-9
1,3-Dichloropropane

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With tetrachloromethane; triphenylphosphine In acetonitrile Product distribution; Mechanism;	A 16% B 75%
With hydrogenchloride at 100℃;
With hydrogenchloride
With tert-butylhypochlorite; triphenylphosphine In chloroform Product distribution; 1.) -70 deg C, 2.) RT, 3.) reflux, 24 h;

: 56-23-5
tetrachloromethane

: 504-63-2
trimethyleneglycol

A: 2-(3,3,3-trichloropropyl)-1,3-dioxane

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
hexacarbonyl molybdenum at 140℃; for 6h;	A 27% B 73%

...Expand

: 503-30-0
trimethylene oxide

: 463-72-9
carbamic chloride

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With diethyl ether

: 503-30-0
trimethylene oxide

: 677-22-5
tert-butylmagnesium chloride

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With diethyl ether

: 50-00-0
formaldehyd

: 74-85-1
ethene

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With hydrogenchloride; water; zinc(II) chloride under 44130.5 - 51485.6 Torr;

: 127-08-2
potassium acetate

: 64-19-7
acetic acid

: 109-70-6
1,3-chlorobromopropane

A: 628-66-0
1,3-diacetoxypropane

B: 628-09-1
3-Chloropropyl acetate

C: 592-33-6
3-bromopropyl acetate

D: 627-30-5
1-chloro-3-hydroxypropane

...Expand

: 6001-87-2
methyl 3-chloropropionate

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With lithium aluminium tetrahydride; diethyl ether

: 504-63-2
trimethyleneglycol

A: 2396-61-4
bis(3-hydroxypropyl)ether

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With hydrogenchloride at 100℃; wurde ueber das Diacetat gereinigt;

: 503-30-0
trimethylene oxide

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With hydrogenchloride

: 107-05-1
3-chloroprop-1-ene

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
(i) bis-(2-methyl-butyl)-borane, THF, H2O2, (ii) aq. NaOH; Multistep reaction;

: 75-89-8
2,2,2-trifluoroethanol

: 94670-19-6
{4-[1-(3-Chloro-propoxy)-ethyl]-phenyl}-dimethyl-amine; compound with perchloric acid

A: Dimethyl-{4-[1-(2,2,2-trifluoro-ethoxy)-ethyl]-phenyl}-amine; compound with perchloric acid

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With sodium perchlorate In water at 25℃; Equilibrium constant;

...Expand

: 75-89-8
2,2,2-trifluoroethanol

: 94670-24-3
1-(1-(3-chloropropoxy)ethyl)-4-methoxybenzene

A: 94670-31-2
1-(4-methoxyphenyl)ethyl trifluoroethyl ether

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With sodium perchlorate In water at 25℃; Equilibrium constant;

...Expand

: 109-70-6
1,3-chlorobromopropane

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With water; triethylamine In ethanol at 125℃; Kinetics; further temperatures, further solvent, activation enthalpy and entropy;
With haloalkane dehalogenase from Xanthobacter autotrophicus GJ10; water In aq. phosphate buffer at 30℃; pH=8; Reagent/catalyst; Enzymatic reaction;

: 94670-19-6
{4-[1-(3-Chloro-propoxy)-ethyl]-phenyl}-dimethyl-amine; compound with perchloric acid

A: 1-(4-Dimethylamino-phenyl)-ethanol; compound with perchloric acid

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With sodium perchlorate; water at 25℃; Equilibrium constant;

: 94670-24-3
1-(1-(3-chloropropoxy)ethyl)-4-methoxybenzene

A: 3319-15-1
rac-1-(4-methoxyphenyl)-ethanol

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With sodium perchlorate; water at 25℃; Equilibrium constant;

: 107-05-1
3-chloroprop-1-ene

A: 71-23-8
propan-1-ol

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide Product distribution; 1) THF, 25 deg C, 2 h;	A 1 % Chromat. B 93 % Chromat.

: 106-89-8
epichlorohydrin

A: 127-00-4
1-Chloro-2-propanol

B: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With zinc(II) tetrahydroborate; silica gel In tetrahydrofuran for 24h; Product distribution; Ambient temperature; other epoxides;
With zinc(II) tetrahydroborate; silica gel In tetrahydrofuran for 24h; Ambient temperature; Yield given. Yields of byproduct given;
With zeolite supported zinc borohydride In tetrahydrofuran at 20℃; for 12h; Yield given. Yields of byproduct given;
With hydrogen; palladium on activated charcoal In ethyl acetate at 23℃; under 760.051 Torr; for 20h;	A 91 % Chromat. B 9.0 % Chromat.

: 503-30-0
trimethylene oxide

: 7647-01-0
hydrogenchloride

: 71-43-2
benzene

: 627-30-5
1-chloro-3-hydroxypropane

...Expand

: 503-30-0
trimethylene oxide

: 7446-70-0
aluminium trichloride

: 71-43-2
benzene

A: 122-97-4
3-Phenyl-1-propanol

B: 627-30-5
1-chloro-3-hydroxypropane

...Expand

trimethylenechloro acetate: trimethylenechloro acetate

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
With hydrogenchloride; methanol

: 504-63-2
trimethyleneglycol

S2cl2: S2cl2

: 627-30-5
1-chloro-3-hydroxypropane

: 7647-01-0
hydrogenchloride

: 50-00-0
formaldehyd

: 74-85-1
ethene

ZnCl2: ZnCl2

: 627-30-5
1-chloro-3-hydroxypropane

Conditions

Conditions	Yield
under 44130.5 - 51485.6 Torr; bei Raumtemperatur;
at 20℃; under 44130.5 - 51485.6 Torr;

...Expand

: 107-94-8
chloropropionic acid

: 60-29-7
diethyl ether

lithium alanate: lithium alanate

A: 71-23-8
propan-1-ol

B: 627-30-5
1-chloro-3-hydroxypropane

...Expand

: 7647-01-0
hydrogenchloride

: 504-63-2
trimethyleneglycol

A: 2396-61-4
bis(3-hydroxypropyl)ether

B: 142-28-9
1,3-Dichloropropane

C: 627-30-5
1-chloro-3-hydroxypropane

...Expand

: 110-86-1
pyridine

: 627-30-5
1-chloro-3-hydroxypropane

: 1-(3-hydroxypropyl)pyridinium chloride

Conditions

Conditions	Yield
at 124℃; for 24h; Inert atmosphere;	100%
for 12h; Heating;	98%
at 100℃; Inert atmosphere;	92%

: 115012-09-4
6,7-Dihydro-7-hydroxy-5H-pyrrolo<3,4-b>pyridin-5-one

: 627-30-5
1-chloro-3-hydroxypropane

: 135128-34-6
7-(3-Chloro-propoxy)-6,7-dihydro-pyrrolo[3,4-b]pyridin-5-one

Conditions

Conditions	Yield
With toluene-4-sulfonic acid at 80℃; for 0.5h;	100%

: 623-73-4
diazoacetic acid ethyl ester

: 627-30-5
1-chloro-3-hydroxypropane

: 143165-48-4
ethyl 2-(3-chloropropoxy)acetate

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 37℃;	100%
With boron trifluoride diethyl etherate In dichloromethane for 3h;	75%
boron trifluoride diethyl etherate In dichloromethane at 37℃; cooling with ice-methanol;	65%
boron trifluoride diethyl etherate In chloroform for 3h; Condensation;
With trifluoroborane diethyl ether In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran

: 603-85-0
2-Amino-3-nitrophenol

: 627-30-5
1-chloro-3-hydroxypropane

: 59820-28-9
2-(2-amino-3-nitrophenoxy)ethanol

Conditions

Conditions	Yield
With potassium carbonate In acetone for 20h; Heating; Reflux;	100%

: 2713-34-0
3,5-difluorophenol

: 627-30-5
1-chloro-3-hydroxypropane

: 3-(3,5-difluorophenoxy)propan-1-ol

Conditions

Conditions	Yield
With sodium hydride In N,N-dimethyl-formamide at 0 - 80℃; Large scale;	100%

: 603-85-0
2-Amino-3-nitrophenol

: 627-30-5
1-chloro-3-hydroxypropane

: 1188915-87-8
3-(2-amino-3-nitrophenoxy)propan-1-ol

Conditions

Conditions	Yield
With potassium carbonate In acetone for 20h; Reflux;	100%
With potassium carbonate In acetone for 20h; Reflux;	100%

: 25372-14-9
N-(2-methylphenyl)-2-mercaptoimidazole

: 627-30-5
1-chloro-3-hydroxypropane

: 161190-54-1
3-(1-o-tolyl-1H-imidazol-2-ylsulfanyl)propan-1-ol

Conditions

Conditions	Yield
With sodium hydroxide In isopropyl alcohol for 2.5h; Heating;	99.8%

: 627-30-5
1-chloro-3-hydroxypropane

: 40440-12-8
(3-hydroxypropyl)hydrazine

Conditions

Conditions	Yield
With hydrazine hydrate; sodium hydroxide at 98℃; for 1h; Inert atmosphere;	99%
With sodium hydroxide; hydrazine hydrate at 95 - 100℃; Inert atmosphere;	43%
With sodium hydroxide; hydrazine hydrate

: 115-11-7
isobutene

: 627-30-5
1-chloro-3-hydroxypropane

: 1190-17-6
3-(1,1-dimethylethoxy)-1-chloropropane

Conditions

Conditions	Yield
With sulfuric acid In dichloromethane at -78℃; Addition;	99%
With sulfuric acid for 24h;	78%
sulfuric acid for 24h; in an autoclave;	78%

: 627-30-5
1-chloro-3-hydroxypropane

: 72320-38-8
3-azidopropan-1-ol

Conditions

Conditions	Yield
With sodium azide In N,N-dimethyl-formamide at 60℃; for 24h; Substitution;	99%
With sodium azide In water for 16h; Reflux;	99%
With sodium azide In water at 80℃; for 15h;	99%

: 22325-16-2
(1S)-6,7-dimethoxy-2-methyl-1-(2,4,5-trimethoxyphenyl)-1,2,3,4-tetrahydroisoquinoline

: 78-93-3
butanone

: 627-30-5
1-chloro-3-hydroxypropane

: 6,7-dimethoxy-2-(3-hydroxypropyl)-2-methyl-1-(3,4,5-trimethoxyphenyl)-1,2,3,4-tetrahydroisoquinolinium chloride

Conditions

Conditions	Yield
With sodium iodide; sodium carbonate In water	99%

...Expand

: 489-91-8, 528-16-5, 552-12-5, 577-46-8, 643-33-4, 2240-07-5, 6294-16-2, 10133-02-5, 18402-78-3, 18968-14-4, 21179-08-8, 23018-83-9, 33599-45-0, 33599-46-1, 46171-67-9, 46171-69-1, 46172-26-3, 70021-34-0, 71031-08-8, 104195-06-4, 106499-29-0, 124817-72-7
D-glucuronic acid

: 627-30-5
1-chloro-3-hydroxypropane

: 3'-chloropropyl D-glucofuranosidurono-6,3-lactone

Conditions

Conditions	Yield
at 60℃; for 0.166667h; Microwave irradiation;	99%

: 2033-24-1
cycl-isopropylidene malonate

: 627-30-5
1-chloro-3-hydroxypropane

: C6H9ClO4

Conditions

Conditions	Yield
at 120℃; for 3h;	99%

: 617-86-7
triethylsilane

: 627-30-5
1-chloro-3-hydroxypropane

: 2290-35-9
(3-chloropropyl)triethylsilane

Conditions

Conditions	Yield
With potassium carbonate In tetrahydrofuran; N,N-dimethyl-formamide at 60℃; for 18h; Inert atmosphere;	99%

: 144292-32-0
2,3-difluoro-4-bromophenol

: 627-30-5
1-chloro-3-hydroxypropane

: C9H9BrF2O2

Conditions

Conditions	Yield
With potassium carbonate In acetonitrile at 80℃; for 40h;	98.42%

: 1849-36-1
para-nitrobenzenethiol

: 627-30-5
1-chloro-3-hydroxypropane

: 75032-30-3
γ-<(p-nitrophenyl)thio>propanol

Conditions

Conditions	Yield
With sodium hydroxide In water at 80℃; for 3.41667h;	98%
With potassium hydroxide

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 627-30-5
1-chloro-3-hydroxypropane

: 18171-15-8
(3-chloropropoxy)trimethylsilane

Conditions

Conditions	Yield
With ammonium thiocyanate In dichloromethane at 0℃; for 0.166667h;	98%
for 48h; Heating;

: 1,4,7,10-tetraazabicyclo<5.5.3>pentadecane trihydrobromide

: 627-30-5
1-chloro-3-hydroxypropane

: 4,10-{bis(3-hydroxypropyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane} monohydrobromide

Conditions

Conditions	Yield
With molecular sieve; sodium carbonate In acetonitrile for 168h; Condensation; Heating;	98%

: 34451-26-8
2-perfluorohexylethanethiol

: 627-30-5
1-chloro-3-hydroxypropane

: 36880-06-5
3-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octylsulfanyl)-propan-1-ol

Conditions

Conditions	Yield
With potassium carbonate In ethanol at 75℃; for 6h;	98%

: 83-56-7
1,5-dihydroxynaphthalene

: 627-30-5
1-chloro-3-hydroxypropane

: 220223-39-2
1,5-bis(3-hydroxypropoxy)naphthalene

Conditions

Conditions	Yield
Stage #1: 1,5-dihydroxynaphthalene With potassium carbonate In acetonitrile for 1h; Inert atmosphere; Reflux; Stage #2: 1-chloro-3-hydroxypropane With potassium iodide In acetonitrile for 24h; Inert atmosphere; Heating;	98%
With caesium carbonate In acetonitrile Reflux;	45%

: 13992-16-0, 23661-28-1, 24404-53-3, 28512-68-7, 65236-85-3, 86782-39-0, 121524-01-4, 121570-34-1, 108032-93-5
phenyl 2,3,4,6-tetra-O-acetyl-1-thio-α-D-mannopyranoside

: 627-30-5
1-chloro-3-hydroxypropane

: 2,3,4,6-tetra-O-acetyl-1-O-(3-chloropropyl)-α-D-mannopyranoside

Conditions

Conditions	Yield
Stage #1: phenyl 2,3,4,6-tetra-O-acetyl-1-thio-α-D-mannopyranoside; 1-chloro-3-hydroxypropane In dichloromethane at 25℃; for 0.5h; Molecular sieve; Inert atmosphere; Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 25℃; for 1h; Molecular sieve; Inert atmosphere; Stage #3: With acetic anhydride In dichloromethane at 25℃; for 0.5h; Molecular sieve; Inert atmosphere;	98%

Yield

Stage #1: phenyl 2,3,4,6-tetra-O-acetyl-1-thio-α-D-mannopyranoside; 1-chloro-3-hydroxypropane In dichloromethane at 25℃; for 0.5h; Molecular sieve; Inert atmosphere;
Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 25℃; for 1h; Molecular sieve; Inert atmosphere;
Stage #3: With acetic anhydride In dichloromethane at 25℃; for 0.5h; Molecular sieve; Inert atmosphere;

98%

: 80-09-1
4,4'-sulfonediphenol

: 627-30-5
1-chloro-3-hydroxypropane

: C18H22O6S

Conditions

Conditions	Yield
With potassium hydroxide In ethanol at 70℃; for 24h;	98%

: 116-11-0
2-Methoxypropene

: 24057-28-1
pyridinium p-toluenesulfonate

: 627-30-5
1-chloro-3-hydroxypropane

: 149741-67-3
1-chloro-3-(1-methoxy-1-methylethoxy)-propane

Conditions

Conditions	Yield
	97.4%

...Expand

: 100-44-7
benzyl chloride

: 627-30-5
1-chloro-3-hydroxypropane

: 26420-79-1
1-chloro-3-benzyloxypropane

Conditions

Conditions	Yield
With sodium hydride In N,N-dimethyl-formamide for 1.5h; Ambient temperature;	97%

: 116-11-0
2-Methoxypropene

: 627-30-5
1-chloro-3-hydroxypropane

A: 30453-37-3
2,2-bis-(3-chloro-propoxy)-propane

B: 1-chloro-3-(1-methoxy-1-methylethoxy)-propane

Conditions

Conditions	Yield
With pyridinium p-toluenesulfonate at -65 - -60℃; for 1h;	A 2% B 97%

...Expand

: 35787-71-4
thianthrene cation radical perchlorate

: 627-30-5
1-chloro-3-hydroxypropane

A: thianthrenium perchlorate

B: 5-(3-Chloro-propoxy)-thianthren-5-ium; perchlorate

Conditions

Conditions	Yield
In dichloromethane for 26h; Ambient temperature;	A n/a B 97%

...Expand

: 55791-06-5
benzyl mesylate

: 627-30-5
1-chloro-3-hydroxypropane

: 26420-79-1
1-chloro-3-benzyloxypropane

Conditions

Conditions	Yield
With magnesium oxide; lithium trifluoromethanesulfonate; lithium tetrakis(pentafluorophenyl)borate In dichloromethane; cyclohexane at 20℃; for 24h;	97%