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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 3-Chloropropionic Acid supplier in China

Cas:107-94-8

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

3-Chloropropionic Acid

Cas:107-94-8

Min.Order:1 Pound

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-chloropropionic acid

Cas:107-94-8

Min.Order:1

Negotiable

Type:Other

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

3-Chloropropionic acid

Cas:107-94-8

Min.Order:1 Kilogram

FOB Price: $4.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Chloropropionic acid

Cas:107-94-8

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

3-Chloropropionic acid

Cas:107-94-8

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

TIANFU-CHEM_3-Chloropropionic acid,107-94-8

Cas:107-94-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

3-Chloropropionic acid CAS NO.107-94-8

Cas:107-94-8

Min.Order:10 Gram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Chlorpropionic acid

Cas:107-94-8

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 3-Chloropropionic Acid

Cas:107-94-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: 3-Chloropropionic Acid CAS No.:107-94-8 Molecule Formula:C3H4ClO2 Molecule Weight:107.52 Purity: 98.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard

Best Quality 3-Chloropropionic Acid

Cas:107-94-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

3-Chloropropionic acidCAS NO.: 107-94-8

Cas:107-94-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:White crystals Storage:Airtight, moisture-proof, anti-leaching, anti-high temperature Package:as per your request Application:Used as Pharmaceutical Intermediates Transportation:as p

3-Chloropropionic acid

Cas:107-94-8

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

Propanoic acid,3-chloro-

Cas:107-94-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

3-Chloropropionic Acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory supply CAS 107-94-8 with competitive price

Cas:107-94-8

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Propanoic acid,3-chloro-

Cas:107-94-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Other

inquiry

Hubei Langyou International Trading Co., Ltd

Factory Supply 98% Synthesis Intermediate 3-Chloropropionic Acid Best Raw Powder Application:Factory Supply 98% Synthesis Intermediate 3-Chloropropionic Acid Best Raw Powder

Luyunjia Chemistry Xiamen Limited

Xiamen Luyunjia Trading Co.,Ltd Package:1kg/bag; 947kg/drum, or as customer's request. Application:Xiamen Luyunjia Trading Co.,Ltd Transportation:DHL, EMS, FedEx, TNT, AIR, SEA Port:Beijing,Shanghai,Guangzhou ,China main port

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

107-94-8 Application:intermediate

3-Chloropropionic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

Factory Supply 98% Synthesis Intermediate 3-Chloropropionic Acid Best Raw PowderAppearance:White crystalline Storage:Store below +30°C. Package:foil bag,drum,fluoride bottle and so on Application:synthesis intermediates for antiepileptic drug Transpo

Factory Supply 98% Synthesis Intermediate 3-Chloropropionic Acid Best Raw Powder

Cas:107-94-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Chloropropionic acid 107-94-8

Cas:107-94-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Bide Pharmatech Ltd

Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical

3-Chloropropanoic acid

Cas:107-94-8

Min.Order:0

Negotiable

Type:Other

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#107-94-8;CAT#A801783

Cas:107-94-8

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

3-Chloropropionitrile
542-76-7

3-Chloropropionitrile

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With benzene-1,2-dicarboxylic acid for 0.75h; microwave irradiation;91%
With benzene-1,2-dicarboxylic acid at 240℃; under 3040 Torr; for 1h;72%
With hydrogenchloride
With water In dimethyl sulfoxide at 26℃; for 72h; pH=7; aq. phosphate buffer;25 %Chromat.
2-chloropropionyl chloride
625-36-5

2-chloropropionyl chloride

benzylamine
100-46-9

benzylamine

A

chloropropionic acid
107-94-8

chloropropionic acid

B

N-benzylacrylamide
13304-62-6

N-benzylacrylamide

C

Beclamide
501-68-8

Beclamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100℃; for 0.0833333h; Temperature; Concentration;A 6%
B 5%
C 89%
2-chloropropionyl chloride
625-36-5

2-chloropropionyl chloride

benzylamine
100-46-9

benzylamine

A

chloropropionic acid
107-94-8

chloropropionic acid

B

Beclamide
501-68-8

Beclamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 50℃; for 0.0166667h; Time;A 22%
B 78%
propionic acid
802294-64-0

propionic acid

A

3-Bromopropionic acid
590-92-1

3-Bromopropionic acid

B

chloropropionic acid
107-94-8

chloropropionic acid

C

2-Bromopropionic acid
598-72-1

2-Bromopropionic acid

D

(R,S)-2-chloropropionic acid
598-78-7

(R,S)-2-chloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride; oxygen; potassium bromide; sodium nitrite In chloroform; water at 40℃; under 760.051 Torr; for 18h; Sealed tube; Irradiation;A 65%
B n/a
C 23%
D n/a
acrylic acid
79-10-7

acrylic acid

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride at 65 - 70℃; for 4h;32.3%
With hydrogenchloride
With hydrogenchloride at 12℃;
β-Propiolactone
57-57-8

β-Propiolactone

benzylmagnesium chloride
6921-34-2

benzylmagnesium chloride

A

chloropropionic acid
107-94-8

chloropropionic acid

B

4-Phenylbutyric acid
1821-12-1

4-Phenylbutyric acid

β-Propiolactone
57-57-8

β-Propiolactone

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride; sodium chloride at 30 - 45℃;
With hydrogenchloride
3-chloropropanaldehyde
19434-65-2

3-chloropropanaldehyde

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With nitric acid
With nitric acid
3-iodopropanoic acid
141-76-4

3-iodopropanoic acid

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With chlorine
1,1,1,3-tetrachloropropane
1070-78-6

1,1,1,3-tetrachloropropane

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With sulfuric acid
propionyl chloride
79-03-8

propionyl chloride

propionic acid
802294-64-0

propionic acid

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
at 75 - 80℃; unter Belichtung;
propionic acid
802294-64-0

propionic acid

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With tetrachloromethane; sulfuryl dichloride; dibenzoyl peroxide
With chlorine at 400℃; in der Dampfphase;
With tetrachloromethane; sulfuryl dichloride; dibenzoyl peroxide
With chlorine at 120℃; in fluessiges Phase;
With chlorine at 30 - 60℃; unter Belichtung;
propionic acid
802294-64-0

propionic acid

A

chloropropionic acid
107-94-8

chloropropionic acid

B

(R,S)-2-chloropropionic acid
598-78-7

(R,S)-2-chloropropionic acid

Conditions
ConditionsYield
With chlorine Irradiation.im UV-Licht;
With hydrogenchloride Electrolysis.an einer Platinanode;
With hydrogenchloride Electrolysis.an Platinanode;
propionic acid
802294-64-0

propionic acid

A

chloropropionic acid
107-94-8

chloropropionic acid

B

2,3-dichloropropanoic acid
565-64-0

2,3-dichloropropanoic acid

C

(R,S)-2-chloropropionic acid
598-78-7

(R,S)-2-chloropropionic acid

Conditions
ConditionsYield
beim Chlorieren in der fluessigen Phase unter Belichtung;
acrylonitrile
107-13-1

acrylonitrile

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride bei Siedetemperatur;
3-Hydroxypropionitrile
109-78-4

3-Hydroxypropionitrile

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride
With hydrogenchloride at 100℃;
With hydrogenchloride und Kochen des Reaktionsgemisches unter weiterem Durchleiten von Chlorwasserstoff;
With hydrogenchloride; water und Kochen des Reaktionsgemisches unter weiterem Durchleiten von Chlorwasserstoff;
2-chloropropionyl chloride
625-36-5

2-chloropropionyl chloride

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride
1-chloro-3-hydroxypropane
627-30-5

1-chloro-3-hydroxypropane

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With nitric acid
With alkaline KMNO4
With nitric acid
With oxygen; sodium hydroxide In water at 60℃; under 8258.9 Torr; Kinetics; Autoclave;
3-hydroxypropionic acid
503-66-2

3-hydroxypropionic acid

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With hydrogenchloride at 120℃;
3-Bromopropionic acid
590-92-1

3-Bromopropionic acid

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With lithium chloride In dimethyl sulfoxide at 100℃; for 6h;
3-chloroperpropionic acid
40861-09-4

3-chloroperpropionic acid

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
With benzonitrile; (5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride at 30℃; Rate constant;
3,12-bis(3'-bromo-1'-oxopropyl)-3,12-diaza-6,9-diazoniadispiro<5.2.5.2>hexadecane dichloride
86641-76-1

3,12-bis(3'-bromo-1'-oxopropyl)-3,12-diaza-6,9-diazoniadispiro<5.2.5.2>hexadecane dichloride

A

3-Bromopropionic acid
590-92-1

3-Bromopropionic acid

B

chloropropionic acid
107-94-8

chloropropionic acid

C

3,12-bis(3'-chloro-1'-oxopropyl)-3,12-diaza-6,9-diazoniadispiro<5.2.5.2>hexadecane dibromide
121051-82-9

3,12-bis(3'-chloro-1'-oxopropyl)-3,12-diaza-6,9-diazoniadispiro<5.2.5.2>hexadecane dibromide

D

3,12-Bisacrylyl-3,12-diaza-6,9-diazoniadispiro<5,2,5,2>hexadecane dichloride
95461-34-0

3,12-Bisacrylyl-3,12-diaza-6,9-diazoniadispiro<5,2,5,2>hexadecane dichloride

E

3,12-bis(3'-hydroxy-1'-oxopropyl)-3,12-diaza-6,9-diazoniadispiro<5.2.5.2>hexadecane dichloride
122842-21-1

3,12-bis(3'-hydroxy-1'-oxopropyl)-3,12-diaza-6,9-diazoniadispiro<5.2.5.2>hexadecane dichloride

F

3-hydroxypropionic acid
503-66-2

3-hydroxypropionic acid

Conditions
ConditionsYield
In water at 70℃; for 5h; Product distribution; Kinetics; Rate constant; various time; other temperature;
ethyl 3-chloropropanoate
623-71-2

ethyl 3-chloropropanoate

A

chloropropionic acid
107-94-8

chloropropionic acid

B

ethene
74-85-1

ethene

Conditions
ConditionsYield
In gas at 360 - 420℃; under 49 - 209 Torr; Rate constant; Kinetics; Thermodynamic data; E(act);
4,4'-Di-tert-butyldiphenyliodonium chloride
5421-53-4

4,4'-Di-tert-butyldiphenyliodonium chloride

A

chloropropionic acid
107-94-8

chloropropionic acid

B

tert-butylbenzene
253185-03-4, 253185-04-5

tert-butylbenzene

C

1-tert-butyl-4-iodobenzene
35779-04-5

1-tert-butyl-4-iodobenzene

D

4-(tert-butyl)chlorobenzene
3972-56-3

4-(tert-butyl)chlorobenzene

Conditions
ConditionsYield
With (+)-cis-dioxolane; 2,2'-azobis(isobutyronitrile) at 75℃; for 7h; Product distribution; Quantum yield; various reaction conditions; also photochemical reaction;
1,3-Dichloropropane
142-28-9

1,3-Dichloropropane

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
Product distribution; dehalogenation; P. butanovora strain ml-15; aerobic condition; other bacterium strains; other halogeno alkanes;
3-Chloro-propionic acid 1-phenoxy-ethyl ester

3-Chloro-propionic acid 1-phenoxy-ethyl ester

A

chloropropionic acid
107-94-8

chloropropionic acid

B

acetaldehyde
75-07-0

acetaldehyde

C

phenol
108-95-2

phenol

Conditions
ConditionsYield
With water In acetonitrile Rate constant; var. pH;
β-Propiolactone
57-57-8

β-Propiolactone

water
7732-18-5

water

NaCl

NaCl

chloropropionic acid
107-94-8

chloropropionic acid

hydrogenchloride
7647-01-0

hydrogenchloride

acrylonitrile
107-13-1

acrylonitrile

chloropropionic acid
107-94-8

chloropropionic acid

hydrogenchloride
7647-01-0

hydrogenchloride

3-Hydroxypropionitrile
109-78-4

3-Hydroxypropionitrile

chloropropionic acid
107-94-8

chloropropionic acid

Conditions
ConditionsYield
at 100℃;
bei nachfolgenden Kochen unter weiterem Durchleiten von Chlorwasserstoff;analog verlauft die Einw. von Bromwasserstoff u Jodwasserstoff;
Conditions
ConditionsYield
Stage #1: chloropropionic acid With (chloro-phenylthio-methylene)dimethylammonium chloride In dichloromethane at 0℃; for 0.5h;
Stage #2: 2,4-dimethylcyclohexan-1-ol In dichloromethane at 20℃; for 12h;
100%
chloropropionic acid
107-94-8

chloropropionic acid

2,5-Difluorothiophenol
77380-28-0

2,5-Difluorothiophenol

3-((2,5-difluorophenyl)thio)propanoic acid
926232-57-7

3-((2,5-difluorophenyl)thio)propanoic acid

Conditions
ConditionsYield
Stage #1: 2,5-Difluorothiophenol With sodium hydroxide In water at 0℃; for 0.0833333h;
Stage #2: chloropropionic acid In water at 70℃;
Stage #3: With hydrogenchloride In water at 0℃;
100%
chloropropionic acid
107-94-8

chloropropionic acid

4-(6-hydroxyhexyl)benzoic acid
137757-24-5

4-(6-hydroxyhexyl)benzoic acid

4-{6-[(3-chloropropionyl)oxy]hexyl}benzoic acid

4-{6-[(3-chloropropionyl)oxy]hexyl}benzoic acid

Conditions
ConditionsYield
With toluene-4-sulfonic acid In dichloromethane at 50℃; for 18h; Dean-Stark;100%
chloropropionic acid
107-94-8

chloropropionic acid

ethanol
64-17-5

ethanol

ethyl 3-chloropropanoate
623-71-2

ethyl 3-chloropropanoate

Conditions
ConditionsYield
hydrogenchloride In water for 8h; Product distribution / selectivity;99%
With hydrogenchloride
With sulfuric acid
With sulfuric acid
chloropropionic acid
107-94-8

chloropropionic acid

3-chloropropanoic anhydride
20495-99-2

3-chloropropanoic anhydride

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide In dichloromethane at 20℃; Inert atmosphere; Glovebox;99%
With dicyclohexyl-carbodiimide for 0.0833333h;65 % Spectr.
chloropropionic acid
107-94-8

chloropropionic acid

2-amino-4-chloro-6-methyl-10,10-dioxo-10,11-dihydro-5-oxa-10λ6-thia-dibenzo[a,d]cycloheptene-8-carboxylic acid methyl ester
887003-12-5

2-amino-4-chloro-6-methyl-10,10-dioxo-10,11-dihydro-5-oxa-10λ6-thia-dibenzo[a,d]cycloheptene-8-carboxylic acid methyl ester

4-chloro-2-(3-chloro-propylamino)-6-methyl-10,10-dioxo-10,11-dihydro-5-oxa-10λ6-thia-dibenzo[a,d]cycloheptene-8-carboxylic acid methyl ester
887003-66-9

4-chloro-2-(3-chloro-propylamino)-6-methyl-10,10-dioxo-10,11-dihydro-5-oxa-10λ6-thia-dibenzo[a,d]cycloheptene-8-carboxylic acid methyl ester

Conditions
ConditionsYield
Stage #1: chloropropionic acid With sodium tetrahydroborate In tetrahydrofuran; benzene at 0 - 20℃; for 1h;
Stage #2: 2-amino-4-chloro-6-methyl-10,10-dioxo-10,11-dihydro-5-oxa-10λ6-thia-dibenzo[a,d]cycloheptene-8-carboxylic acid methyl ester In tetrahydrofuran; benzene for 3h; Heating / reflux;
99%
chloropropionic acid
107-94-8

chloropropionic acid

3-chloro-10,11-dihydro-5H-dibenzo[b,f]azepine
32943-25-2

3-chloro-10,11-dihydro-5H-dibenzo[b,f]azepine

C17H17Cl2N*ClH

C17H17Cl2N*ClH

Conditions
ConditionsYield
Stage #1: chloropropionic acid With sodium tetrahydroborate In toluene at 0 - 5℃;
Stage #2: 3-chloro-10,11-dihydro-5H-dibenzo[b,f]azepine With sodium tetrahydroborate In toluene at 25 - 80℃; for 7h;
Stage #3: With hydrogenchloride In water; isopropyl alcohol
99%
chloropropionic acid
107-94-8

chloropropionic acid

2-chloropropionyl chloride
625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With bis(trichloromethyl) carbonate In toluene at 25℃; for 8h; Reagent/catalyst; Temperature;98.5%
With thionyl chloride63%
With phosphorus trichloride
chloropropionic acid
107-94-8

chloropropionic acid

4-Chlororesorcinol
95-88-5

4-Chlororesorcinol

3-chloro-1-(5-chloro-2,4-dihydroxyphenyl)propan-1-one
1202889-56-2

3-chloro-1-(5-chloro-2,4-dihydroxyphenyl)propan-1-one

Conditions
ConditionsYield
Stage #1: 4-Chlororesorcinol With trifluorormethanesulfonic acid at 4 - 10℃;
Stage #2: chloropropionic acid at 10 - 55℃; Product distribution / selectivity;
98.4%
Stage #1: 4-Chlororesorcinol With trifluorormethanesulfonic acid at 4 - 10℃;
Stage #2: chloropropionic acid at 10 - 55℃; Product distribution / selectivity;
98.4%
1-methyl-1H-imidazole
616-47-7

1-methyl-1H-imidazole

chloropropionic acid
107-94-8

chloropropionic acid

1-(2-hydroxycarbonyl)ethyl-3-methyl-3H-imidazolium chloride

1-(2-hydroxycarbonyl)ethyl-3-methyl-3H-imidazolium chloride

Conditions
ConditionsYield
at 70℃; for 50h;98%
In toluene for 5h; Reflux; Inert atmosphere;86%
In toluene Schlenk technique;80%
In ethyl acetate at 70℃; for 24h;
chloropropionic acid
107-94-8

chloropropionic acid

1-azaphenothiazine
261-96-1

1-azaphenothiazine

10-(3-chloropropyl)-10H-benzo[b]pyrido[2,3-e][1,4]thiazine hydrochloride

10-(3-chloropropyl)-10H-benzo[b]pyrido[2,3-e][1,4]thiazine hydrochloride

Conditions
ConditionsYield
Stage #1: chloropropionic acid With sodium tetrahydroborate In toluene at 0 - 5℃;
Stage #2: 1-azaphenothiazine With sodium tetrahydroborate In toluene at 25 - 75℃; for 6h;
Stage #3: With hydrogenchloride In water; isopropyl alcohol
98%
chloropropionic acid
107-94-8

chloropropionic acid

para-thiocresol
106-45-6

para-thiocresol

3-[(4-methylphenyl)thio]propionic acid
13739-35-0

3-[(4-methylphenyl)thio]propionic acid

Conditions
ConditionsYield
With sodium hydroxide In water for 0.5h; Microwave irradiation;97%
Stage #1: chloropropionic acid; para-thiocresol With potassium hydroxide; potassium carbonate In ethanol Reflux;
Stage #2: With hydrogenchloride In ethanol; water Large scale reaction;
77%
With sodium hydroxide
chloropropionic acid
107-94-8

chloropropionic acid

10H-phenothiazine
92-84-2

10H-phenothiazine

C15H14ClNS*ClH

C15H14ClNS*ClH

Conditions
ConditionsYield
Stage #1: chloropropionic acid With sodium tetrahydroborate In toluene at 0 - 5℃;
Stage #2: 10H-phenothiazine With sodium tetrahydroborate In toluene at 25 - 80℃; for 5h;
Stage #3: With hydrogenchloride In water; isopropyl alcohol
97%
chloropropionic acid
107-94-8

chloropropionic acid

10H-acridin-9-one
578-95-0

10H-acridin-9-one

3-(9-oxo-9,10-dihydro-10-acridinyl)propanoic acid
226424-38-0

3-(9-oxo-9,10-dihydro-10-acridinyl)propanoic acid

Conditions
ConditionsYield
With 1-ethyl-3-methylimidazolium hydroxide at 50℃; for 8h; Ionic liquid;95.9%
chloropropionic acid
107-94-8

chloropropionic acid

3-cyano-4-(dimethylformamidyl)-aniline

3-cyano-4-(dimethylformamidyl)-aniline

1-(3-chloropropionyl)-3-cyano-4-(dimethylformamidyl)aniline

1-(3-chloropropionyl)-3-cyano-4-(dimethylformamidyl)aniline

Conditions
ConditionsYield
With 4-methyl-morpholine In tetrahydrofuran at 0 - 5℃; for 1.75h;95.7%
chloropropionic acid
107-94-8

chloropropionic acid

4-sulfanylphenol
637-89-8

4-sulfanylphenol

3-[(4-hydroxyphenyl)sulfanyl]propanoic acid
30512-65-3

3-[(4-hydroxyphenyl)sulfanyl]propanoic acid

Conditions
ConditionsYield
With sodium hydroxide In water at 100℃; for 3h;95%
With potassium hydroxide In water at 80℃; for 2.5h; pH=12;
chloropropionic acid
107-94-8

chloropropionic acid

5-fluorobenzo[d]oxazole-2-thiol
13451-78-0

5-fluorobenzo[d]oxazole-2-thiol

3-((5-fluorobenzo[d]oxazol-2-yl)thio)propanoic acid

3-((5-fluorobenzo[d]oxazol-2-yl)thio)propanoic acid

Conditions
ConditionsYield
With caesium carbonate In acetonitrile at 100℃; for 1h; Microwave irradiation;95%
chloropropionic acid
107-94-8

chloropropionic acid

thiophenol
108-98-5

thiophenol

acide phenylthio-3 propanoique
5219-65-8

acide phenylthio-3 propanoique

Conditions
ConditionsYield
Stage #1: thiophenol With sodium hydroxide In water at 20℃;
Stage #2: chloropropionic acid In water for 4h; Reflux;
Stage #3: With hydrogenchloride In water at 20℃; pH=< 2;
94%
With potassium carbonate; potassium hydroxide In ethanol; water at 0℃; for 5h; Reflux;70%
Stage #1: chloropropionic acid; thiophenol With potassium hydroxide; potassium carbonate In ethanol Reflux;
Stage #2: With hydrogenchloride In ethanol; water
63%
chloropropionic acid
107-94-8

chloropropionic acid

4-Fluorothiophenol
371-42-6

4-Fluorothiophenol

3-(4-fluorophenylthio)propanoic acid
19543-85-2

3-(4-fluorophenylthio)propanoic acid

Conditions
ConditionsYield
Stage #1: 4-Fluorothiophenol With potassium hydroxide In ethanol; water at 60℃;
Stage #2: chloropropionic acid With potassium carbonate In ethanol; water at 20 - 96℃; for 5.5h;
94%
With potassium carbonate; potassium hydroxide In ethanol; water at 0℃; for 5h; Reflux;92%
Stage #1: chloropropionic acid; 4-Fluorothiophenol With potassium hydroxide; potassium carbonate In ethanol Reflux;
Stage #2: With hydrogenchloride In ethanol; water
90%
chloropropionic acid
107-94-8

chloropropionic acid

N,0-dimethylhydroxylamine
1117-97-1

N,0-dimethylhydroxylamine

3-chloro-N-methoxy-N-methylpropanamide
1062512-53-1

3-chloro-N-methoxy-N-methylpropanamide

Conditions
ConditionsYield
Stage #1: chloropropionic acid; N,0-dimethylhydroxylamine In toluene at 0℃; for 0.166667h;
Stage #2: With phosphorus trichloride In toluene at 20 - 60℃; for 0.5h;
94%
chloropropionic acid
107-94-8

chloropropionic acid

triphenylphosphine
603-35-0

triphenylphosphine

(2-carboxyethyl)triphenylphosphonium chloride
36626-29-6

(2-carboxyethyl)triphenylphosphonium chloride

Conditions
ConditionsYield
In toluene at 110℃; for 18h;93%
In xylene for 18h; Heating;89%
In 5,5-dimethyl-1,3-cyclohexadiene; water for 4h; Reflux;84%
chloropropionic acid
107-94-8

chloropropionic acid

recorcinol
108-46-3

recorcinol

2',4'-dihydroxy-3-chloropropiophenone
151884-07-0

2',4'-dihydroxy-3-chloropropiophenone

Conditions
ConditionsYield
With trifluorormethanesulfonic acid at 80℃; for 1h;92%
With trifluorormethanesulfonic acid at 80℃; for 1h;90%
With trifluorormethanesulfonic acid at 85℃; for 0.75h;86%
chloropropionic acid
107-94-8

chloropropionic acid

C6H18N3O3P
1062512-43-9

C6H18N3O3P

3-chloro-N-methoxy-N-methylpropanamide
1062512-53-1

3-chloro-N-methoxy-N-methylpropanamide

Conditions
ConditionsYield
In toluene at 60℃;92%
chloropropionic acid
107-94-8

chloropropionic acid

N-[2-((2-S-(4-methoxybenzyl)sulfanyl)ethyl)amino]acetyl-S-(4-methoxybenzyl)-2-aminoethanethiol
202582-35-2

N-[2-((2-S-(4-methoxybenzyl)sulfanyl)ethyl)amino]acetyl-S-(4-methoxybenzyl)-2-aminoethanethiol

C25H34N2O5S2

C25H34N2O5S2

Conditions
ConditionsYield
With triethylamine In acetonitrile at 80℃;92%
chloropropionic acid
107-94-8

chloropropionic acid

8-amino-6-(4-aminophenyl)-2-phenyl-1,2,4-triazolo[4,3-a]pyrazin-3(2H)-one

8-amino-6-(4-aminophenyl)-2-phenyl-1,2,4-triazolo[4,3-a]pyrazin-3(2H)-one

N-(4-(8-amino-3-oxo-2-phenyl-2,3-dihydro-1,2,4-triazolo-[4,3-a]pyrazin-6-yl)phenyl)acrylamide

N-(4-(8-amino-3-oxo-2-phenyl-2,3-dihydro-1,2,4-triazolo-[4,3-a]pyrazin-6-yl)phenyl)acrylamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 2h;92%
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃;22%
chloropropionic acid
107-94-8

chloropropionic acid

2-((trifluoromethyl)thio)benzo[d]isothiazol-3(2H)-one 1,1-dioxide

2-((trifluoromethyl)thio)benzo[d]isothiazol-3(2H)-one 1,1-dioxide

cyclohexene
110-83-8

cyclohexene

2-((trifluoromethyl)thio)cyclohexyl 3-chloropropanoate

2-((trifluoromethyl)thio)cyclohexyl 3-chloropropanoate

Conditions
ConditionsYield
With trifluorormethanesulfonic acid; bis(4-methoxyphenyl)selenide In hexane at 20℃; for 24h; Sealed tube;91%
pyridine
110-86-1

pyridine

chloropropionic acid
107-94-8

chloropropionic acid

1-(2-carboxy-ethyl)-pyridinium; chloride
15168-37-3

1-(2-carboxy-ethyl)-pyridinium; chloride

Conditions
ConditionsYield
at 70 - 80℃;90%
chloropropionic acid
107-94-8

chloropropionic acid

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

3-(diphenyl-phosphinoyl)-propionic acid
29874-10-0

3-(diphenyl-phosphinoyl)-propionic acid

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 50℃; for 1h;90%
(i) NaOEt, EtOH, (ii) /BRN= 1098495/; Multistep reaction;

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