99% Appearance:Colourless or light yellow liquid Storage:cool and dry warehouse Package:190KG/DRUM Application:Pharmaceutical intermediate Transportation:BY SEA Port:SHANGHAI, HANGZHOU, NINGBO
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 3-Hydroxypropionitrile
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Product Name: 3-Hydroxypropionitrile Synonyms: Glycol cyanohydrin;glycolcyanohydrin;Hydroxyacrylonitrile;Hydroxypropanenitrile;propanoicacid,3-hydroxy,nitrile;Propionitrile, 3-hydroxy-;USAF rh-7;usafrh-7 CAS: 109-78-4 MF: C3H5NO MW: 71.08 EINE
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inquiryName: 3-Hydroxypropionitrile CAS No. :109-78-4 Molecular formula: C3H5NO Molecular weight: 71.07790 Appearance:Colorless liquid Storage: Preserve in well-closed, light-resistant and airtight containers. Package: 25kgs/drum Application:used in th
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inquiryProduct Name: 3-Hydroxypropionitrile CAS: 109-78-4 MF: C3H5NO MW: 71.08 EINECS: 203-704-8 Mol File: 109-78-4.mol 3-Hydroxypropionitrile Structure 3-Hydroxypropionitrile Chemical Properties Melting point -46 °C (lit.) Boili
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inquiry3-Hydroxypropionitrile CAS:109-78-4 Specification Product Name 3-Hydroxypropionitrile CAS No. 109-78-4 Appearance Colorless viscous liquid Assay
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inquiryConditions | Yield |
---|---|
With sodium sulfide; benzyltri(n-butyl)ammonium chloride In water for 0.166667h; | A 98% B n/a |
Conditions | Yield |
---|---|
With aluminum oxide; boron trifluoride diethyl etherate In propylene glycol at -10 - 10℃; for 28h; Reagent/catalyst; Temperature; | 97.3% |
Conditions | Yield |
---|---|
With PEG400 for 6h; Heating; | 93% |
Conditions | Yield |
---|---|
With sodium hydroxide at 50℃; for 0.2h; | 92% |
With sodium hydroxide In water at 50℃; for 4h; | 65% |
With water; copper(II) oxide |
3-((tetrahydro-2H-pyran-2-yl)oxy)propanenitrile
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With silica-supported NaHSO4 In methanol at 20℃; for 0.25h; | 92% |
With zinc(II) trifluoromethanesulfonate In methanol at 20℃; for 0.666667h; | 81% |
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite at 20℃; for 18h; Green chemistry; chemoselective reaction; | 84% |
Conditions | Yield |
---|---|
With sodium iodide In ethanol for 5h; Heating; | 80% |
at 100℃; | |
With ethanol |
3-(1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilan-2-yl)propanenitrile
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With 2,3-dimethyl-1,4-benzoquinone; tetrabutyl ammonium fluoride; oxygen In tetrahydrofuran for 0.833333h; Ambient temperature; | 71% |
acrylonitrile
phenol
A
3-phenoxypropionitrile
B
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With tetramethyl ammoniumhydroxide In water at 60℃; for 0.5h; Temperature; Reagent/catalyst; Time; Michael Addition; Microwave irradiation; | A 68% B n/a |
Conditions | Yield |
---|---|
With lithium hypochlorite In water Ambient temperature; | A 9.8% B 60% |
With lithium hypochlorite In water Product distribution; Mechanism; Ambient temperature; other solvent and additives; var. cyclopropanamines; | A 9.8% B 60% |
Conditions | Yield |
---|---|
With lithium aluminium hydride on silica gel In diethyl ether for 3h; Heating; | 54% |
bromopropionitrile
A
acetic acid
B
acrylonitrile
C
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With oxygen; tetraethylammonium perchlorate In N,N-dimethyl-formamide at 20℃; electroreduction at -1.1 V; | A 40 % Chromat. B 10 % Chromat. C 36% |
Conditions | Yield |
---|---|
With lithium hypochlorite In water Ambient temperature; | A 15% B 30 mg |
copper
acrylonitrile
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
In water | 1.3% |
Conditions | Yield |
---|---|
(i) NaN3, H2O, (ii) Pd, 2,5-dimethyl-hex-3-yne-2,5-diol, benzene; Multistep reaction; |
methyl 1-aminocyclopropane-1-carboxylate
A
ethene
B
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With lithium hypochlorite In water at 5 - 10℃; for 0.333333h; |
Conditions | Yield |
---|---|
With sodium hydroxide; Pt(Ppy3)4; water at 80℃; for 1h; Product distribution; var. platinum(0) catalysts; | |
at 70℃; for 8h; Product distribution; The selective hydration with several metal oxide catalysts.; | |
manganese(IV) oxide at 70℃; for 8h; Yield given; |
acrylonitrile
A
2-cyanoethyl ether
B
2-propenamide
C
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
trans- at 80℃; Mechanism; Rate constant; Product distribution; in the absence or in the presence of different quantity of water; | |
trans- at 25℃; Rate constant; Product distribution; also in the presence of different quantity of acetamide; | |
sodium hydroxide In water at 80℃; Product distribution; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol for 16h; |
N-nitro-β-aminopropionitrile
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With sulfuric acid at 25 - 85℃; Kinetics; Mechanism; Thermodynamic data; ΔH(excit.), -ΔS(excit.); |
furfural
water
N-benzyl-trimethylammonium hydroxide
acrylonitrile
A
bis-(2-cyano-3ξ-[2]furyl-allyl)-ether
B
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
at 20℃; Kinetics; | |
at 40℃; Kinetics; |
acrylonitrile
A
2-cyanoethyl ether
B
2-propenamide
C
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With water; Ni(b),Cu(35) (X%) at 75℃; for 6h; Product distribution; Thermodynamic data; other time and catalyst composition; ΔE(excit); effect on the rate and product distribution; |
Conditions | Yield |
---|---|
Reaktion von Calciumcyanid; | |
Reaktion von Calciumcyanid; |
oxirane
hydrogen cyanide
sodium cyanide
water
3-Hydroxypropionitrile
3-Hydroxypropionitrile
3-hydroxypropanimidamide hydrochloride
Conditions | Yield |
---|---|
Stage #1: 3-Hydroxypropionitrile With acetyl chloride In methanol; toluene at 0 - 20℃; for 18h; Stage #2: With ammonia In methanol at 0 - 20℃; for 18h; | 100% |
With hydrogenchloride; methanol; diethyl ether Umsetzen des Reaktionsprodukts mit NH3 in Metahnol bei 0grad; |
3-Hydroxypropionitrile
5'-O-(4,4'-dimethoxytrityl)thymidin-3'-yl-(N,N-diisopropylamino)phosphorofluoridite
O-[5'-O-(4,4'-dimethoxytrityl)thymidin-3'-yl] O-(2-cyanoethyl) phosphorofluoridite
Conditions | Yield |
---|---|
With 1H-tetrazole In acetonitrile for 0.166667h; Ambient temperature; | 100% |
3-Hydroxypropionitrile
O-(5'-O-(4,4'-dimethoxytrityl)-N6-benzoyl-2-deoxyadenosin-3'-yl) N,N-diisopropylfluorophosphoramidite
Phosphorofluoridous acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester
Conditions | Yield |
---|---|
With 1H-tetrazole In acetonitrile for 0.166667h; Ambient temperature; | 100% |
bis(trichloromethyl) carbonate
3-Hydroxypropionitrile
β-cyanoethyl chlorocarbonate
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate; 3-Hydroxypropionitrile In tetrahydrofuran at 0 - 20℃; Stage #2: With pyridine In tetrahydrofuran at 0 - 20℃; | 100% |
In pyridine; toluene at 0℃; |
tert-butyldimethylsilyl chloride
3-Hydroxypropionitrile
3-((tert-butyldimethylsilyl)oxy)propanenitrile
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 30℃; | 100% |
With 1H-imidazole In tetrahydrofuran at 40℃; for 15h; Condensation; | 98% |
With 1H-imidazole In dichloromethane at 20℃; | 94% |
triisopropylsilyl chloride
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 16h; | 100% |
Conditions | Yield |
---|---|
In dichloromethane for 1h; | 100% |
(1'S)-1-(1'-phenylethyl)-3,4-epoxypyrrolidine
tert-butyl methyl ether
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With sodium methylate In methanol; water | 100% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
Stage #1: 3-Hydroxypropionitrile With acetyl chloride In methanol; toluene at 0 - 20℃; for 18h; Stage #2: With ammonia In tetrahydrofuran; methanol at 0 - 20℃; for 18h; | 100% |
3-Hydroxypropionitrile
1-<3-(N-tert-butoxycarbonylamino)propyl>-4-phenylpiperidine-4-carboxylic acid
1-N-(tert-butoxycarbonyl)-3-<4-(2-cyanoethoxycarbonyl)-4-phenylpiperidin-1-yl>propylamine
Conditions | Yield |
---|---|
With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane for 16h; Heating; | 99% |
Conditions | Yield |
---|---|
With Iron(III) isopropoxide; zirconium(IV) tetraisopropoxide In n-heptane for 23h; | 99% |
tetrachlorobis(tetrahydrofuran)hafnium(IV) In toluene for 24h; Heating; | 94% |
zirconium(IV) oxychloride In n-heptane for 5h; Heating; |
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 65℃; | 99% |
5-methyl-1,2,3-thiadiazolyl-4-carboxylic acid
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In 1,2-dichloro-ethane at 0 - 20℃; for 3.5h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; for 12h; Inert atmosphere; | 99% |
chloro-trimethyl-silane
3-Hydroxypropionitrile
3-trimethylsilanyloxypropionitrile
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 0 - 23℃; for 16.3333h; | 98% |
Stage #1: 3-Hydroxypropionitrile With triethylamine at 0℃; Stage #2: chloro-trimethyl-silane In diethyl ether at 0℃; for 0.583333h; | 98.5% |
With triethylamine In diethyl ether at 0 - 23℃; for 16h; Inert atmosphere; Schlenk technique; | 98% |
2,2,6-trimethyl-4H-1,3-dioxin-4-one
3-Hydroxypropionitrile
2-cyanoethylacetoacetate
Conditions | Yield |
---|---|
In o-xylene at 141℃; for 2h; | 98.3% |
In 5,5-dimethyl-1,3-cyclohexadiene at 140 - 145℃; for 1h; | 90% |
In xylene at 140 - 145℃; for 1h; | 81.6% |
Conditions | Yield |
---|---|
With manganese(IV) oxide; water In isopropyl alcohol at 100℃; under 5171.62 Torr; for 0.833333h; | 98% |
With CF3O3S(1-)*C36H35ClFeOP3Pt(1+); water; silver trifluoromethanesulfonate In tetrahydrofuran at 40℃; for 12h; Catalytic behavior; Inert atmosphere; | 92% |
With silver tetrafluoroborate; C36H35ClFeOP3Pt(1+)*BF4(1-) In tetrahydrofuran; water at 80℃; for 12h; | 92% |
Conditions | Yield |
---|---|
With ammonium hydroxide; hydrogen; silver nitrate In methanol at 45 - 75℃; under 1500.15 Torr; Temperature; High pressure; Inert atmosphere; Autoclave; | 98% |
With hydrogen; nickel In isopropyl alcohol at 60℃; under 3102.9 Torr; 20-24 h; | 88% |
With ammonium hydroxide; hydrogen at 80℃; under 60006 Torr; for 6h; Sealed tube; | 80% |
3-Hydroxypropionitrile
2-chlorophenyl dichlorophosphate
2-chlorophenyl bis<2-cyanoethyl>phosphate
Conditions | Yield |
---|---|
With pyridine In 1,4-dioxane for 4.5h; Ambient temperature; | 98% |
2-(carboxymethyl)-5-nitrobenzoic acid
3-Hydroxypropionitrile
2-(2-cyano-ethoxycarbonylmethyl)-5-nitro-benzoic acid
Conditions | Yield |
---|---|
With sulfuric acid at 70℃; for 0.116667h; | 98% |
1-benzyloxycarbonylpiperidine-4-carboxylic acid
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 5h; Ambient temperature; | 97% |
1,1,1,3,3,3-hexamethyl-disilazane
3-Hydroxypropionitrile
3-trimethylsilanyloxypropionitrile
Conditions | Yield |
---|---|
With ammonium thiocyanate In dichloromethane at 0℃; for 0.166667h; | 97% |
at 135℃; for 2h; | 167 g |
toluene-4-sulfonic acid at 100℃; for 2.5h; | |
toluene-4-sulfonic acid at 60 - 80℃; for 2.5 - 4.5h; |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 0℃; for 2h; | 97% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane; N,N-dimethyl-formamide Ambient temperature; | 88% |
3-Hydroxypropionitrile
O-(2-thiono-1,3,2-oxathiaphospholanyl)-N-(tert-butoxycarbonyl)serine methyl ester
2-tert-butoxycarbonylamino-3-[(2-cyano-ethoxy)-mercapto-phosphoryloxy]-propionic acid methyl ester
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 3h; | 97% |
ethanol
3-Hydroxypropionitrile
Ethyl 3-hydroxypropionimidate hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether at 20℃; for 3h; Pinner Imino Ether Synthesis; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
dirhodium tetraacetate In chloroform | 96% |
3-Hydroxypropionitrile
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 3h; | 96% |
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