Sichuan Tongsheng is the most strongest manufacturer and exporter of amino acids and their derivatives in China, we have the best quality and price. Guarantee high quality, competive price and reliable service. We fully compliance with ISO9001:2008,
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:4530-20-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWhy is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c
Cas:4530-20-5
Min.Order:25 Kilogram
Negotiable
Type:Trading Company
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:4530-20-5
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
Cas:4530-20-5
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryManufacturer supply BOC-Glycine CAS 4530-20-5 with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed a
Cas:4530-20-5
Min.Order:10 Kilogram
FOB Price: $10.0
Type:Trading Company
inquiryHebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
high quality Appearance:White or off white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:4530-20-5
Min.Order:1
Negotiable
Type:Other
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:4530-20-5
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:4530-20-5
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryBOC-Glycine 4530-20-5 BOC-Glycine Basic information Product Name: BOC-Glycine Synonyms: BOC-GLYCINE-OH;BOC-GLY;BOC-GLYCINE;BOC-GLY-OH;BOC-L-GLY;BOC-AMINOXYACETIC ACID;N-T-BOC-GLYCINE;N
Cas:4530-20-5
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:4530-20-5
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:4530-20-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryProduct name BOC-Glycine Alias N-(tert-Butoxycarbonyl)glycine; N-Boc-glycine; Boc-Gly-OH~N-(tert-Butoxycarbonyl)glycine; NtertButoxycarbonylglycine; Boc-Gly-OH; [(tert-butoxycarbonyl)amino]acetate;
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:4530-20-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:4530-20-5
Min.Order:1 Kilogram
FOB Price: $75.0 / 100.0
Type:Trading Company
inquiryBOC-Glycine CAS:4530-20-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:4530-20-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and als
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:4530-20-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHigh purity BOC-Gly-OH 4530-20-5 in stock immediately delivery good supplierAppearance:Powder Storage:Dry and ventilated Package:according to customers' requirements Application:APIs Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(
Cas:4530-20-5
Min.Order:1 Gram
Negotiable
Type:Other
inquirymoderate price & quick delivery Appearance:White To Off-White Powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used in the composition
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane; water at 20℃; for 12h; | 100% |
Stage #1: glycine With sodium hydroxide In 1,4-dioxane; water at 0℃; for 0.25h; Stage #2: di-tert-butyl dicarbonate In 1,4-dioxane; water at 0 - 20℃; | 100% |
With sodium hydroxide In 1,4-dioxane | 100% |
2-oxo-2-phenylethyl 2-(tert-butoxycarbonylamino)acetate
A
BOC-glycine
B
acetophenone
Conditions | Yield |
---|---|
With N,N,N',N'-tetramethyl-o-phenylenediamine In acetonitrile for 2h; Irradiation; | A 100% B n/a |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal for 3h; | A 100% B n/a |
A
BOC-glycine
B
C16H10O3S
Conditions | Yield |
---|---|
In chloroform-d1 for 0.25h; Solvent; Photolysis; Inert atmosphere; | A 97% B n/a |
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane at 20℃; for 8h; | 95% |
Conditions | Yield |
---|---|
With sodium hydroxide In water; acetone at 25℃; for 12h; | 94% |
(N-hydroxy-5-norbornene-2,3-diformylimino)tert-butyl ester
glycine
BOC-glycine
Conditions | Yield |
---|---|
With tertiary amine In 1,4-dioxane; water for 3h; | 85% |
tert-butyl 4,6-dimethoxy-1,3,5-triazinyl carbonate
glycine
BOC-glycine
Conditions | Yield |
---|---|
With triethylamine In methanol at 20℃; for 0.5h; | 85% |
4-nitrobenzyl N-(tert-butoxycarbonyl)glycinate
BOC-glycine
Conditions | Yield |
---|---|
With sodium dithionite; sodium carbonate In acetonitrile | 80% |
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane; water for 0.166667h; Ambient temperature; | 80% |
2-oxo-2-phenylethyl 2-(tert-butoxycarbonylamino)acetate
A
BOC-glycine
B
(tert-butoxycarbonyl)glycine hydrazide
Conditions | Yield |
---|---|
With hydrazine hydrate In methanol Product distribution; | A 75% B 12% |
N-Boc-glycine 2-(2-acetylphenyl)-1-methylethyl ester
BOC-glycine
Conditions | Yield |
---|---|
In acetonitrile for 3h; Photolysis; | 73% |
(E)-3-methoxyallyl 2-((tert-butoxycarbonyl)amino)acetate
BOC-glycine
Conditions | Yield |
---|---|
With zinc(II) chloride; lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 59% |
With potassium hexamethylsilazane; zinc(II) chloride In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 54% |
tert-Butoxycarbonylamino-acetic acid (2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl ester
glycine ethyl ester hydrochloride
A
BOC-glycine
B
N-tert-butoxycarbonyl glycyl glycine methyl ester
Conditions | Yield |
---|---|
With 4-methyl-morpholine In N,N-dimethyl-formamide at 38℃; for 96h; | A n/a B 57% |
glycine ethyl ester hydrochloride
2,3,4,6-tetra-O-benzyl-1-O-(N-tert-butoxycarbonyl-glycyl)-β-D-glucopyranose
A
BOC-glycine
B
N-tert-butoxycarbonyl glycyl glycine methyl ester
2,3,4,6-tetra-O-benzyl-D-glucopyranose
Conditions | Yield |
---|---|
With 4-methyl-morpholine In N,N-dimethyl-formamide at 38℃; for 96h; | A n/a B 55% C n/a |
Conditions | Yield |
---|---|
With sodium carbonate In water; acetonitrile at -5 - 20℃; | 35% |
Glycine tert-butyl ester
2-oxo-2-phenylethyl 2-(tert-butoxycarbonylamino)acetate
A
BOC-glycine
B
Boc-glycylglycine tert-butyl ester
Conditions | Yield |
---|---|
In ethyl acetate for 24h; Product distribution; Ambient temperature; | A 10% B 30% |
Conditions | Yield |
---|---|
With sodium hydroxide; tert-butyl alcohol |
Conditions | Yield |
---|---|
With toluene Erwaermen des Reaktionsprodukts mit tert-Butylalkohol und anschliessenden Hydrolyse; |
Conditions | Yield |
---|---|
With triethylamine Behandeln des Reaktionsprodukts mit wss.NaOH und Dioxan; |
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
Stage #1: BOC-glycine; benzylamine With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 0.0166667h; Stage #2: With HATU for 18h; | 100% |
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 99% |
With zirconium(IV) chloride In tetrahydrofuran at 70℃; for 24h; Molecular sieve; Inert atmosphere; | 99% |
BOC-glycine
methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride
Nα-tert-butoxycarbonylglycyl-Nε-benzyloxycarbonyl-L-lysine methyl ester
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at -20 - 20℃; for 4h; Acylation; | 100% |
Stage #1: BOC-glycine With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 0.5h; Cooling with ice; Stage #2: methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 92.2% |
(i) Et3N, ClCO2iBu, (ii) /BRN= 3578476/, Et3N; Multistep reaction; | |
With 4-methyl-morpholine; triethylamine; isobutyl chloroformate 1) THF, -10 deg C, 15 min, 2) THF, 12 h; Yield given. Multistep reaction; |
BOC-glycine
L-alanine benzyl ester p-toluenesulfonate
Boc-Gly-Ala-OBzl
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine | 100% |
With TEA; diphenyl phosphoryl azide In N,N-dimethyl-formamide 1.) 0 deg C, 4 h; 2.) r.t., overnight; | 85% |
Stage #1: BOC-glycine; L-alanine benzyl ester p-toluenesulfonate With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 0.166667h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h; Inert atmosphere; |
BOC-glycine
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride
(S)-1-(2-tert-butoxycarbonylaminoacetyl)pyrrolidine-2-carboxylic acid benzyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; triethylamine In chloroform | 100% |
With benzotriazol-1-ol; triethylamine In chloroform | 100% |
With benzotriazol-1-ol; triethylamine In chloroform | 100% |
BOC-glycine
L-valine benzyl ester p-toluenesulfonate salt
N-t-butoxycarbonylglycyl-L-valine benzyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine | 100% |
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 0 - 20℃; for 12h; Inert atmosphere; | 94% |
With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide 1.) 0 deg C, 2.) overnight, 4 deg C; | 89% |
With 4-methyl-morpholine; isobutyl chloroformate 1.) THF, -15 deg C, 2.) DMF, a) -15 deg C, 30 min, b) r.t., 30 min.; Yield given. Multistep reaction; |
BOC-glycine
(-)-8-phenylmenthol
(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl (tert-butoxycarbonyl)aminoacetate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 13h; | 100% |
Stage #1: BOC-glycine With dmap; dicyclohexyl-carbodiimide In dichloromethane at -30℃; for 0.166667h; Stage #2: (-)-8-phenylmenthol In dichloromethane for 20h; Heating; | 96% |
With dmap; dicyclohexyl-carbodiimide | 93% |
BOC-glycine
2-(N-tert-butoxycarbonylamino)ethanol
Conditions | Yield |
---|---|
Stage #1: BOC-glycine With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at -15℃; for 0.25h; Stage #2: With sodium tetrahydroborate In tetrahydrofuran; water at -15℃; for 1h; | 100% |
With diisopropoxytitanium(III) tetrahydroborate In dichloromethane for 4h; Ambient temperature; | 88% |
With sodium bis(2-methoxyethoxy)aluminium dihydride In tetrahydrofuran; toluene at 0℃; for 2h; | 77.1% |
BOC-glycine
benzyl bromide
tert-butoxycarbonylamino-acetic acid benzyl ester
Conditions | Yield |
---|---|
Stage #1: BOC-glycine With caesium carbonate In methanol pH=7; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 5h; Further stages.; | 100% |
Stage #1: BOC-glycine With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 0℃; for 18h; Further stages; | 100% |
With triethylamine In N,N-dimethyl-formamide at 25℃; for 5h; | 54% |
With caesium carbonate 1) MeOH, water, pH 7.0, 2) DMF, 5 h; Yield given. Multistep reaction; | |
With sodium iodide In acetone for 2h; Reflux; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0℃; for 1h; Stage #2: In tetrahydrofuran at 0℃; | 100% |
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃; Stage #2: With citric acid In water pH=2 - 3; | 100% |
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃; Stage #2: With citric acid In water pH=2 - 3; | 100% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 50℃; for 16h; | 100% |
With N-ethyl-N,N-diisopropylamine for 0.666667h; Reflux; | 91% |
With caesium carbonate In acetonitrile | 90% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 25℃; for 5h; | 100% |
With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 5h; | 99% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 6h; | 96.9% |
BOC-glycine
isobutyl chloroformate
N-(t-butoxycarbonyl)glycyl i-butyl carbonate
Conditions | Yield |
---|---|
With 4-methyl-morpholine In tetrahydrofuran at -15℃; for 0.0833333h; | 100% |
With 4-methyl-morpholine In tetrahydrofuran at -20℃; for 0.05h; |
BOC-glycine
tetrakis-5,10,15,20-(o-aminophenyl)porphyrin
Conditions | Yield |
---|---|
With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at -5 - 20℃; for 50h; Condensation; | 100% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane Inert atmosphere; Cooling with ice; | 62% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane |
Conditions | Yield |
---|---|
Stage #1: H-Ala-Glu(OBzl)-OBzl hydrochloride With triethylamine In dichloromethane Hydrolysis; Stage #2: BOC-glycine With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 0 - 25℃; for 14h; Condensation; | 100% |
BOC-glycine
phenethylamine
tert-butyl N-{[(2-phenylethyl)carbamoyl]methyl}carbamate
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In acetonitrile at 0 - 20℃; Acylation; | 100% |
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In ethyl acetate at 20℃; for 72h; | 94% |
Stage #1: BOC-glycine With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 1h; Stage #2: phenethylamine In dichloromethane for 16h; | 81% |
Stage #1: BOC-glycine With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: phenethylamine In N,N-dimethyl-formamide at 20℃; | 72% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 23℃; for 4h; Inert atmosphere; | 71% |
1-aza-18-crown-6
BOC-glycine
[2-oxo-2-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl)-ethyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With bis(trichloromethyl) carbonate; lutidine In tetrahydrofuran at 25 - 50℃; for 2h; | 100% |
With 2,6-dimethylpyridine; bis(trichloromethyl) carbonate In tetrahydrofuran Inert atmosphere; |
BOC-glycine
4-{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutyl]amino}benzyl alcohol
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 24h; | 100% |
BOC-glycine
4,6-O-di(tert-butyl)silanediyl-D-glucal
3-O-(N-tert-butoxycarbonyl-2'-amino-ethanoyl)-4,6-O-di-tert-butylsilanediyl-D-glucal
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane | 100% |
BOC-glycine
Propargylamine
tert-butyl (2-oxo-2-(prop-2-yn-1-ylamino)ethyl)carbamate
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 6h; Inert atmosphere; | 100% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 16h; Inert atmosphere; | 99% |
With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide In acetonitrile at 20℃; | 96% |
Conditions | Yield |
---|---|
Stage #1: BOC-glycine; anthranilic acid With pyridine; triphenyl phosphite at 150℃; for 0.166667h; microwave irradiation; Stage #2: 2-methoxyethylamine at 220℃; for 0.0666667h; microwave irradiation; | 100% |
Conditions | Yield |
---|---|
Stage #1: BOC-glycine; anthranilic acid With pyridine; triphenyl phosphite at 150℃; for 0.166667h; microwave irradiation; Stage #2: 2-methoxyethylamine at 180℃; for 0.05h; microwave irradiation; | 100% |
(3S,10R,16S)-16-{(1R)-3-[4-(hydroxymethyl)phenyl]-1-methylallyl}-3-isobutyl-10-(4-methoxybenzyl)-1-oxa-4,8,11-triazacyclohexadec-13-ene-2,5,9,12-tetraone
BOC-glycine
tert-butoxycarbonylamino-acetic acid 4-{3-[3-isobutyl-10-(4-methoxy-benzyl)-2,5,9,12-tetraoxo-1-oxa-4,8,11-triaza-cyclohexadec-13-en-16-yl]-but-1-enyl}-benzyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 3h; | 100% |
BOC-glycine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In dichloromethane for 3h; pH=9; | 100% |
BOC-glycine
2-(N-t-butoxycarbonylamino)thioacetamide
Conditions | Yield |
---|---|
With Lawessons reagent In dichloromethane at 25℃; for 16h; | 100% |
Stage #1: BOC-glycine With ammonium hydroxide; triethylamine; isobutyl chloroformate In tetrahydrofuran Stage #2: With tetraphosphorus decasulfide; sodium carbonate In tetrahydrofuran | 83% |
Multi-step reaction with 3 steps 1: Et3N / tetrahydrofuran / 0.42 h / -10 °C 2: aq. MH3 / tetrahydrofuran / 0.75 h / -10 °C 3: 85 percent / Lawesson's reagent / CH2Cl2 / 16 h / Ambient temperature View Scheme |
BOC-glycine
p-aminoiodobenzene
[(4-iodophenylcarbamoyl)methyl]carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With dacarbazine; dmap In dichloromethane | 100% |
With dmap; diisopropyl-carbodiimide In dichloromethane for 20h; Inert atmosphere; | 100% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 5h; | 98% |
BOC-glycine
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane | 100% |
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 5h; | 100% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View