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inquiry2,5-Difluoro thiophenol Application:2,5-Difluoro thiophenol
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Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Prompt reaction, good quality and best service make us reliable and outstanding in this industry.Appearance:Colorless to light yellow l
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inquiry2,5-Difluoro thiophenolAppearance:liquid Package:EMS, DHL, FEDEX, UPS, TNT Application:Intermediates/Pharmaceutical intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea
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inquiryStable supply of goods and provision of high-quality services Application:As raw materials in the field of medicine and biology
factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
2,5-difluorobenzenesulfonyl chloride
2,5-Difluorothiophenol
Conditions | Yield |
---|---|
With formic acid; 6% Pd/C; triphenylphosphine at 60℃; for 8h; | 87% |
With potassium formate at 200℃; for 7h; neat (no solvent); | 68% |
2,5-Difluorothiophenol
Conditions | Yield |
---|---|
With 6% Pd/C; iodine; triphenylphosphine; isopropyl alcohol for 10h; Reflux; | 85% |
2,5-difluoroaniline
2,5-Difluorothiophenol
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
chloropropionic acid
2,5-Difluorothiophenol
3-((2,5-difluorophenyl)thio)propanoic acid
Conditions | Yield |
---|---|
Stage #1: 2,5-Difluorothiophenol With sodium hydroxide In water at 0℃; for 0.0833333h; Stage #2: chloropropionic acid In water at 70℃; Stage #3: With hydrogenchloride In water at 0℃; | 100% |
2-Chloro-5-(trifluoromethylthio)benzaldehyde
2,5-Difluorothiophenol
5-(Trifluoromethylthio)-2-(2,5-difluorophenylthio)benzaldehyde
Conditions | Yield |
---|---|
With sodium hydroxide In N,N,N,N,N,N-hexamethylphosphoric triamide at 100℃; for 5.5h; | 75% |
2,5-dichloro-benzaldehyde
2,5-Difluorothiophenol
5-Chloro-2-(2,5-difluorophenylthio)benzaldehyde
Conditions | Yield |
---|---|
With sodium hydroxide In N,N,N,N,N,N-hexamethylphosphoric triamide at 100℃; for 5.5h; | 74% |
o-iodophenylacetic acid
2,5-Difluorothiophenol
<2-(2,5-difluorophenylthio)phenyl>acetic acid
Conditions | Yield |
---|---|
With potassium hydroxide; copper In water for 16h; Heating; | 64% |
2-bromo-5-methoxy-benzaldehyde
2,5-Difluorothiophenol
A
2-(2,5-difluorophenylthio)-5-hydroxybenzaldehyde
B
2-(2,5-Difluorophenylthio)-5-methoxybenzaldehyde
Conditions | Yield |
---|---|
With copper In N,N-dimethyl-formamide at 150℃; for 6h; | A 2.8 g B 39% |
2,5-Difluorothiophenol
(3-(benzyloxy)cyclobutyl)(2,5-difluorophenyl)sulfane
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; | 12% |
2,5-Difluorothiophenol
1,4-difluorodibenzothiepin
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 64 percent / KOH, Cu / H2O / 16 h / Heating 2: 3.60 g / polyphosphoric acid / 2.5 h / 120 - 125 °C 3: 94 percent / NaBH4, aq. NaOH / ethanol; benzene / 4 h / Heating 4: 97 percent / HCl, CaCl2 / benzene / Ambient temperature 5: 21 percent / CHCl3 / 8 h / Heating View Scheme |
2,5-Difluorothiophenol
6,9-difluorodibenzothiepin-10(11H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 64 percent / KOH, Cu / H2O / 16 h / Heating 2: 3.60 g / polyphosphoric acid / 2.5 h / 120 - 125 °C View Scheme |
2,5-Difluorothiophenol
8-chloro-2-fluoro-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 74 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg / 1) THF, 2) THF, reflux, 2 h 3: 1.75 g / NaH / dimethylformamide / 1) RT, 2 h; 2) 50 deg C, 14 h View Scheme |
2,5-Difluorothiophenol
11-chloro-1,4-difluoro-10,11-dihydrodibenzothiepin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 64 percent / KOH, Cu / H2O / 16 h / Heating 2: 3.60 g / polyphosphoric acid / 2.5 h / 120 - 125 °C 3: 94 percent / NaBH4, aq. NaOH / ethanol; benzene / 4 h / Heating 4: 97 percent / HCl, CaCl2 / benzene / Ambient temperature View Scheme |
2,5-Difluorothiophenol
6,9-difluoro-10,11-dihydrodibenzothiepin-10-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 64 percent / KOH, Cu / H2O / 16 h / Heating 2: 3.60 g / polyphosphoric acid / 2.5 h / 120 - 125 °C 3: 94 percent / NaBH4, aq. NaOH / ethanol; benzene / 4 h / Heating View Scheme |
2,5-Difluorothiophenol
2-fluoro-8-methoxy-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 39 percent / Cu / dimethylformamide / 6 h / 150 °C 2: 1) Mg / 1) THF, reflux, 1.5 h; 2) THF, reflux, 3 h 3: 1.06 g / NaH / dimethylformamide; tetrahydrofuran / 11 h / 70 °C View Scheme |
2,5-Difluorothiophenol
[5-Chloro-2-(2,5-difluoro-phenylsulfanyl)-phenyl]-(1-methyl-piperidin-4-yl)-methanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 74 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg / 1) THF, 2) THF, reflux, 2 h View Scheme |
2,5-Difluorothiophenol
[2-(2,5-Difluoro-phenylsulfanyl)-5-trifluoromethylsulfanyl-phenyl]-(1-methyl-piperidin-4-yl)-methanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg View Scheme |
2,5-Difluorothiophenol
6,9-difluoro-11-<2-(2,5-difluorophenylthio)phenyl>acetyldibenzothiepin-10-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 64 percent / KOH, Cu / H2O / 16 h / Heating 2: 0.25 g / polyphosphoric acid / 2.5 h / 120 - 125 °C View Scheme |
2,5-Difluorothiophenol
4-(2-Chloro-7-fluoro-11H-10-oxa-5-thia-dibenzo[a,d]cyclohepten-11-yl)-1-methyl-piperidine; hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 74 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg / 1) THF, 2) THF, reflux, 2 h 3: 36 percent / NaH / dimethylformamide / 1) RT, 2 h; 2) 50 deg C, 14 h 4: 0.35 g / 1) ethyl chloroformate, 2) KOH / 1) benzene, reflux, 1.5 h; 2) ethanol, 125 deg C, 2 h View Scheme |
2,5-Difluorothiophenol
8-Chloro-2-fluoro-6-(4-piperidyl)-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 74 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg / 1) THF, 2) THF, reflux, 2 h 3: 36 percent / NaH / dimethylformamide / 1) RT, 2 h; 2) 50 deg C, 14 h 4: 1) ethyl chloroformate, 2) KOH / 1) benzene, reflux, 1.5 h; 2) ethanol, 125 deg C, 2 h View Scheme |
2,5-Difluorothiophenol
2-fluoro-8-methoxy-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 39 percent / Cu / dimethylformamide / 6 h / 150 °C 2: 1) Mg / 1) THF, reflux, 1.5 h; 2) THF, reflux, 3 h 3: 61 percent / NaH / dimethylformamide; tetrahydrofuran / 11 h / 70 °C View Scheme |
2,5-Difluorothiophenol
8-Chloro-2-fluoro-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 74 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg / 1) THF, 2) THF, reflux, 2 h 3: 36 percent / NaH / dimethylformamide / 1) RT, 2 h; 2) 50 deg C, 14 h View Scheme |
2,5-Difluorothiophenol
1,4-difluoro-11-(4-methylpiperazino)-10,11-dihydrodibenzothiepin
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 64 percent / KOH, Cu / H2O / 16 h / Heating 2: 3.60 g / polyphosphoric acid / 2.5 h / 120 - 125 °C 3: 94 percent / NaBH4, aq. NaOH / ethanol; benzene / 4 h / Heating 4: 97 percent / HCl, CaCl2 / benzene / Ambient temperature 5: 67 percent / CHCl3 / 8 h / Heating View Scheme |
2,5-Difluorothiophenol
2-(2,5-Difluorophenylthio)-5-methoxy-α-(1-methyl-4-piperidyl)benzyl Alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 39 percent / Cu / dimethylformamide / 6 h / 150 °C 2: 1) Mg / 1) THF, reflux, 1.5 h; 2) THF, reflux, 3 h View Scheme |
2,5-Difluorothiophenol
8-Chloro-2-fluoro-6-<1-(2-hydroxyethyl)-4-piperidyl>-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 74 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg / 1) THF, 2) THF, reflux, 2 h 3: 36 percent / NaH / dimethylformamide / 1) RT, 2 h; 2) 50 deg C, 14 h 4: 1) ethyl chloroformate, 2) KOH / 1) benzene, reflux, 1.5 h; 2) ethanol, 125 deg C, 2 h 5: 69 percent / K2CO3 / acetone / 6 h / Heating View Scheme |
2,5-Difluorothiophenol
2-Fluoro-8-(trifluoromethylthio)-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 75 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg 3: 21 percent / NaH / dimethylformamide / 15 h / 70 °C View Scheme |
2,5-Difluorothiophenol
8-Chloro-6-<1-(2-decanoyloxyethyl)-4-piperidyl>-2-fluoro-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 74 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 100 °C 2: 1) Mg / 1) THF, 2) THF, reflux, 2 h 3: 36 percent / NaH / dimethylformamide / 1) RT, 2 h; 2) 50 deg C, 14 h 4: 1) ethyl chloroformate, 2) KOH / 1) benzene, reflux, 1.5 h; 2) ethanol, 125 deg C, 2 h 5: 69 percent / K2CO3 / acetone / 6 h / Heating 6: 55 percent / xylene / 6 h / Heating View Scheme |
2,5-Difluorothiophenol
6,9-difluoro-4H-thieno[3,2-c]thiochromene-2-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: sodium hydroxide / water / 0.08 h / 0 °C 1.2: 70 °C 1.3: 0 °C 2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C 3.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere 3.2: Cooling with ice 4.1: trichlorophosphate / 2 h / 0 - 80 °C 5.1: sodium ethanolate / ethanol / 0 - 70 °C 6.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 60 - 68 °C 6.2: 20 °C / pH 2 View Scheme |
2,5-Difluorothiophenol
ethyl 6,9-difluoro-4H-thieno[3,2-c]thiochromene-2-carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: sodium hydroxide / water / 0.08 h / 0 °C 1.2: 70 °C 1.3: 0 °C 2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C 3.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere 3.2: Cooling with ice 4.1: trichlorophosphate / 2 h / 0 - 80 °C 5.1: sodium ethanolate / ethanol / 0 - 70 °C View Scheme |
2,5-Difluorothiophenol
5,8-difluorothiochroman-4-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydroxide / water / 0.08 h / 0 °C 1.2: 70 °C 1.3: 0 °C 2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C 3.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere 3.2: Cooling with ice View Scheme |
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