DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:627-31-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Min.Order:10 Gram
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Type:Trading Company
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1,3-Diiodopropane CAS:627-31-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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Min.Order:10 Gram
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inquiry1,3-Diiodopropane Chemical Properties Melting point -20°C Boiling point 111-113 °C/31 mmHg (lit.) density 2.576 g/mL at 25 °C (lit.) refractive index n20/D 1.642(lit.) Fp >230 °F storage temp. 2-8°C form
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Min.Order:1 Kilogram
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Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Cas:627-31-6
Min.Order:0
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Conditions | Yield |
---|---|
With sodium iodide In acetone at 50℃; | 99% |
With potassium iodide In acetone for 72h; Reflux; Inert atmosphere; | 63% |
With ethanol; potassium iodide |
1,3-propanediylbis{triphenylplumbane}
A
iodobenzene
B
1,3-Diiodopropane
Conditions | Yield |
---|---|
With I2 In chloroform-d1 (N2), stirred, treated with 6 equiv I2 at 25°C; filtered; NMR, IR, mass. spectra; | A 87% B 72% C 90% |
Conditions | Yield |
---|---|
With diphosphorous tetraiodide In carbon disulfide for 4h; Ambient temperature; | A 15% B 68% C 2% |
3-chloropropyl thiocyanate
A
1,3-Diiodopropane
B
1,3-bis(thiocyanato)propane
C
3-iodopropyl thiocyanate
Conditions | Yield |
---|---|
With sodium iodide In acetone for 24h; Finkelstein Reaction; Reflux; | A n/a B n/a C 24% |
Conditions | Yield |
---|---|
With water; dibenzoyl peroxide at 95℃; under 312591 - 330978 Torr; |
1,3-Diiodopropane
Conditions | Yield |
---|---|
at 25℃; beim Aufbewehren; |
1,5-bis(p-toluenesulphonyl)-1,5-diazacyclooctane
acetone
methyl iodide
A
1,3-Diiodopropane
B
tertamethylammonium iodide
Conditions | Yield |
---|---|
at 160℃; |
Conditions | Yield |
---|---|
With acetone; sodium iodide |
Conditions | Yield |
---|---|
With acetone; sodium iodide |
Conditions | Yield |
---|---|
With triphenyl phosphite |
Conditions | Yield |
---|---|
With hydrogen iodide | |
With hydrogen iodide at 100℃; | |
With phosphorous triiodide | |
With N,N'-dicyclohexyl-N-methylcarbodiimidium iodide In tetrahydrofuran | |
(i) P2I4, CS2, (ii) K2CO3; Multistep reaction; |
Conditions | Yield |
---|---|
With lead(IV) acetate; iodine In tetrachloromethane Irradiation; |
Conditions | Yield |
---|---|
With sodium iodide In acetone Heating; |
Conditions | Yield |
---|---|
at 250℃; |
N,N-dimethyl-formamide
1,3-dibromo-propane
A
propene
B
1,3-Diiodopropane
Conditions | Yield |
---|---|
at 170℃; |
3-butoxypropanol
hydrogen iodide
A
1-iodo-butane
B
1,3-Diiodopropane
1,3-Diiodopropane
7,16-dimethyl-7,16-diaza-1,4,10,13-tetraoxacyclooctadecane
C17H36N2O4(2+)*2I(1-)
Conditions | Yield |
---|---|
In acetone at 25℃; under 10000 Torr; for 20h; | 100% |
Conditions | Yield |
---|---|
In acetonitrile for 48h; Inert atmosphere; Reflux; | 100% |
In acetonitrile for 72h; Heating; | 95% |
In acetonitrile for 48h; Reflux; | 85% |
In acetonitrile at 90℃; for 72h; | 85% |
1,3-Diiodopropane
diisopropyl phthalate
diisopropyl cis-2,3-dihydro-1H-indene-3a,7a-dicarboxylate
Conditions | Yield |
---|---|
Stage #1: diisopropyl phthalate With (trimethylstannyl)lithium In tetrahydrofuran; diethyl ether at -78℃; for 1h; Stage #2: 1,3-Diiodopropane In tetrahydrofuran; diethyl ether at -78℃; for 1h; | 99% |
Conditions | Yield |
---|---|
Stage #1: benzene-1,2,4-tricarboxylic acid trimethyl ester With (trimethylstannyl)lithium In tetrahydrofuran; diethyl ether at -78℃; for 1h; Stage #2: 1,3-Diiodopropane In tetrahydrofuran; diethyl ether at -78 - 20℃; for 3h; | 99% |
Conditions | Yield |
---|---|
In acetonitrile Inert atmosphere; Reflux; | 98% |
In acetonitrile Inert atmosphere; Reflux; | 90.6% |
In acetonitrile Inert atmosphere; Reflux; | 89% |
In acetonitrile Inert atmosphere; Reflux; | 77% |
In acetonitrile at 85℃; |
1,4-diaza-bicyclo[2.2.2]octane
1,3-Diiodopropane
1,1'-(1,3-propanediyl)bis<4-aza-1-azoniabicyclo<2.2.2>octane> diiodide
Conditions | Yield |
---|---|
In acetone at 20℃; for 14h; | 97% |
1H-perimidine-2(3H)-thione
1,3-Diiodopropane
10,11-dihydro-(9H)-1,3-thiazino<3,2-a>perimidine
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate In acetonitrile for 0.333333h; Heating; | 97% |
1,3-Diiodopropane
4,5-bis(2'-cyanoethylthio)-4,5-dimethyl-tetrathiafulvalene
1,3-bis[3(2-cyanoethylthio)-6,7-bis(methyl)tetrathiafulvalen-2-ylthio]propane
Conditions | Yield |
---|---|
Stage #1: 4,5-bis(2'-cyanoethylthio)-4,5-dimethyl-tetrathiafulvalene With cesium hydroxide In methanol; N,N-dimethyl-formamide for 0.25h; Stage #2: 1,3-Diiodopropane In methanol; N,N-dimethyl-formamide for 2h; Further stages.; | 97% |
1,3-Diiodopropane
N,N'-bis(2-methylphenyl)formamidine
Conditions | Yield |
---|---|
Stage #1: 1,3-Diiodopropane; N,N'-bis(2-methylphenyl)formamidine With potassium carbonate In acetonitrile Reflux; Inert atmosphere; Stage #2: With sodium tetrafluoroborate In water; acetonitrile at 20℃; for 0.166667h; | 97% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In ethanol for 8h; Reflux; | 96.5% |
1,3-Diiodopropane
2,3-bis(2-cyanoethylseleno)-6,7-ethylenediselenotetrathiafulvalene
1,3-bis[3(2-cyanoethylseleno)-6,7-ethylenediselenotetrathiafulvalen-2-ylseleno]propane
Conditions | Yield |
---|---|
Stage #1: 2,3-bis(2-cyanoethylseleno)-6,7-ethylenediselenotetrathiafulvalene With cesium hydroxide In methanol; N,N-dimethyl-formamide for 0.25h; Stage #2: 1,3-Diiodopropane In methanol; N,N-dimethyl-formamide for 2h; Further stages.; | 96% |
1,3-Diiodopropane
1-[3-(trimethoxysilyl)propyl]imidazole
Conditions | Yield |
---|---|
at 110℃; for 17h; | 96% |
1,3-Diiodopropane
Pyridine-2,5-dicarboxylic acid diisopropyl ester
(RS)-2,3-dihydroindolizine-6,8a(1H)-dicarboxylic acid diisopropyl ester
Conditions | Yield |
---|---|
Stage #1: Pyridine-2,5-dicarboxylic acid diisopropyl ester With (trimethylstannyl)lithium In tetrahydrofuran; diethyl ether at -78℃; for 1h; Stage #2: 1,3-Diiodopropane In tetrahydrofuran; diethyl ether at -78 - 20℃; for 16h; | 96% |
Conditions | Yield |
---|---|
With ammonium acetate; tetrabutyl-ammonium chloride; potassium carbonate In water at 20℃; for 10h; | 96% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In ethanol for 8h; Reflux; | 96% |
1,3-Diiodopropane
Conditions | Yield |
---|---|
Stage #1: tert-butyl 2-((ethylthio)carbonyl)hydrazine-1-carboxylate With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine In tetrahydrofuran at 0℃; for 0.166667h; Stage #2: 1,3-Diiodopropane In tetrahydrofuran at 0℃; for 1h; Reagent/catalyst; Solvent; | 96% |
1,3-Diiodopropane
(pyridin-1-iumyl)[(pyridin-2-yl)aminide]
Conditions | Yield |
---|---|
In acetone at 20℃; | 95% |
1,3-Diiodopropane
4,5-bis(cyanoethylthio)-1,3-dithiole-2-[(4,5-ethylenedithio)-1,3-dithiole-2-ylidene]
1,3-bis[3(2-cyanoethylthio)-6,7-ethylenedithiotetrathiafulvalen-2-ylthio]propane
Conditions | Yield |
---|---|
Stage #1: 4,5-bis(cyanoethylthio)-1,3-dithiole-2-[(4,5-ethylenedithio)-1,3-dithiole-2-ylidene] With cesium hydroxide In methanol; N,N-dimethyl-formamide for 0.25h; Stage #2: 1,3-Diiodopropane In methanol; N,N-dimethyl-formamide for 2h; Further stages.; | 95% |
1,3-Diiodopropane
Conditions | Yield |
---|---|
With BuLi In tetrahydrofuran N2-atmosphere; stirring (room temp., 1 h); evapn., chromy. (alumina, hexane / CH2Cl2), crystn. (CH2Cl2 / pentane); elem. anal.; | 95% |
Conditions | Yield |
---|---|
In acetonitrile for 5h; Reflux; | 95% |
Conditions | Yield |
---|---|
In toluene for 24h; Reflux; | 94.24% |
In acetonitrile for 24h; Inert atmosphere; Reflux; | 75% |
1,3-Diiodopropane
3-(2-aminophenyl)-4-methyl-1,3-thiazole-2(3H)-thione
Conditions | Yield |
---|---|
In chloroform for 24h; Reflux; | 94% |
1,3-Diiodopropane
4-(Triphenylphosphoranylidenamino)pyridin
Conditions | Yield |
---|---|
In acetonitrile at 85℃; for 18h; | 94% |
(dimethylamino(methyl))carbene(pentacarbonyl)tungsten(0)
1,3-Diiodopropane
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane (Ar or N2); W-compound in THF treated with n-BuLi in hexane at -78°C, stirred (-78°C, 30 min), treated with 1,3-diiodopropane, stirred (6 h), warmed to 25°C; solvent removed (vac.), flash chromy. (silica gel, 20% CH2Cl2/80% hexane), yellow fractions are collected, solvent removed under vac.; elem. anal.; | 93% |
1,3-Diiodopropane
malonic acid dimethyl ester
dimethyl 2,6-bis(methoxycarbonyl)heptandioate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20 - 100℃; for 28h; | 93% |
1,3-Diiodopropane
Potassium; 2,2,5,5-tetrakis-trifluoromethyl-2,5-dihydro-thiazole-4-thiolate
4,4'-<1,3-Propandiylbis(thio)bis<2,5-dihydro-2,2,5,5-tetrakis(trifluormethyl)thiazol>>
Conditions | Yield |
---|---|
In acetonitrile for 2h; Heating; | 92% |
1,3-Diiodopropane
1,5,9-triazatricyclo[7.3.1.05,13 ]tridecane
Conditions | Yield |
---|---|
92% |
1,3-Diiodopropane
(S)-2-(diphenylmethyl)pyrrolidine
Conditions | Yield |
---|---|
With potassium carbonate In ethanol for 8h; Heating; | 92% |
1,3-Diiodopropane
N-(1,3-dimethylimidazolidin-2-ylidene)pyridin-4-amine
Conditions | Yield |
---|---|
In acetonitrile Inert atmosphere; Reflux; | 92% |
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