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Cas:123-15-9
Min.Order:1 Metric Ton
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Cas:123-15-9
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Cas:123-15-9
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Cas:123-15-9
Min.Order:1 Gram
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inquiryProduct name: 2-Methylpentanal CAS No.:123-15-9 Molecule Formula:C6H12O Molecule Weight:100.16 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:123-15-9
Min.Order:1 Kilogram
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Cas:123-15-9
Min.Order:1 Kilogram
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Cas:123-15-9
Min.Order:10 Milligram
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inquiryProduct name: Methyl valeraldehyde CAS#: 123-15-9 EINECS#:204-605-2 Molecular formula: C6H12O Molecular weight:100.16 Appearance:Colorless liquid Storage:Keep in a cool, dry, dark location in a tightly sealed container or cylinder Por
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Cas:123-15-9
Min.Order:10 Gram
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Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrakis(acetonitrile)copper(I)tetrafluoroborate; oxygen In acetonitrile at 20℃; for 11h; | 98% |
With 1-methyl-1H-imidazole; [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrakisacetonitrile copper(I) trifluoromethanesulfonate; oxygen In acetonitrile at 20℃; for 11h; | 98% |
With manganese(II) nitrate; C70H128N16O4; oxygen; cobalt(II) nitrate In acetic acid at 25℃; for 1h; Mechanism; | 97% |
Conditions | Yield |
---|---|
With acetylacetonatodicarbonylrhodium(l); hydrogen; triphenylphosphine In neat (no solvent) at 80℃; under 7500.75 Torr; for 1h; Catalytic behavior; Time; Autoclave; | A 11.1% B 83.7% |
With hydrogen; (polymer-PPh2)2Ru(CO)3 In benzene at 140℃; under 51714.8 Torr; for 20h; Product distribution; further temperature, pressure; other catalysts; | |
With water; dodecacarbonyltetrairidium In methanol at 150℃; under 41371.8 Torr; for 0.5h; Product distribution; other group 8 transition-metal catalysts; |
1-Methoxy-2-methyl-pentan-2-ol
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With phosphoric acid at 100℃; for 3h; | 83% |
(E)-2-methylpent-2-enal
A
2-methylpent-2-enoic acid
B
2-methylvaleraldehyde
C
(S)-2-methylpentanoic acid
Conditions | Yield |
---|---|
With aldehyde dehydrogenase from E.coli; ene-reductase from Saccharomyces cerevisiae; NADH In aq. phosphate buffer at 30℃; for 0.75h; pH=7; Enzymatic reaction; stereoselective reaction; | A 13% B 6% C 77% |
propionaldehyde
A
propan-1-ol
B
2-methylpentan-1-ol
C
2-methyl-2-pentenal
D
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; nickel; molybdenum at 180℃; under 51714.8 Torr; Product distribution; Further Variations:; Catalysts; Temperatures; | A 69.1% B 12.3% C 1% D 7.9% |
2-Methylpentanoic acid
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With isobutylmagnesium bromide; bis(cyclopentadienyl)titanium dichloride In diethyl ether for 4h; Ambient temperature; | 65% |
With hydrogen; 2,2-dimethylpropanoic anhydride; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 80℃; under 22501.8 Torr; for 24h; | 64 % Spectr. |
With hydrogen; 2,2-dimethylpropanoic anhydride; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 80℃; under 22501.8 Torr; for 24h; | 64 % Spectr. |
Conditions | Yield |
---|---|
Stage #1: 2,2,6,6-tetramethyl-1-(pent-1-enyl)piperidine; methyl iodide In [D3]acetonitrile for 3h; Stage #2: With water; sodium acetate; acetic acid | 30% |
(E)-2-methylpent-2-enal
A
2-methylpent-2-enoic acid
B
2-Methylpentanoic acid
C
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With aldehyde dehydrogenase from E.coli; ene-reductase from Saccharomyces cerevisiae; NADH In aq. phosphate buffer at 30℃; for 0.5h; pH=7; Time; Enzymatic reaction; | A 11% B 29% C 8% |
carbon monoxide
2-pentene
A
2-Ethylbutyraldehyde
B
2-methylvaleraldehyde
C
hexanal
Conditions | Yield |
---|---|
With hydrogen In methoxybenzene at 120℃; under 37503 Torr; for 6h; Product distribution; Further Variations:; Reagents; Pressures; Temperatures; | A n/a B n/a C 20% |
Conditions | Yield |
---|---|
In acetonitrile Ambient temperature; electrochemical synthesis: divided cell, Pt plate electrodes, -2.30 V vs Ag/Ag(+), Br as supporting electrolyte; | 5% |
Conditions | Yield |
---|---|
With aluminum oxide; silver at 250℃; |
3-methyl-3-propyl-oxiranecarboxylic acid ethyl ester
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With sodium hydroxide Versetzen der Reaktionsloesung mit Schwefelsaeure und Erhitzen des Reaktionsprodukts bis auf 200grad; | |
(i) NaOH, (ii) H+, (iii) (decarboxylation); Multistep reaction; |
2-methylpentan-1-ol
A
2-methylvaleraldehyde
B
2-methylpentyl 2-methylpentanoate
Conditions | Yield |
---|---|
With sodium dichromate; sulfuric acid |
2-methyl-2-pentenal
A
2-methylpentan-1-ol
B
2-methylvaleraldehyde
Conditions | Yield |
---|---|
at 200℃; Druckhydrierung an Nickel-Kieselgur; |
2-methyl-2-pentenal
A
2-methyl-pent-2-en-1-ol
B
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With ethanol; hydrogen; palladium |
2-methyl-2-pentenal
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With acetic acid | |
With ethanol; palladium Hydrogenation; | |
With nickel In diethyl ether |
Conditions | Yield |
---|---|
With nickel Hydrogenation; | |
With hydrogen; palladium on activated charcoal In diethyl ether for 24h; | |
With glucose dehydrogenase; β-D-glucose; ene-reductase from Enterobacter cloacae; NADH In aq. phosphate buffer at 30℃; for 1h; pH=7; Reagent/catalyst; Enzymatic reaction; |
Conditions | Yield |
---|---|
With sodium hydroxide; pentacarbonyl iron |
diethylborinic acid (E)-2-methyl-pent-1-enyl ester
2-methylvaleraldehyde
Conditions | Yield |
---|---|
In methanol |
Conditions | Yield |
---|---|
(i) EtMgBr, THF, (ii) /BRN= 505937/; Multistep reaction; |
ethyl-phenyl-borinic acid (E)-2-methyl-pent-1-enyl ester
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With acetylacetone at 80℃; |
2-Methylpentanoic acid
formic acid ethyl ester
2-methylvaleraldehyde
Conditions | Yield |
---|---|
(i) LDA, (ii) /BRN= 906769/, aq. HCl; Multistep reaction; |
Conditions | Yield |
---|---|
(i) iBu2NH, benzene, (ii) /BRN= 969135/, MeCN; Multistep reaction; |
Conditions | Yield |
---|---|
(i) benzene, (ii) aq. NaOAc, AcOH; Multistep reaction; |
Conditions | Yield |
---|---|
In acetonitrile |
Conditions | Yield |
---|---|
With ethylmagnesium bromide Yield given. Multistep reaction; |
(E)-pent-2-ene
carbon monoxide
A
2-Ethylbutyraldehyde
B
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With hydrogen; cobaltcluster at 150℃; under 51154.1 - 57829.6 Torr; for 22.5h; Mechanism; Product distribution; determination of selectivity, velocity and decomposition of cluster; also with phosphanes; other temperatures, pressures and times; | |
With hydrogen; acetylacetonatodicarbonylrhodium(l) In dichloromethane at 120℃; under 15514.9 Torr; for 16h; |
1-penten
A
2-methylpentan-1-ol
B
2-methylvaleraldehyde
C
hexanal
D
hexan-1-ol
Conditions | Yield |
---|---|
With carbon monoxide; hydrogen; 3*Co(CO)8 In octane at 180℃; under 24823.1 - 26374.6 Torr; for 14h; Product distribution; n-Pentadecane; |
Conditions | Yield |
---|---|
With Graphite In acetonitrile at 20℃; for 2h; Irradiation; | 100% |
With Benzoylformic acid In Petroleum ether at 20℃; Irradiation; Green chemistry; |
2-methylvaleraldehyde
2-Methylpentanoic acid
Conditions | Yield |
---|---|
With C4H11FeMo6NO24(3-)*3C16H36N(1+); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 8h; Green chemistry; | 99% |
With 4H3N*4H(1+)*CuMo6O18(OH)6(4-); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 12h; | 99% |
With 2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In acetonitrile at 20℃; | 80% |
2-methylvaleraldehyde
S-<1-(3,6,9-trioxadecyl)benzimidazol-2-yl>hexanethioate
A
Hexanoic acid (Z)-2-methyl-pent-1-enyl ester
Conditions | Yield |
---|---|
With cesium fluoride In N,N-dimethyl-formamide; benzene for 48h; Ambient temperature; | A 97% B n/a |
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In ethyl acetate for 2h; Heating; | 97% |
Conditions | Yield |
---|---|
With (S)-1-(2-(diphenylphosphanyl)naphthalen-1-yl)isoquinoline; copper(I) bromide In toluene at 20℃; for 43h; Schlenk technique; Inert atmosphere; Molecular sieve; enantioselective reaction; | 97% |
Conditions | Yield |
---|---|
With [[{(2,6-iPr2C6H3N)P(Ph2)}2N]AlH]+[HB(C6F5)3]- In toluene at 20℃; for 3h; Schlenk technique; Glovebox; | 97% |
Conditions | Yield |
---|---|
With L-isoleucine; potassium hydroxide In chloroform at 25℃; for 14h; Michael Addition; stereoselective reaction; | 96% |
Conditions | Yield |
---|---|
Stage #1: nitromethane; 2-methylvaleraldehyde With sodium hydroxide In ethanol; water at 4 - 20℃; Stage #2: With hydrogenchloride In water pH=~ 7; | 94.2% |
With potassium fluoride In isopropyl alcohol at 20℃; for 14h; | 62% |
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; water | 93.3% |
2-methylvaleraldehyde
Conditions | Yield |
---|---|
With 1,1,1,3,3,3-hexamethyl-disilazane; cobalt(II) bromide at 110℃; for 6h; | 93% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; sodium bromide In water; 1,2-dichloro-ethane at 20℃; for 18h; Irradiation; Green chemistry; | 93% |
With trifluorormethanesulfonic acid; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; ammonium bromide In toluene at 60℃; for 22h; Irradiation; Inert atmosphere; | 32% |
2-methylvaleraldehyde
S-tert-butylsulfinimide
Conditions | Yield |
---|---|
With benzyl bromide; zinc In tetrahydrofuran at 20℃; | 91% |
Conditions | Yield |
---|---|
With L-isoleucine; potassium hydroxide In chloroform at 25℃; for 40h; Michael Addition; stereoselective reaction; | 91% |
2-methylvaleraldehyde
Conditions | Yield |
---|---|
methyltrioxorhenium(VII) for 144h; | 90% |
2-methylvaleraldehyde
Conditions | Yield |
---|---|
Stage #1: [((4-methoxy-2-methylbutan-2-yl)oxy)diphenylsilyl]methyl phenyl sulfone With lithium hexamethyldisilazane at 0℃; for 0.25h; Peterson Olefination; Inert atmosphere; Stage #2: 2-methylvaleraldehyde at 0℃; for 2h; Peterson Olefination; Inert atmosphere; stereoselective reaction; | 90% |
2-methylvaleraldehyde
2-methylpentyl 2-methylpentanoate
Conditions | Yield |
---|---|
With trimethylaluminum; benzene-1,2-diol; isopropyl alcohol In dichloromethane at 20℃; for 2h; | 89% |
Conditions | Yield |
---|---|
With L-isoleucine; potassium hydroxide In chloroform at 25℃; for 35h; Michael Addition; stereoselective reaction; | 89% |
Conditions | Yield |
---|---|
With borax; disodium hydrogenphosphate; ethylenediaminetetraacetic acid; bis(dibutylethyl)hexamethylenediammonium hydroxide; triethylamine In water at 25℃; pH=10; Electrochemical reaction; | 88.4% |
2-methylvaleraldehyde
di-isopropyl azodicarboxylate
(+)-2-[N,N'-bis(isopropanoxycarbonyl)hydrazino]-2-(n-propyl)-propionaldehyde
Conditions | Yield |
---|---|
With L-3-(naphthalen-1-yl)alanine hydrochloride In tetrahydrofuran at 0℃; for 15h; | 88% |
With (S)-N-((1R,2R)-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)cyclohexyl)pyrrolidine-2-carboxamide; salicylic acid In dichloromethane at 0℃; for 45h; enantioselective reaction; |
Conditions | Yield |
---|---|
Stage #1: 2-methylvaleraldehyde With hydroxylamine hydrochloride In dimethyl sulfoxide at 100℃; Stage #2: With water; dihydrogen peroxide; sodium hydroxide In dimethyl sulfoxide | 87% |
With trimethylsilylazide; tetrabutylammomium bromide; iron(II) bromide In neat (no solvent) at 60℃; for 4h; Irradiation; | 70% |
2-methylvaleraldehyde
Diethyl phosphonate
(1-Hydroxy-2-methyl-pentyl)-phosphonic acid diethyl ester
Conditions | Yield |
---|---|
triethylamine Ambient temperature; | 86.1% |
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In 1,2-dichloro-benzene at 130℃; for 12h; Minisci Aromatic Substitution; Sealed tube; regioselective reaction; | 86% |
Stage #1: isoquinoline With trifluoroacetic acid In 1,2-dichloro-ethane at 20℃; for 0.0833333h; Stage #2: 2-methylvaleraldehyde With oxygen In 1,2-dichloro-ethane at 0 - 115℃; under 760.051 Torr; for 16h; | 60% |
Conditions | Yield |
---|---|
Stage #1: pyrid-2-ylhydrazine; 2-methylvaleraldehyde In acetic acid at 20℃; for 0.0833333h; Stage #2: With chromium(VI) oxide In acetic acid at 110℃; for 0.25h; | 86% |
Multi-step reaction with 2 steps 1: acetonitrile / 20 °C / Green chemistry 2: tetrabutylammonium tetrafluoroborate / acetonitrile; water / 4 h / 70 °C / Electrolysis; Green chemistry View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide; cetyltrimethylammonium chloride for 2h; Ambient temperature; | 85% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium iodide In acetonitrile for 1.5h; Heating; | 85% |
With hydroxylamine hydrochloride In dimethyl sulfoxide at 100℃; for 1h; | 71% |
Conditions | Yield |
---|---|
With 1-((1R,2R)-2-aminocyclohexyl)-3-(((1R,4aS,10ar)-7-isopropyl-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthren-1-yl)methyl)thiourea In dichloromethane at 25℃; for 48h; Michael Addition; stereoselective reaction; | 85% |
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; manganese(II) acetate In 1,2-dichloro-benzene at 130℃; for 6h; Inert atmosphere; Sealed tube; | 84% |
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