CAS No.100-97-0,Hexamethylenetetramine Suppliers,MSDS download

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Synthetic route

: 2691-41-0
octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With 1-Benzyl-1,4-dihydronicotinamide In N,N-dimethyl-formamide for 24h; Kinetics; Ambient temperature; Irradiation; other nitramines, var. solvents, var. temperatures;	100%

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With borohydride exchange resin; nickel diacetate In methanol for 3h;	100%

: C17H30B2O2

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ammonium hydroxide; Fe(H)2(1,2-bis(dimethylphosphino)ethane)2 In tetrahydrofuran at 20 - 60℃; for 36h; Reagent/catalyst; Schlenk technique; Glovebox; Inert atmosphere;	98%

: 50-00-0
formaldehyd

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ammonium hydroxide In water Schlenk technique; Glovebox; Inert atmosphere;	97%
With ammonium hydroxide at 15 - 20℃;	83%
With ammonium sulfate

: 50-00-0
formaldehyd

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

A: 107-46-0
Hexamethyldisiloxane

B: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
In N,N-dimethyl-formamide for 1h;	A 93% B 77%

...Expand

: 50-00-0
formaldehyd

A: 5962-66-3
1,3,5-dithiazinane

B: 281-20-9
1,5-dithia-3,7-diazabicyclo<3.3.1>nonane

C: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ammonium hydroxide; hydrogen sulfide In water at 15℃;	A 4% B 44% C 29%
With ammonium hydroxide; hydrogen sulfide In water at 40℃;	A 5% B 19% C 42%

...Expand

: 2035-89-4
N-methyl-N-(methyleneamino)methanamine

: 107-13-1
acrylonitrile

A: 34714-77-7
dimethylaminomethyleneacetonitrile

B: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With hydroquinone In acetonitrile at 100℃; for 10h; Product distribution;	A 36% B 12%

...Expand

: (1,2-di-tert-butyldiaziridin-3-ylidene)(methyl)amine

A: 691-24-7
1,3-di-tert-butylcarbodiimide

B: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With sodium hydride In cyclohexane at 180℃; for 0.583333h;	A n/a B 32%

: 5805-57-2
2-Aminomethylbenzimidazole

: 75-09-2
dichloromethane

A: 100-97-0
hexamethylenetetramine

B: 7H,16H-8,17-Methano-9H,18H-benzimidazolo<1,2-c><8,2'>-spiro-benzimidazolidino<1,3,6>triazonin

Conditions

Conditions	Yield
With ammonia at 40℃; for 10h;	A 12% B 27%

...Expand

: 34557-54-5
methane

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ammonia; oxygen; copper at 500 - 700℃;
With silver copper; ammonia; oxygen at 500 - 700℃;

: 75-09-2
dichloromethane

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ammonium hydroxide at 100 - 120℃;
With sodium hydroxide; ammonia at 100 - 120℃;
With ammonium hydroxide at 100 - 120℃;

: 26940-74-9, 59481-40-2, 59481-41-3, 81646-16-4
hexamethylenetetramine; compound with phenol

: 71-43-2
benzene

A: 100-97-0
hexamethylenetetramine

B: 108-95-2
phenol

...Expand

: 135-19-3
β-naphthol

A: 100-97-0
hexamethylenetetramine

B: 1096-84-0
bis(2-hydroxy-1-naphthyl)methane

C: 77204-14-9
1,3-diformyl-2-naphthol

D: 77204-15-0
2-formyl-2,3-dihydro-1H-naphth<1,2-e><1,3>oxazine

Conditions

Conditions	Yield
With hydrogenchloride; acetic acid 1) 2h, steambath, 2) 30 min.; Yield given. Multistep reaction. Yields of byproduct given;

...Expand

: 2-c,3-t-diisopropyl-1-r-methyltriaziridin

A: 15464-00-3
azobisisopropane

B: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
for 10h; Product distribution; thermolysis;

: 4857-04-9
2-chloromethyl-1H-benzimidazole

: 75-09-2
dichloromethane

A: 100-97-0
hexamethylenetetramine

B: 7H,16H-8,17-Methano-9H,18H-benzimidazolo<1,2-c><8,2'>-spiro-benzimidazolidino<1,3,6>triazonin

Conditions

Conditions	Yield
With ammonia at 40℃; for 10h; Yield given. Yields of byproduct given;

...Expand

: 50-00-0
formaldehyd

: 74-89-5
methylamine

A: 100-97-0
hexamethylenetetramine

B: N-methylhexamethylenetetrammonium fluoride

Conditions

Conditions	Yield
With hydrogen fluoride; ammonia In methanol

...Expand

: 56-81-5
glycerol

A: 100-97-0
hexamethylenetetramine

B: 541-43-5
barium formate

Conditions

Conditions	Yield
With barium dihydroxide; phosphoric acid; ammonia; periodic acid Product distribution; multistep reaction;

: 50-00-0
formaldehyd

ammonium carbonate: ammonium carbonate

: 100-97-0
hexamethylenetetramine

carbon monoxide: carbon monoxide

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With nickel kieselguhr; ammonia; hydrogen at 250 - 280℃;

: 67-56-1
methanol

NH3: NH3

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With water bei der Beruehrung mit einem gluehenden Nickel-Draht;

: 50-00-0
formaldehyd

NH3: NH3

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With water

: 64-17-5
ethanol

NH3: NH3

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
bei der Einwirkung dunkler elektrischer Entladungen;

: 75-09-2
dichloromethane

NH3: NH3

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ethanol at 125℃;

: 5342-31-4
bis(benzoyloxy)methane

NH3: NH3

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ethanol

methylene glycol diacetate: methylene glycol diacetate

NH3: NH3

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With ethanol

polyoxymethylene: polyoxymethylene

NH3: NH3

: 100-97-0
hexamethylenetetramine

: 7664-41-7
ammonia

: sodium amide

: 106-89-8
epichlorohydrin

A: 35042-52-5
(E)-2-penten-4-yn-1-ol

B: 100-97-0
hexamethylenetetramine

C: 107-19-7
propargyl alcohol

...Expand

: 13372-32-2
5-methyl-4-oxo-1,3-dioxolane

: 7664-41-7
ammonia

A: 100-97-0
hexamethylenetetramine

B: 598-81-2, 2043-43-8, 65144-02-7, 89673-71-2
(+/-)-lactamide

...Expand

: 63579-00-0
tris(chloromethyl)-s-triazinetrione

: 7664-41-7
ammonia

A: 100-97-0
hexamethylenetetramine

B: ammonium chloride

C: 108-80-5
isocyanuric acid

Conditions

Conditions	Yield
at 100℃;

...Expand

: 1476-11-5
Z-1,4-dichlorobutene

: 100-97-0
hexamethylenetetramine

: 117175-09-4
1-<(Z)-4-Chloro-2-butenyl>-1-azonia-3,5,7-triazatricyclo<3.3.1.1.3,7>decane chloride

Conditions

Conditions	Yield
In dichloromethane for 5h; Reflux; Large scale reaction;	100%
In ethanol; chloroform for 4h; Heating;	99%
In chloroform at 60℃; for 4h;	94%
In chloroform for 4h; Heating;	91%
In chloroform for 4h; Reflux;	91%

: 19381-40-9
1-(3-(benzyloxy)phenyl)-2-bromoethanone

: 100-97-0
hexamethylenetetramine

: 115851-98-4
1-[2-(3-Benzyloxy-phenyl)-2-oxo-ethyl]-3,5,7-triaza-1-azonia-tricyclo[3.3.1.13,7]decane; bromide

Conditions

Conditions	Yield
In diethyl ether; chloroform Ambient temperature;	100%

: 100-97-0
hexamethylenetetramine

: 3752-97-4
1,4-bis(chloromethyl)-2,5-dimethoxybenzene

: 114558-97-3
1,1'-(2,5-dimethoxy-p-xylylene)-bis-hexamethylenetetraminium; dichloride

Conditions

Conditions	Yield
In dichloromethane for 16h; Heating;	100%
In chloroform 1.) reflux, 30 min, 2.) r.t., overnight;
In chloroform at 90℃; for 24h;

: 100-97-0
hexamethylenetetramine

: 99-81-0
4-Nitrophenacyl bromide

: 88260-40-6
(4-nitrophenacyl)hexaminium bromide

Conditions

Conditions	Yield
In chloroform for 2h;	100%
In chloroform at 20℃; for 12h; Delepine reaction;

: 100-97-0
hexamethylenetetramine

: 3289-75-6
2-chloro-N-(4-chlorophenyl)acetamide

: 79988-56-0
N,N'-methylenebis<3-(4-chlorophenyl)>-4-imidazolidinone

Conditions

Conditions	Yield
In ethanol 60 deg C, 1 h, then reflux, 1.5 h;	100%

: 100-97-0
hexamethylenetetramine

: 74-88-4
methyl iodide

: 50982-79-1
N-methylhexamethylenetetrammonium iodide

Conditions

Conditions	Yield
In chloroform at 20℃;	100%
at 80℃; for 7h; Temperature;	95.8%
In ethanol
In chloroform

: 100-97-0
hexamethylenetetramine

: 60254-03-7
4-tert-butyl-2-(diphenyl-phosphinoyl)-phenol

: 5-tert-butyl-3-(diphenyl-phosphinoyl)-2-hydroxy-benzaldehyde

Conditions

Conditions	Yield
With trifluoroacetic acid for 20h; Heating;	100%

: 858037-60-2
1-benzo[1,3]dioxol-5-yl-2-(2,5-dichloro-phenyl)-ethane-1,2-dione

: 100-97-0
hexamethylenetetramine

: 858037-61-3
5-benzo[1,3]dioxol-5-yl-4-(2,5-dichloro-phenyl)-1H-imidazole

Conditions

Conditions	Yield
With ammonium acetate In acetic acid at 95℃; for 2.5h;	100%

: 835-64-3
2-(2-Hydroxyphenyl)benzoxazole

: 100-97-0
hexamethylenetetramine

: 1275589-01-9
5-(1,3-benzoxazol-2-yl)-4-hydroxyisophthalic aldehyde

Conditions

Conditions	Yield
With trifluoroacetic acid for 48h; Reflux;	100%
With acetic acid In toluene for 18h; Duff reaction; Reflux;	91%
With trifluoroacetic acid Reflux;	91%

: 100-97-0
hexamethylenetetramine

: 2100-42-7
2-chloro-1,4-dimethoxybenzene

: 90064-48-5
2,5-dimethoxy-4-chlorobenzaldehyde

Conditions

Conditions	Yield
With trifluoroacetic acid at 95℃; for 5h;	100%
With trifluoroacetic acid at 95℃;	72.7%

: 120-47-8
Ethyl 4-hydroxybenzoate

: 100-97-0
hexamethylenetetramine

: 329904-04-3
3,5-diformyl-4-hydroxybenzoic acid ethyl ester

Conditions

Conditions	Yield
Stage #1: Ethyl 4-hydroxybenzoate; hexamethylenetetramine With trifluoroacetic acid Reflux; Stage #2: With water at 20 - 80℃; for 2h;	100%
With trifluoroacetic acid
With trifluoroacetic acid Duff Aldehyde Synthesis; Reflux;
With trifluoroacetic acid Duff Aldehyde Synthesis;

: 100-97-0
hexamethylenetetramine

: 99-96-7
4-hydroxy-benzoic acid

: 1384440-57-6
3,5-diformyl-4-hydroxybenzoic acid

Conditions

Conditions	Yield
Stage #1: hexamethylenetetramine; 4-hydroxy-benzoic acid With trifluoroacetic acid for 72h; Reflux; Stage #2: With water at 20 - 80℃; for 4h;	100%
With trifluoroacetic acid at 110℃; for 48h;	70%
With trifluoroacetic acid at 110℃; for 48h;	70%

: cyclopentadienecarboxylic acid manganese tricarbonyl

: 100-97-0
hexamethylenetetramine

: 1416228-92-6
C9H5MnO5*C6H12N4

Conditions

Conditions	Yield
In methanol at 20 - 60℃; Darkness;	100%

: 60468-36-2
α-chloro-2',5'-difluoroacetophenone

: 100-97-0
hexamethylenetetramine

: 1-(2,5-difluorophenyl)ethanone-2-hexamethylentetrammonium chloride

Conditions

Conditions	Yield
In chloroform Solvent; Temperature; Reflux;	100%

: 100-97-0
hexamethylenetetramine

: 69267-75-0
2-bromo-1-cyclopropylethan-1-one

: 1-(2-cyclopropyl-2-oxoethyl)-3,5,7-triaza-1-azoniatricyclo[3.3.1.13,7]decane bromide

Conditions

Conditions	Yield
In chloroform at 20℃; for 12h;	100%
In chloroform at 20℃; for 12h;	100%

: 542-75-6
E/Z-1,3-Dichloropropene

: 100-97-0
hexamethylenetetramine

: 1-(3-chloroallyl)-3,5,7-triaza-1-azoniaadamantane chloride

Conditions

Conditions	Yield
In chloroform at 60℃; for 12h;	99.9%

: 100-97-0
hexamethylenetetramine

: 452-07-3
2,4-difluorobenzyl chloride

: (2,4-difluoro-benzyl)-hexamethylenetetraminium; chloride

Conditions

Conditions	Yield
In toluene for 2h; Solvent; Reflux; Industrial scale;	99.9%

: 10436-39-2
1,1,2,3-Tetrachloropropene

: 100-97-0
hexamethylenetetramine

: N-β,γ,γ-trichloroallylhexamethylenetetramine chloride

Conditions

Conditions	Yield
In chloroform at 60℃; for 12h;	99.6%

: 100-97-0
hexamethylenetetramine

: 16395-67-8
tris-(chloromethyl)amine

Conditions

Conditions	Yield
With phosphorus pentachloride at 100℃; for 5.5h; Neat (no solvent);	99%
With phosphorus pentachloride
With phosphorus pentachloride

: 63158-38-3
2-bromoacetyl-1-methyl-5-nitropyrrole

: 100-97-0
hexamethylenetetramine

: 1-[2-(1-methyl-5-nitro-1H-pyrrol-2-yl)-2-oxo-ethyl]-3,5,7-triaza-1-azonia-tricyclo[3.3.1.13,7]decane; bromide

Conditions

Conditions	Yield
In chloroform Alkylation;	99%
In chloroform	99%

: 100-97-0
hexamethylenetetramine

: 256950-23-9
2-bromo-1-[5-fluoro-2-(methylthio)phenyl]ethanone

: 1-[5-fluoro-2-(methylthio)phenyl]ethanone-2-hexaminium bromide

Conditions

Conditions	Yield
In chloroform at 20℃;	99%

: 100-97-0
hexamethylenetetramine

: 1835-02-5
2-Bromo-1-(3,4-dimethoxyphenyl)ethanone

: 1234216-77-3
2-hexamethylenetetramino-1-(3,4-dimethoxyphenyl)ethanone-2-ium bromide

Conditions

Conditions	Yield
In chloroform at 20℃; for 4h;	99%
In chloroform at 20℃;

: 100-97-0
hexamethylenetetramine

: 1528493-04-0
C76H120O4

: 1528492-99-0
C78H120O6

Conditions

Conditions	Yield
Stage #1: hexamethylenetetramine; C76H120O4 With trifluoroacetic acid at 125℃; for 4h; Stage #2: With hydrogenchloride; water In dichloromethane at 20℃; for 3h;	99%

: 100-97-0
hexamethylenetetramine

: 301221-79-4
4-Bromoacetyl-1-(t-butoxycarbonyl)piperidine

: 1-[2-(1-tert-butoxycarbonyl-piperidin-4-yl)-2-oxo-ethyl]-3,5,7-triaza-1-azonia-tricyclo[3.3.1.13,7]decane bromide

Conditions

Conditions	Yield
In chloroform at 50℃; for 1h;	99%

: 100-97-0
hexamethylenetetramine

: (Z)-3-chloro-2-fl uoro-1-phenylpropene

: (Z)-N-(2-fluoro-3-phenylallyl)urotropinium chloride

Conditions

Conditions	Yield
In dichloromethane for 24h; Reflux;	99%

: 533939-04-7
6-ethyl-1H-pyrrolo[2,3-b]pyridine

: 100-97-0
hexamethylenetetramine

: 6-ethyl-1H-pyrrolo[2,3-b]pyridine-3-carbaldehyde

Conditions

Conditions	Yield
With acetic acid In water at 120℃; for 8h;	99%

: 100-97-0
hexamethylenetetramine

: 2-bromo-1-(tetrahydro-2H-pyran-3-yl)ethan-1-one

: rac-1-{2-[oxan-3-yl]-2-oxoethyl}-1,3,5,7-tetraazatricyclo[3.3.1.13,7]decan-1-ium bromide

Conditions

Conditions	Yield
In chloroform at 20℃; for 12h;	99%

: 271-63-6
7-Azaindole

: 100-97-0
hexamethylenetetramine

: 4649-09-6
1H-pyrrolo[2,3-b]pyridin-3-carbaldehyde

Conditions

Conditions	Yield
With propionic acid In ethanol at 80℃; for 6h; Temperature;	98.9%
Stage #1: 7-Azaindole; hexamethylenetetramine With acetic acid for 6h; Duff reaction; Heating; Stage #2: With water at 20℃; Further stages.;	77%
With acetic acid In water for 12h; Heating / reflux;	76%

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