Taizhou FremChem Co. Ltd. is a high-tech enterprise located in China Medical City specializing in R&D, manufacturing, sales of new APIS, pharmaceutical intermediates and fine chemicals. All of our company is committed to provide high quality chemical
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:271-63-6
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:271-63-6
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inquiryHigh quality 7-Azaindole CAS 271-63-6 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, F
Cas:271-63-6
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inquiryProduct description: Product name 7-Azaindole CAS number 271-63-6 Assay ≥98% Appearance Off-white powder Capacity 200mt/year Application Organic synthesis More info
high quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:271-63-6
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Name: 7-Azaindole Synonyms: 1,7-Diaza-1H-indene;7-Aza-7H-indole;7-Dideazapurine;7-Azaindole, 98% 5GR;NSC 67063;NSC 77951;7-AZAINDOLE FOR SYNTHESIS 1 G;7-Azaindole SynonyMs 1H-Pyrrolo[2,3-b]pyridine CAS: 271-63-6 MF:
Cas:271-63-6
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inquiryAbout Product Details 7-Azaindole Basic information Product Name: 7-Azaindole Synonyms: 1,7-Diaza-1H-indene;7-Aza-7H-indole;7-Aza-1-pyrindine;7H-Pyrrolo[2,3-b]pyridine;Pyrrolo(2,3
Cas:271-63-6
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:271-63-6
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:271-63-6
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powder 2. Fact
Cas:271-63-6
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inquiryName: 1H-Pyrrolo[2,3-b]pyridine Molecular Formula:C7H6N2 Molecular Weight:118.14 CAS No.:271-63-6 Appearance:Similar White Or Slight Yellow Solid Appearance:Similar White Or Slight Yellow Solid Storage:Store in cool and dry place, away from su
Our Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
Cas:271-63-6
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Cas:271-63-6
Min.Order:1 Kilogram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
7-Azaindole CAS:271-63-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:271-63-6
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Product Detail Minimum Order Qty. 10 Gram
Cas:271-63-6
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:271-63-6
Min.Order:10 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
NewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:271-63-6
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1-(tert-butoxycarbonyl)-1H-pyrrolo<2,3-b>pyridine
7-Azaindole
Conditions | Yield |
---|---|
With sodium carbonate In 1,2-dimethoxyethane; water for 20h; Heating; | 100% |
With water at 100℃; for 1h; | 99% |
With potassium phosphate In methanol at 120℃; under 5171.62 Torr; for 0.0333333h; Microwave irradiation; | 98% |
tert-butyl (3-methylpyridin-2-yl)carbamate
7-Azaindole
Conditions | Yield |
---|---|
Stage #1: tert-butyl (3-methylpyridin-2-yl)carbamate With n-butyllithium; N,N-dimethyl-formamide In tetrahydrofuran at 0℃; Stage #2: With hydrogenchloride In tetrahydrofuran; water at 50℃; | 100% |
With n-butyllithium In tetrahydrofuran; hexane; N,N-dimethyl-formamide at -15 - 25℃; for 17.5h; | 3.8 g |
Stage #1: tert-butyl (3-methylpyridin-2-yl)carbamate With trimethylsilyl bromide In tetrahydrofuran; N,N-dimethyl-formamide at -30℃; for 1.75h; Inert atmosphere; Stage #2: With hydrogenchloride In tetrahydrofuran; water; N,N-dimethyl-formamide at 0 - 40℃; for 3h; | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran / 4 h / 0 °C 1.2: 0 °C 2.1: hydrogenchloride / water / 8 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Stage #1: methyl bromide; tert-butyl (3-methylpyridin-2-yl)carbamate In diethyl ether at 0℃; for 4h; Stage #2: With N,N-dimethyl-formamide In diethyl ether at 0℃; for 0.5h; Concentration; | 99.1% |
7-azaindoline
7-Azaindole
Conditions | Yield |
---|---|
With carbon dioxide; DBN; Eosin Y In dimethyl sulfoxide at 25 - 30℃; for 48h; Irradiation; | 97% |
With potassium tert-butylate In decane at 150℃; for 36h; Inert atmosphere; Schlenk technique; | 90% |
With 4-tert-Butylcatechol; oxygen In water at 20℃; for 20h; Green chemistry; | 90% |
(Z)-2-amino-3-(2-ethoxyethenyl)pyridine
7-Azaindole
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 2h; Heating; | 94% |
1-(2-amino-3-pyridinyl)-1-ethanone
7-Azaindole
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water at 90℃; pH=3; Temperature; pH-value; Microwave irradiation; | 93.2% |
1-benzenesulfonyl-1H-pyrrolo[2,3-b]pyridine
7-Azaindole
Conditions | Yield |
---|---|
With sodium t-butanolate In 1,4-dioxane at 80℃; for 3h; Inert atmosphere; | 93% |
7-azaindole-2-carboxylic acid
7-Azaindole
Conditions | Yield |
---|---|
With zinc(II) oxide In toluene at 90℃; for 2h; Temperature; | 91.8% |
1H-Pyrrolo[2,3-b]pyridine-7-oxide
7-Azaindole
Conditions | Yield |
---|---|
With (4,4′-di-tert-butyl-2,2′-bipyridine)bis[(2-pyridinyl)phenyl]iridium(III) hexafluorophosphate; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In acetonitrile at 20℃; for 2h; Inert atmosphere; Irradiation; chemoselective reaction; | 91% |
With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate In dichloromethane at 31℃; for 16h; Sealed tube; Irradiation; | 83% |
With styrene; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; hydrazine hydrate In dimethyl sulfoxide at 20℃; for 13h; Inert atmosphere; Irradiation; chemoselective reaction; | 74% |
1-[(4-methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridine
7-Azaindole
Conditions | Yield |
---|---|
With cetyltrimethylammonim bromide; potassium hydroxide In tetrahydrofuran; water for 10h; Reagent/catalyst; Temperature; Time; Reflux; Green chemistry; | 90% |
With potassium tert-butylate In dimethyl sulfoxide at 20℃; for 1h; Inert atmosphere; Darkness; Schlenk technique; | 87% |
With formic acid; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 24h; Inert atmosphere; Sealed tube; Irradiation; | 70% |
With caesium carbonate In tetrahydrofuran; methanol at 22℃; for 2h; |
7-Azaindole
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] In benzene at 130℃; for 24h; Sealed tube; Glovebox; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With hydrogenchloride; water for 48h; Reflux; Large scale; | 72.9% |
5-fluoro-1H-pyrrolo[2,3‐b]pyridine
7-Azaindole
Conditions | Yield |
---|---|
With 2-methyl-propan-1-ol; methanesulfonato(2-dicyclohexylphosphino -2’,6’-di-i-propoxy-1,1‘-biphenyl)(2’-amino-1,1’-biphenyl-2-yl)palladium(II); sodium tert-pentoxide In toluene at 80℃; for 48h; Sealed tube; Inert atmosphere; | 68% |
tert-butyl (3-methylpyridin-2-yl)carbamate
N,N-dimethyl-formamide
7-Azaindole
Conditions | Yield |
---|---|
Stage #1: tert-butyl (3-methylpyridin-2-yl)carbamate With n-butyllithium In tetrahydrofuran at -10 - 0℃; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at 0 - 15℃; Stage #3: With hydrogenchloride; water at -5 - 5℃; | 67% |
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -20℃; for 5h; Reagent/catalyst; Inert atmosphere; | 65% |
2-phenyloxepino[2,3-b]pyridine
7-Azaindole
Conditions | Yield |
---|---|
With acetamide; potassium tert-butylate In dimethyl sulfoxide at 80℃; for 48h; Inert atmosphere; | 52% |
A
7-Azaindole
B
C10H14N2Si
Conditions | Yield |
---|---|
With sodium t-butanolate In 1,4-dioxane at 80℃; for 3h; Inert atmosphere; | A 44% B 42% |
3-ethenyl-2-nitropyridine
7-Azaindole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 1,10-Phenanthroline; carbon monoxide In acetonitrile at 120℃; under 4560.31 Torr; for 180h; | 41% |
1-acetyl-2,3-dihydropyrrolo<2,3-b>pyridine
7-Azaindole
Conditions | Yield |
---|---|
With n-Dodecylamine In 1,2-dichloro-ethane for 1h; Irradiation; | 25% |
7-Azaindole
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran; toluene at 90℃; for 0.5h; | 25% |
Conditions | Yield |
---|---|
With perchloric acid adsorbed on silica gel; anthranilic acid amide In acetonitrile at 80℃; for 12h; | 25% |
Conditions | Yield |
---|---|
With bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate; XPhos In tert-butyl alcohol at 110℃; for 24h; Sealed tube; Inert atmosphere; | 9% |
Conditions | Yield |
---|---|
With sodium ethanolate at 350℃; | |
With sodium formate; sodium anilide at 290 - 310℃; | |
With hydrogenchloride In diethyl ether; water; pentane at -20℃; Inert atmosphere; Reflux; |
1H-pyrrolo[2,3-b]pyridine-3,6-dicarboxylic acid
7-Azaindole
Conditions | Yield |
---|---|
at 320 - 330℃; |
oxirane
3-bromo-1H-pyrrolo[2,3-b]pyridine
A
7-Azaindole
B
1-(2-hydroxyethyl)-7-azaindole
C
3-(2-hydroxyethyl)-7-azaindole
Conditions | Yield |
---|---|
With n-butyllithium 1.) ether, 1,2-dimethoxyethane, -5 deg C, 1 h; 2.) 0 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given; |
7-Azaindole
Conditions | Yield |
---|---|
With hydrogenchloride for 8h; Heating; Yield given; |
1-(1H-pyrrolo[2,3-b]pyridin-1-yl)ethanone
A
7-Azaindole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 89 percent / H2 / Pd-C / ethanol; 1,2-dimethoxy-ethane / 5 h / 20 °C 2: 25 percent / dodecylamine / 1,2-dichloro-ethane / 1 h / Irradiation View Scheme |
2,2-dimethyl-N-(3-methylpyridin-2-yl)propionamide
7-Azaindole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) n-BuLi / 1.) THF, -5 to 0 deg C, 4 h, 2.) THF, 0 deg C, 40 min 2: 5.5 M HCl / 8 h / Heating View Scheme |
3-hydroxy-2-nitropyridine
7-Azaindole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 52 percent / 60percent NaH / benzene / 60 h / Heating 2: 74 percent / Pd(PPh3)2Cl2, Et4NCl / acetonitrile / 1 h / Heating 3: 78 percent / H2 / W-2 Raney Ni / methanol 4: 94 percent / conc. HCl / methanol / 2 h / Heating View Scheme |
7-Azaindole
chloroacetyl chloride
2-chloro-1-(1H-pyrrolo[2,3-b]pyridin-3-yl)ethan-1-one
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With aluminum (III) chloride In dichloromethane at 20℃; for 1.5h; Inert atmosphere; Stage #2: chloroacetyl chloride In dichloromethane at 0 - 20℃; for 18h; Inert atmosphere; | 100% |
With aluminium trichloride In carbon disulfide at 50℃; for 2h; | 82% |
With aluminium trichloride In carbon disulfide at 50℃; for 2h; Product distribution; | 81% |
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere; Stage #2: methyl iodide In N,N-dimethyl-formamide for 1h; Inert atmosphere; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere; Stage #2: methyl iodide In N,N-dimethyl-formamide for 1h; Inert atmosphere; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere; Stage #2: methyl iodide In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 98% |
7-Azaindole
(2-trimethylethylsilylethoxy)methyl chloride
1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1.25h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide; mineral oil for 1.25h; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1.25h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide; mineral oil for 1.25h; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide; mineral oil for 1h; | 100% |
7-Azaindole
7-nitroquinoxaline-2(1H)-one
Conditions | Yield |
---|---|
With trifluoroacetic acid In N,N-dimethyl-formamide at 80℃; for 1h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: n-pentyl halide In N,N-dimethyl-formamide at 20℃; for 15h; | 100% |
Conditions | Yield |
---|---|
With potassium phosphate; trans-1,2-Diaminocyclohexane; copper(l) iodide In 1,4-dioxane at 110℃; for 24h; | 100% |
With triethylamine In N,N-dimethyl-formamide at 110℃; for 3h; | 96% |
With copper(l) iodide; manganese(II) fluoride; (1R,2R)-1,2-diaminocyclohexane; potassium hydroxide In water at 60℃; for 24h; | 93% |
3-Bromopyridine
7-Azaindole
1-(pyridin-3-yl)-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
With potassium phosphate; trans-1,2-Diaminocyclohexane; copper(l) iodide In 1,4-dioxane at 110℃; for 95h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 1-Bromopentane In N,N-dimethyl-formamide at 20℃; for 3.5h; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 1-Bromopentane In N,N-dimethyl-formamide at 20℃; for 3.5h; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 1-Bromopentane In N,N-dimethyl-formamide at 20℃; for 3.5h; | 100% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; | 100% |
7-Azaindole
Conditions | Yield |
---|---|
With N-chloro-succinimide In tetrachloromethane; chloroform for 4h; Ambient temperature; | 99% |
With 1-aza-4,6,11-trioxa-5-boratricyclo[3.3.3.0(1,5)]undecane; nickel diacetate; chlorine at 90℃; for 3h; Reflux; | 99.3% |
With 1,3-dichloro-5,5-dimethylhydantoin In 1,4-dioxane at 80℃; for 0.5h; | 92% |
With sodium hypochlorite; sodium azide; acetic acid In water; toluene at 20℃; for 0.5h; | 91% |
With 1-chloro-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one In N,N-dimethyl-formamide at 20℃; for 12h; regioselective reaction; | 77% |
Conditions | Yield |
---|---|
With zinc diacetate In trifluoroacetic acid at 120℃; for 6h; Solvent; Concentration; | 99.1% |
7-Azaindole
3-bromo-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
With 1-aza-4,6,11-trioxa-5-boratricyclo[3.3.3.0(1,5)]undecane; bromine; nickel diacetate at 100℃; for 3h; Temperature; Reflux; | 99% |
With N-Bromosuccinimide In dichloromethane at 20℃; for 16h; | 96% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 4h; Cooling with ice; | 96% |
7-Azaindole
benzenesulfonyl chloride
1-benzenesulfonyl-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With tetrabutylammomium bromide; sodium hydroxide In dichloromethane Stage #2: benzenesulfonyl chloride In dichloromethane at 0 - 20℃; | 99% |
With dmap; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 98% |
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In dichloromethane at 20℃; for 2h; Cooling with ice; | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; Addition; Michael addition; | 99% |
7-Azaindole
3,5-dimethylphenyl iodide
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane; dodecane at 110℃; for 24h; | 99% |
With copper(I) oxide; potassium phosphate; N1,N2-bis(furan-2-ylmethyl)oxalamide In acetonitrile at 80℃; | 94% |
With potassium phosphate monohydrate; iron(III) chloride hexahydrate; trans-N,N'-dimethylcyclohexane-1,2-diamine In water at 135℃; for 24h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: n-butyl halide In N,N-dimethyl-formamide at 20℃; for 15h; | 99% |
7-Azaindole
tris(pentafluorophenyl)borate
7-[tris(pentafluorophenyl)borane]-7-azaindole
Conditions | Yield |
---|---|
In dichloromethane (N2); a soln. of ligand added at room temp. to a soln. of B(C6F5)3, stirred for 1 h; evapd. (vac.); elem. anal.; | 99% |
Conditions | Yield |
---|---|
With hafnium tetrakis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 0.2h; Inert atmosphere; regioselective reaction; | 99% |
3-iodopyridine
7-Azaindole
1-(pyridin-3-yl)-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
With manganese(II) fluoride; (S,S)-1,2-diaminocyclohexane; caesium carbonate In water at 130℃; for 24h; Reagent/catalyst; | 99% |
With copper(l) iodide; manganese(II) fluoride; (1R,2R)-1,2-diaminocyclohexane; potassium hydroxide In water at 100℃; for 48h; | 94% |
With copper(I) oxide; caesium carbonate In dimethyl sulfoxide at 100℃; for 24h; Reagent/catalyst; Solvent; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; Stage #2: bromopentene In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 99% |
7-Azaindole
hexamethylenetetramine
1H-pyrrolo[2,3-b]pyridin-3-carbaldehyde
Conditions | Yield |
---|---|
With propionic acid In ethanol at 80℃; for 6h; Temperature; | 98.9% |
Stage #1: 7-Azaindole; hexamethylenetetramine With acetic acid for 6h; Duff reaction; Heating; Stage #2: With water at 20℃; Further stages.; | 77% |
With acetic acid In water for 12h; Heating / reflux; | 76% |
7-Azaindole
cyclopentyl trimethoxysilane
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With n-butyllithium In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; Cooling with ice; Stage #2: cyclopentyl trimethoxysilane In tetrahydrofuran at 0 - 20℃; for 8h; Inert atmosphere; | 98.3% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 2h; Friedel-Crafts Alkylation; | 98.3% |
Conditions | Yield |
---|---|
In benzene for 2h; Heating; | 98% |
7-Azaindole
3-iodo-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With iodine In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; | 98% |
With iodine; potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.75h; Inert atmosphere; | 97% |
With iodine; potassium hydroxide In N,N-dimethyl-formamide at 20℃; | 97% |
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: n-propyl halide In N,N-dimethyl-formamide at 20℃; for 15h; | 98% |
7-Azaindole
Phenyl glycidyl ether
1-phenoxy-3-(1H-pyrrolo[2,3-b]pyridin-1-yl)propan-2-ol
Conditions | Yield |
---|---|
ruthenium trichloride at 20℃; for 4h; Friedel-Crafts alkylation; | 98% |
With ruthenium-exchanged FAU-Y zeolite at 20℃; for 0.5h; Friedel Crafts alkylation; Ultrasound irradiation; Neat (no solvent); regioselective reaction; | 98% |
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