Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:76513-69-4
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:76513-69-4
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inquiryItems Standard Result Appearance Colorless,transparent liquid Complies Content% ≥99.90
Cas:76513-69-4
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inquiryFactory supply 2-(Trimethylsilyl)ethoxymethyl chlorided CAS 76513-69-4 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its inte
Cas:76513-69-4
Min.Order:10 Kilogram
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:76513-69-4
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:76513-69-4
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:76513-69-4
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2-chloromethyl 2-(trimethylsilyl)ethyl ether CAS No. 76513-
Cas:76513-69-4
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:76513-69-4
Min.Order:1 Kilogram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:76513-69-4
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryName 2-(Trimethylsilyl)ethoxymethyl chloride Structural Formula CAS No. 76513-69-4 Molecular Formula
Cas:76513-69-4
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:76513-69-4
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inquiry2-(Trimethylsilyl)ethoxymethyl chloride CAS:76513-69-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
Cas:76513-69-4
Min.Order:1 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:76513-69-4
Min.Order:4 Kilogram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:76513-69-4
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:76513-69-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:76513-69-4
Min.Order:1 Gram
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inquiryProduct Name: 2-(Trimethylsilyl)ethoxymethyl chloride Synonyms: SEM-CHLORIDE;SEM-CI;SEM-CL;CHLOROMETHYL 2-TRIMETHYLSILYLETHYL ETHER;2-(TRIMETHYLSILYL)ETHOXYMETHYL CHLORIDE;2-(CHLOROMETHOXY)ETHYLTRIMETHYLSILANE;2-chloromethyl 2-(trimethylsily
Cas:76513-69-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:76513-69-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry2-(Trimethylsilyl)ethoxymethyl chloride Basic information Product Name: 2-(Trimethylsilyl)ethoxymethyl chloride Synonyms: SEM-CHLORIDE;SEM-CI;SEM-CL;2-(TRIMETHYLSILYL)ETHOXYMETHYL CHLORIDE;2-(CHLOROMETHOXY)ETHYLTRIMETHYLSILANE;CHLOROMETHYL 2-T
Cas:76513-69-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:76513-69-4
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryName: 2-(Trimethylsilyl) ethoxymethylchloride. Synonym:SEM-CHLORIDE;SEM-CI;SEM-CL;2-(TRIMETHYLSILYL)ETHOXYMETHYLCHLORIDE;2-(CHLOROMETHOXY)ETHYLTRIMETHYLSILANE;CHLOROMETHYL2-TRIMETHYLSILYLETHYLETHER;2-(Trimethylsilyl)ethoxymethylchloride,95%[0.1%d
Cas:76513-69-4
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Cas:76513-69-4
Min.Order:0
Negotiable
Type:Manufacturers
inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:76513-69-4
Min.Order:0
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Type:Lab/Research institutions
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Cas:76513-69-4
Min.Order:1 Kilogram
Negotiable
Type:Other
inquirychloro-trimethyl-silane
1-bromo-2-(chloromethoxy)ethane
(2-trimethylethylsilylethoxy)methyl chloride
Conditions | Yield |
---|---|
Stage #1: 1-bromo-2-(chloromethoxy)ethane With magnesium for 4h; Reflux; Stage #2: chloro-trimethyl-silane at 20℃; Reagent/catalyst; | 99% |
Stage #1: 1-bromo-2-(chloromethoxy)ethane With n-butyllithium; methylmagnesium chloride In tetrahydrofuran; hexane at 20 - 30℃; for 0.333333h; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at 20 - 30℃; for 0.333333h; | 85.8% |
Stage #1: 1-bromo-2-(chloromethoxy)ethane With n-butyllithium; butyl magnesium bromide In tetrahydrofuran; hexane at 15 - 30℃; for 0.333333h; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at 30℃; for 0.333333h; | 80.4% |
formaldehyd
2-(Trimethylsilyl)ethanol
(2-trimethylethylsilylethoxy)methyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride for 0.5h; | 90% |
With hydrogenchloride at 0℃; | 87% |
With hydrogenchloride for 0.433333h; | 85% |
1H-imidazole
(2-trimethylethylsilylethoxy)methyl chloride
1-((2-(trimethylsilyl)ethoxy)methyl)-1H-imidazole
Conditions | Yield |
---|---|
Stage #1: 1H-imidazole With sodium hydride In tetrahydrofuran at 0 - 25℃; for 0.5h; Inert atmosphere; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In tetrahydrofuran at 0 - 25℃; for 14h; Inert atmosphere; | 100% |
Stage #1: 1H-imidazole With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.75h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In tetrahydrofuran; mineral oil at 20℃; | 93% |
Stage #1: 1H-imidazole With potassium tert-butylate In dimethyl sulfoxide at 0℃; for 0.5h; Large scale; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In dimethyl sulfoxide at 0 - 15℃; for 16h; Large scale; | 90% |
1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-ribo-hex-1-enopyranose
(2-trimethylethylsilylethoxy)methyl chloride
1,5-anhydro-4,6-O-benzylidene-2-deoxy-3-O-<<2-(trimethylsilyl)ethoxy>methyl>-D-ribo-hex-1-enopyranose
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane for 5h; Ambient temperature; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(1R,7aS)-tetrahydro-1-methyl-1-(hydroxymethyl)-1H,3H-pyrrolo<1,2-c>oxazol-3-one
(1R,7aS)-tetrahydro-1-methyl-1-<<2-(trimethylsilyl)ethoxy>methoxy>methyl-1H,3H-pyrrolo<1,2-c>oxazol-3-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 14h; Ambient temperature; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 23℃; Yield given; |
(2-trimethylethylsilylethoxy)methyl chloride
N-(2-Allyl-phenyl)-4-hydroxy-butyramide
N-(2-Allyl-phenyl)-4-(2-trimethylsilanyl-ethoxymethoxy)-butyramide
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
methyl 3-bromo-5-chloro-2,4-dihydroxy-6-methylbenzoate
methyl 2,4-bis[2-(trimethylsilyl)ethoxymethoxy]-3-bromo-5-chloro-6-methylbenzoate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane Yield given; |
(2-trimethylethylsilylethoxy)methyl chloride
7-(4-tert-Butyldimethylsiloxy-2-hydroxybutyl)-1,4-dioxa-8-thiaspiro<4.5>dec-6-ene
7-<4-tert-Butyldimethylsilyloxy-2-(2-trimethylsilylethoxy)methoxybutyl>-1,4-dioxa-8-thiaspiro<4.5>dec-6-ene
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 14h; Ambient temperature; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
14-acetyl-12-<2'-(trimethylsilyl)ethoxymethoxy>podocarpa-8,11,13-triene
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 5h; Ambient temperature; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
ethyl (1R,2S,3R,4R)-2,3-dihydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohex-5-ene-1-carboxylate
ethyl (1R,2S,3R,4R)-2-hydroxy-4-methoxy-5-methyl-3-(2-trimethylsilylethoxymethoxy)-2-(2-trimethylsilyl-3-furyl)cyclohex-5-ene-1-carboxylate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h; | 96% |
(2-trimethylethylsilylethoxy)methyl chloride
(2S)-1-benzyloxy-2-butanol
[2-((S)-1-Benzyloxymethyl-propoxymethoxy)-ethyl]-trimethyl-silane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane Ambient temperature; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(2R,3S,4S,5R)-2,5-bis[N-(benzyloxycarbonyl)amino]-1,6-diphenyl-3,4-hexanediol
dibenzyl ((2R,3S,4S,5R)-1,6-diphenyl-3,4-bis((2-(trimethylsilyl)ethoxy)methoxy)hexane-2,5-diyl)dicarbamate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 16h; Ambient temperature; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; Inert atmosphere; Reflux; | 77% |
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 18h; Ambient temperature; |
4'-hydroxy-2'-methylacetophenone
(2-trimethylethylsilylethoxy)methyl chloride
1-[4-Methyl-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-ethanone
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 0℃; for 1h; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(4S)-4-((2R)-2-hydroxypent-4-enyl)-2,2-dimethyl-1,3-dioxolane
{2-[(R)-1-((S)-2,2-Dimethyl-[1,3]dioxolan-4-ylmethyl)-but-3-enyloxymethoxy]-ethyl}-trimethyl-silane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 16h; Ambient temperature; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(5Z,11E,13E)-(9S,10S)-1-(tert-Butyl-dimethyl-silanyloxy)-16-chloro-9-methoxy-15-(1-methoxy-1-methyl-ethoxy)-6,10,14-trimethyl-hexadeca-5,11,13-trien-4-ol
(3E,5E,11Z)-(7S,8S)-16-(tert-Butyl-dimethyl-silanyloxy)-1-chloro-8-methoxy-2-(1-methoxy-1-methyl-ethoxy)-3,7,11-trimethyl-13-(2-trimethylsilanyl-ethoxymethoxy)-hexadeca-3,5,11-triene
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; diisopropylamine In dichloromethane for 2h; Heating; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
methyl 6-hydroxynaphthalene-2-carboxylate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 6h; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
methyl 7-hydroxy-2-naphthalenecarboxylate
methyl 7-(2-trimethylsilyl-ethoxymethoxy)-naphthalene-2-carboxylate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 6h; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(2R,3S,4S,5R)-6-Benzyloxy-4,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-methyl-1-phenylsulfanyl-hexan-3-ol
C38H68O5SSi3
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane for 6h; Heating; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(2R,5S,8R,3E,6E)-8-tert-butyldimethylsilyloxy-2-chloroacetoxy-5-hydroxytrideca-4,6-dienyl 2,2-dimethylpropanoate
(2R,5S,8R,3E,6E)-8-tert-butyldimethylsilyloxy-2-chloroacetoxy-5-(2-trimethylsilyl)ethoxytrideca-4,6-dienyl 2,2-dimethylpropanoate
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In dichloromethane Substitution; | 100% |
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; | 100% |
2-hydroxybromobenzene
(2-trimethylethylsilylethoxy)methyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 2h; | 100% |
With N,N-diethyl-N-isopropylamine In dichloromethane at 0 - 20℃; | 95% |
With aluminum oxide; potassium fluoride In 1,2-dimethoxyethane at 25℃; | 92% |
(2-trimethylethylsilylethoxy)methyl chloride
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-hydroxybutanoate
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
(2-trimethylethylsilylethoxy)methyl chloride
Conditions | Yield |
---|---|
Stage #1: N-benzyloxycarbonyl-C-(2H-tetrazol-5-yl)methylamine With caesium carbonate In methanol at 20℃; for 2h; deprotonation; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide at 20℃; for 18h; Alkylation; Further stages.; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(S)-2-((4R,5S)-4,8-Dimethyl-spiro[4.5]deca-1,7-dien-1-yl)-2-hydroxy-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
(S)-2-((4R,5S)-4,8-Dimethyl-spiro[4.5]deca-1,7-dien-1-yl)-2-(2-trimethylsilanyl-ethoxymethoxy)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In dichloromethane at 50℃; for 14h; | 100% |
With 1-amino-3-methylbutane; tetra-(n-butyl)ammonium iodide In dichloromethane at 50℃; for 14h; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(5R,6R)-6-hydroxymethyl-5-[(1E)-3-[(4-methoxyphenyl)methoxy]-1-[[[tris-(1-methylethyl)silyl]oxy]methyl]-1-propenyl]-2-(2-nitrophenyl)-2-cyclohexen-1-one
(5R,6R)-5-[(1E)-3-[(4-methoxyphenyl)methoxy]-1-[[[tris-(1-methylethyl)silyl]oxy]methyl]-1-propenyl]-2-(2-nitrophenyl)-6-[[[2-(trimethylsilyl)ethoxy]methoxy]methyl]-2-cyclohexen-1-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
1,1,1,3,3,3-hexafluoro-2-(1,3-thiazol-2-yl)propan-2-ol
2-{1-trifluoromethyl-1-[(2-trimethylsilylethoxy)methoxy]-2,2,2-trifluoroethyl}thiazole
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 48h; | 100% |
(2-trimethylethylsilylethoxy)methyl chloride
(3aR,5aR,6S,9S,9aR,9bR)-9-(tert-butyldimethylsiloxy)-3,3a,4,5a,6,7,8,9,9a,9b-decahydro-6-hydroxy-9b-[3-(methoxymethoxy)propyl]-2,3,3,5a-tetramethyl-5H-benz[e]inden-5-one
(3aR,5aR,6S,9S,9aR,9bR)-9-(tert-butyldimethylsiloxy)-3,3a,4,5a,6,7,8,9,9a,9b-decahydro-9b-[3-(methoxymethoxy)propyl]-2,3,3,5a-tetramethyl-6-[[2-(trimethylsilyl)ethoxy]methoxy]-5H-benz[e]inden-5-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide In dichloromethane at 20℃; | 100% |
N-(2-iodo-4-methoxyphenyl)-1-{tert-butyloxycarbonyl}pyrrolidine-3-carboxamide
(2-trimethylethylsilylethoxy)methyl chloride
N-(2-(trimethylsilyl)ethoxymethyl)-N-[2-iodo-4-methoxyphenyl]-1-{tert-butyloxycarbonyl}pyrrolidine-3-carboxamide
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 3h; | 100% |
7-Azaindole
(2-trimethylethylsilylethoxy)methyl chloride
1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1.25h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide; mineral oil for 1.25h; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1.25h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide; mineral oil for 1.25h; | 100% |
Stage #1: 7-Azaindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide; mineral oil for 1h; | 100% |
(2S,4S)-2-(4-chlorobenzyloxymethyl)-4-(1-chloroisoquinoline-5-sulfonylamino)-pyrrolidine-1-carboxylic acid tert-butyl ester
(2-trimethylethylsilylethoxy)methyl chloride
(2S,4S)-2-(4-chlorobenzyloxymethyl)-4-[(1-chloroisoquinoline-5-sulfonyl)-(2-trimethylsilylethoxymethyl)amino]-pyrrolidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 0℃; for 1.5h; | 100% |
2-bromophenylethyl alcohol
(2-trimethylethylsilylethoxy)methyl chloride
{2-[2-(2-bromo-phenyl)-ethoxymethoxy]-ethyl}-trimethyl-silane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine | 100% |
8-bromo-6-methoxy-4-oxo-1,4-dihydroquinoline-2-carboxylic acid methyl ester
(2-trimethylethylsilylethoxy)methyl chloride
8-bromo-6-methoxy-4-(2-trimethylsilanyl-ethoxymethoxy)-quinoline-2-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With sodium hydride In 1-methyl-pyrrolidin-2-one at 20℃; for 2.5h; | 100% |
In 1-methyl-pyrrolidin-2-one | |
In 1-methyl-pyrrolidin-2-one | |
In 1-methyl-pyrrolidin-2-one |
ethyl 1H-imidazole-2-carboxylate
(2-trimethylethylsilylethoxy)methyl chloride
ethyl 1-((2-(trimethylsilyl)ethoxy)methyl)-1H-imidazole-2-carboxylate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 25℃; for 12h; Concentration; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 100% |
Stage #1: ethyl 1H-imidazole-2-carboxylate With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.333333h; Inert atmosphere; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In tetrahydrofuran; mineral oil at 0 - 20℃; for 2.5h; Inert atmosphere; | 95% |
With potassium carbonate In acetone at 0 - 20℃; for 16h; | 85% |
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